No description available.

Recrystallised alumina is used as a high performance crucible material. Its thermal shock resistance is known to be affected by component shape, and also by processing variables, since the defects and internal stress at both the microscale (i.e. between grains due to anisotropic crystal properties) and macroscale (i.e. due to differential shrinkage during sintering) influence the fracture strength. The aim of this thesis is to study the nucleation and growth of defects in pure alumina and Cr-doped alumina, and to investigate how their behavior is affected by residual stresses, such those introduce by thermal expansion of the crystal grains. In this thesis, digital image correlation is applied to polycrystalline aluminas (i.e. Cr-doped alumina and pure alumina with average grain 3.6 µm and 1.5 µm respectively) that are stressed in an optical microscope. The defect size and the surface crack opening displacement were measured using digital image correlation. The distribution and population of crack nucleating defects were obtained by in-situ observation of the stressed surface and by analysis with digital image correlation. These data are then compared with independent measurements of the defect population using Hertzian indentation, from which defect populations are derived for the pure and Cr-doped alumina samples. Grain boundary plane and grain orientations in the vicinity of crack nuclei were characterised by electron microscopy. Crack nuclei were shown to develop at boundaries predicted to have high tensile thermal strains, caused by the orientation of the grain boundary plane relative to the adjacent grains, such as basal plane grain facets. The techniques of focused ion beam (FIB) milling and electron backscatter diffraction (EBSD) characterization of the crystallographic orientations and structure of cracked grain boundaries were used to provide data for a model to explain the cracking of these boundaries as a result of the thermal strains and the anisotropic thermal expansion behaviour of alumina.

No description available.

Two-phase Ti6246 alloy is a light weight material exhibiting very high strength at higher temperatures compared to the commonly used Ti64 alloy. This particular alloy is used at the later stages of compressor discs within the aero engines. However, compressor discs undergo a number of cyclic stresses, which could eventually lead to fatigue failure. In order to optimize the microstructure for design and lifing models, an improved understanding of the localised deformation mechanisms is crucial, particularly at the surface, as cracks can be initiated leading to failure and in turn affect the life expectancy of the component. Two-phase alloys in use have very complex lamellar microstructures comprising of a mixture of coarse and fine phases and their role in deformation can be very complex and difficult to understand. The focus of this study was particularly based on the importance of the beta phase in strengthening two-phase microstructures. Therefore, this study has been simplified to compare model lamellar microstructures, which have particular sizes of beta phase in between alpha lamellae. Digital Image Correlation along with high resolution imaging was used to develop a detailed understanding of the localised deformation in these microstructures. Widening the beta phase in-between alpha lamellae caused a more homogenous deformation, while ageing the beta phase with fine secondary alpha strengthened the microstructure. However, all microstructures showed that the single continuous alpha layer at beta grain boundaries depicted the highest amount of deformation, which can be detrimental for the life of the component. The behaviour of slip at the α/β interface not only depended on the size of the phases but also depended on the neighbouring crystallographic orientations and the relationship of the two phases, specifically the alignment of the close packed slip directions. Strain maps of these microstructures were subsequently related to corresponding Schmid factor maps and crystal plasticity models to improve this understanding.

Tendinopathy is a common pathology of tendons characterized by pain and a decrease in function resulting from changes in the tissue's structure and/or composition due to injury. Diagnosis of tendinopathy is determined by the qualitative analysis of a trained physician usually with assistance from an imaging modality. Although physicians can often identify tendinopathy, there are no quantitative metrics to evaluate tendon fatigue, damage, or healing. Physical therapy (PT) is a common treatment for patients with tendinopathy, and recent studies have investigated Focused Ultrasound (FUS) for its treatment of tendons. Developments in the use of FUS as a therapeutic have led to studies of the underlying mechanisms by which it operates. Digital Image Correlation (DIC) is a non-contact method of quantifying tissue displacements and strains of a deforming material using high resolution imaging DIC programs can evaluate and interpolate strain data by applying statistical image processing algorithms and solid continuum mechanics principles using a set of sequential image frames capturing the mechanical deformation of the specimen during testing. The studies presented in this thesis investigate methodologies for using DIC with ultrasound imaging of mouse Achilles tendons to characterize strains resulting from FUS therapies. The first method is based upon an orthogonal configuration of therapy and imaging transducers while the second investigates a coaxial experimental configuration. This work explores DIC as a viable means of quantifying the mechanical stimulation caused by FUS therapies on tendon tissue through ultrasound imaging to better understand the underlying mechanisms of FUS therapy. / Master of Science / Tendinopathy is a common injury that many people will experience in their lifetime. Pain and swelling are common symptoms and can make daily actions uncomfortable to perform. Physical therapy (PT) is one of the most common ways to help relieve the symptoms of this condition. A therapy being investigated to help treat tendinopathy utilizes Focused Ultrasound (FUS) technology to help the healing process. PT can be difficult and painful for those experiencing tendinopathy, but if a therapeutic like FUS could mimic the effects of PT, then some patients would not need to perform these physically demanding tasks. To understand if this treatment is viable, we need to better understand the underlying mechanisms by which it operates. Therefore, we are investigating the mechanical stimulation that FUS imparts on tendons because it is believed that the mechanical stimulations from exercise are a primary contributor to healing. Specifically, we want to evaluate the kind of strains applied by FUS therapies to inform decisions about dosage. One method uses Digital Image Correlation (DIC). DIC is a method of evaluating displacements and strains using non-contact high resolution imaging. DIC works using statistically motivated algorithms to calculate the deformation between subsequent video frames in a given material undergoing a state of stress. Using this technology along with ultrasound imaging, this work gives a preliminary exploration of using DIC as a means of quantifying strain to better understand the underlying mechanisms of the mechanical stimulations caused by FUS therapy.

