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The goal of this research is to investigate the fundamentals of fracturing processes in heterogeneous materials such as concrete using geophysical methods and dynamic micromechanical models. This work describes how different aspects of fracture formation in concrete can be investigated using a combination of Acoustic Emission (AE) techniques, ultrasonic wave velocity imaging, and high resolution Computed Tomography (CT). Fracture formation and evolution were studied during shear failure of large reinforced concrete beams and compressive failure of concrete samples. AE analysis includes studying complex spatial and temporal fracture development that precedes shear failure. Predominant microcrack mechanisms were analyzed at different stages of fracture formation. CT images were used to investigate the influence of concrete microstructure on fracture topography. Combined AE and CT damage evaluation techniques revealed different aspects of fracture development, thus expanding our understanding of AE events and their mechanisms. These images show how aggregate particles influence fracture nucleation and development. An emphasis has been placed on the role of coarse aggregates during the interlocking of fracture surfaces at transferring shear stresses. Ultrasonic wave velocity and AE techniques have been applied to uniaxial compression tests of concrete with various aggregate sizes and strengths similar to that of the concrete beams. AE parameters, p-wave velocities, and stress-strain data have been analyzed concurrently to image damage evolution under compression. Influence of material composition on microcracking and material state changes during loading has been investigated in detail. The results of compressive tests were used as building blocks for developing realistic micromechanical numerical models of concrete. The models were designed using a distinct element code, where material is modelled through the combination of bonded particles. A number of procedures were developed to transfer the exact microstructure of material incorporating its visual representation into the model. The models’ behaviour has been verified against experimental data. It was shown that these models exhibit realistic micromechanical behaviour. The results of the experimental investigation of concrete fracturing were expanded by modelling more cases with aggregate size and strength variations. It was shown that geophysical imaging techniques, along with advanced micromechanical numerical modelling, can help us understand damage formation and evolution.

The goal of this research is to investigate the fundamentals of fracturing processes in heterogeneous materials such as concrete using geophysical methods and dynamic micromechanical models. This work describes how different aspects of fracture formation in concrete can be investigated using a combination of Acoustic Emission (AE) techniques, ultrasonic wave velocity imaging, and high resolution Computed Tomography (CT). Fracture formation and evolution were studied during shear failure of large reinforced concrete beams and compressive failure of concrete samples. AE analysis includes studying complex spatial and temporal fracture development that precedes shear failure. Predominant microcrack mechanisms were analyzed at different stages of fracture formation. CT images were used to investigate the influence of concrete microstructure on fracture topography. Combined AE and CT damage evaluation techniques revealed different aspects of fracture development, thus expanding our understanding of AE events and their mechanisms. These images show how aggregate particles influence fracture nucleation and development. An emphasis has been placed on the role of coarse aggregates during the interlocking of fracture surfaces at transferring shear stresses. Ultrasonic wave velocity and AE techniques have been applied to uniaxial compression tests of concrete with various aggregate sizes and strengths similar to that of the concrete beams. AE parameters, p-wave velocities, and stress-strain data have been analyzed concurrently to image damage evolution under compression. Influence of material composition on microcracking and material state changes during loading has been investigated in detail. The results of compressive tests were used as building blocks for developing realistic micromechanical numerical models of concrete. The models were designed using a distinct element code, where material is modelled through the combination of bonded particles. A number of procedures were developed to transfer the exact microstructure of material incorporating its visual representation into the model. The models’ behaviour has been verified against experimental data. It was shown that these models exhibit realistic micromechanical behaviour. The results of the experimental investigation of concrete fracturing were expanded by modelling more cases with aggregate size and strength variations. It was shown that geophysical imaging techniques, along with advanced micromechanical numerical modelling, can help us understand damage formation and evolution.

Orientador: Raquel Gonçalves / Dissertação (mestrado) - Universidade Estadual de Campinas, Faculdade de Engenharia Agricola / Made available in DSpace on 2018-08-07T23:01:52Z (GMT). No. of bitstreams: 1 Trinca_AlexJulio_M.pdf: 4149749 bytes, checksum: 34fcccdf02d4f1b0b171e121e4eb5ac3 (MD5) Previous issue date: 2006 / Resumo: é praticamente toda exportada em sua forma in natura sem que a ela seja agregado valor de beneficiamento. Um dos problemas enfrentados pela indústria moveleira é o fato da madeira não ser submetida à classificação, dificultando a elaboração de projetos e a certificação da qualidade do móvel confeccionado a partir deste material. Nesse contexto as empresas moveleiras brasileiras buscam parâmetros para composição e certificação de seu produto, sendo atualmente a norma brasileira ¿Projeto de Estruturas de Madeira¿ ¿ NBR 7190/97, o único instrumento norteador para a caracterização de propriedades da madeira. No entanto, nesse setor as dificuldades para a obtenção de corpos-de-prova nas dimensões especificadas por esse texto normativo têm gerado dúvidas quanto aos resultados de caracterização de propriedades, de maneira que este trabalho teve como objetivo principal verificar se os valores do módulo de elasticidade e da tensão de ruptura no ensaio de compressão paralela às fibras podem ser considerados estatisticamente equivalentes, desde que sejam mantidas a proporcionalidade da dimensão do corpo-de-prova. Para isso adotou-se, como alternativa ao corpo-de-prova proposto pela NBR 7190/97, a dimensão 0,03 m x 0,03 m x 0,09 m. Os ensaios foram realizados utilizando-se 7 diferentes espécies de madeira com densidades variadas, buscando-se, com essa amostragem, a generalização dos resultados. Como objetivo secundário se buscou avaliar a influência das dimensões do corpo-de-prova e da freqüência do transdutor na velocidade de propagação de ondas de ultra-som na direção longitudinal. As espécies adotadas foram: Cerejeira (Torresea sp), Perobinha (Paratecoma peroba) , Cabreúva-vermelha (Myroxylon peruiferum), Angico-preto (Anadenanthera macrocarpa), Garapeira (Apuleia leiocarpa), Eucalipto grandis ( Eucalyptus grandis) e Pinus elliotti (Pinus elliottii). Todos os corpos-de-prova foram ensaiados com aproximadamente 12% de umidade e os ensaios foram realizados em ambiente controlado (21° C ± 1°C). Os resultados permitiram concluir que a hipótese foi verdadeira para todas as espécies estudadas quando se considera a tensão de ruptura / Abstract: Most of the exported wood in Brazil is unprocessed, without any aggregated value. To change this scenario technology for wood processing and qualification are required. One of the problems faced by the furniture industry refers to the non classification of the wood, which cause difficulties to projects elaboration and quality certification of the furniture made from this material. In this context the Brazilian Industries of furniture seek for parameters to certificate its products, and the NBR 7190/97 standard ¿Project of Structures of Wood " is, nowadays, the only instrument for the characterization of wood properties. However, for the furniture industry it is very difficult to obtaining the dimensions specified by the standard. This research had as main objective to verify if the means values of the modulus of elasticity and rupture in compression parallel to the grain can be considerate statistically equal, when smaller specimen are used, if the proportionality is maintained. For that it was adopted, as alternative to the specimen proposed by NBR 7190/97, the dimension 0.03 x 0.03 x 0.09 m. For the experiments there were used 7 different species with varied densities. The secondary objective was to evaluate the influence of the specimen size and of the transducer frequency in the speed of ultrasound wave propagation in the longitudinal direction. The adopted species were: Cerejeira (Amburana cearensis), Perobinha (Paratecoma peroba), Cabreúva vermelha (Myroxylon peruiferum), Angico-preto (Anadenanthera macrocarpa), Garapeira (Apulleia leiocarpa), Eucalyptus grandis, (Eucalyptus grandis) and Pinus ellioti (Pinus elliottii). All specimens were tested with approximately 12% moisture content and were accomplished in controlled atmosphere (21° C ± 1°C). The results allowed concluding that the hypothesis was true for all the studied species when the rupture in compression parallel to the grain was considered. For the module of elasticity this hypothesis was not confirmed for two species, from the seven evaluated (garapeira e eucalipto). Although, the mean difference between the results obtained in the tests using both specimens size was 10%, smaller then the maximum allowed variability in mechanical tests (18%). For the ultrasonic velocity propagation four species did not presents statistical variation with the modification of the size of the specimens - cerejeira, garapeira, pinus and eucalyptus while for the perobinha, angico and cabreúva the ultrasonic wave velocity propagation could not be considered statistically equal when the dimension of the specimens was modify. On average (considering all the studied species) the relationship among the ultrasonic wave velocity propagation (VLL) in normalized specimen and in proposed specimen was 0.99, being respectively the maximum and the lower relationships of 1.02 and 0.93. The velocity of wave propagation presents larger variations for values of length of wave percolation/wave length (L/?) up to 3, being more constant above that limit. It was also possible to verify, for the studied species, that the velocity of wave propagation increases with the increase of the transducer frequency. Key words: modulus of elasticity of wood; compression strength parallel to the fiber; ultrasonic wave velocity; dynamic constant / Mestrado / Construções Rurais e Ambiencia / Mestre em Engenharia Agrícola

This work deals with the study of diagnostic methods suitable for monitoring of the drying process of brick raw materials. Based on the extensive literature search, several parameters are selected, which are appropriate to monitoring during drying. In addition, a methodology for measuring these selected parameters is proposed. In the experimental part, the use of all described methods is gradually verified on the brick raw material with and without shortening additive (also known as grog). Was carried out: measurement of the surface temperature in the climatic chamber, determination of humidity distribution in the sample, determination of moisture diffusivity, determination of tensile strength, determination of ultrasonic wave velocity and determination of dynamic E-modulus of elasticity. Results of experiments and the gained experiences show, that at least two of the above-mentioned monitoring methods are very appropriate and beneficial – determination of moisture diffusivity and determination of tensile strength. In the work was described in detail the procedure of determination of moisture diffusivity of material. The dependence of moisture diffusivity on the moisture content of the dried material, has been described. Also, differences between raw material with grog and without grog has been described. As part of the practical verification of the experiment designed to determine the tensile strength at different humidity levels of test samples. A new shape of the test specimens and a new device were designed to allow them to be attached to a hydraulic press. The results of this work show that the tensile strength of the ceramic green bodies is primarily dependent on the moisture content of the material. The type of raw material almost does not affect the tensile strength.

Elektro-ultrazvuková spektroskopie je založena na interakci dvou signálů, elektrického střídavého signálu s frekvencí fE a ultrazvukového signálu s frekvencí fU. Ultrazvukový signál mění vzdálenost mezi vodivými zrny ve vzorku a tím mění jeho celkový elektrický odpor R. Změna odporu R je proměnná s frekvencí ultrazvukového signálu fU. Vzorek, který obsahuje mnoho defektů ve své struktuře, vykazuje vysokou změnu odporu R v porovnání se vzorkem bez defektů při stejné hodnotě ultrazvukového a elektrického signálu. V disertační práci je popsána elektro-ultrazvuková metoda na tlustovrstvých rezistorech, hořčíkových slitinách, monokrystalech Si a CdTe, varistorech a také jeden z prvních pokusů aplikace elektro-ultrazvukové spektroskopie na horninové vzorky a tak diagnostikovat jejich stav poškození. V našem případě byl proměřen vzorek žuly. Jelikož se jedná o nedestruktivní metodu testování, tak má tato metoda velmi perspektivní budoucnost. Tato metoda je citlivá na všechny defekty ve vzorku. Její výhodou je, že se měří velikost signálu ne frekvenci danou rozdílem nebo součtem budících frekvencí fE a fU a tím se dá dosáhnout vysoké citlivosti. V mém případě byl vždy měřen signál na rozdílové frekvenci fi = fE-fU.