Disc brake calipers are subjected to complex mechanical loading and interaction of individual components in a typical brake assembly makes design improvement very challenging. To analyse caliper behaviour, complex Finite Element models were created and successfully validated using a variety of experimental techniques, including exceptionally suitable Digital Image Correlation. A novel methodology to optimise caliper design was developed, using non-linear contact Finite Element Analysis and topology optimisation, to generate lightweight, high performance brake calipers. The method was used on a Formula 1 brake assembly and significant improvement in structural design was achieved, with the new caliper being lighter and stiffer than the original. The same approach was used on more conventional 4 pistons calipers using various boundary conditions with particular focus on mass reduction and considerably lighter designs were achieved. The influence of specific features of the optimised calipers on the structural performance was also successfully investigated.

Rail and bridge infrastructure assets are critical elements of Canada’s transportation network and their continued efficient and safe operation is necessary to ensure the nation’s economic livelihood. Monitoring technologies that can detect changes in performance as well as precursors to failure are an important element of ensuring this efficient and safe operation. Digital Image Correlation (DIC) is a monitoring technology that has the potential to provide critical data for infrastructure assessment and to replace various conventional sensors with one integrated monitoring solution. In this research, the accuracy of DIC is evaluated using numerical, laboratory and field-based experiments. The sources of error of particular relevance to dynamic measurement using DIC are identified as (i) bias error in the sub-pixel interpolation scheme, (ii) the ratio of sample rate to the frequency of the signal being monitoring and (iii) the signal to noise ratio. It is also shown that the chosen sub-pixel interpolation scheme can greatly affect the accuracy of dynamic measurements. The use of DIC was investigated for field monitoring of both horizontal and vertical railway displacements at sites with good and poor subgrade conditions under dynamic train loading. It is shown that there is a significant benefit to using an absolute displacement measurement system rather than a relative displacement measurement system as the former can capture irrecoverable rail displacements in both the vertical and horizontal directions. Finally, DIC was also used for field monitoring of a very stiff reinforced concrete bridge during static and dynamic load tests. It is shown that when using DIC for deflection monitoring, corrections may have to be made to compensate for errors such as camera jitter and drift to acquire the most accurate results. Two potential correction methods were the use of a fixed reference point and generating composite images using average pixel intensity values from multiple images. It was found that using a fixed reference point was the optimal choice in this bridge test. It is concluded that DIC can be used as an effective displacement measurement tool for bridge assessment because it shows excellent correlation with linear potentiometer results and it can allow measurements to be taken without having to close the bridge. / Thesis (Master, Civil Engineering) -- Queen's University, 2013-09-26 15:40:16.744

Finite element models are used frequently in both engineering and scientific research. While they can provide useful information as to the performance of materials, as length scales are decreased more sophisticated model descriptions are required. It is also important to develop methods by which existing models may be verified against experimental findings. The present study evaluates the ability of various finite element models to predict materials behaviour at length scales ranging from several microns to tens of nanometers. Considering this motivation, this thesis is provided in manuscript form with the bulk of material coming from two case studies. Following an overview of relevant literature in Chapter 2, Chapter 3 considers the nucleation of delta-zirconium hydrides in a Zircaloy-2 matrix. Zirconium hydrides are an important topic in the nuclear industry as they form a brittle phase which leads to delayed hydride cracking during reactor start-up and shut-down. Several FE models are used to compare present results with literature findings and illustrate the weaknesses of standard FE approaches. It is shown that standard continuum techniques do not sufficiently capture the interfacial effects of an inclusion-matrix system. By using nano-scale material descriptions, nucleation lattice strains are obtained which are in good agreement with previous experimental studies. The motivation for Chapter 4 stems from a recognized need to develop a method for modeling corrosion behaviour of materials. Corrosion is also an issue for reactor design and an ability to predict failure points is needed. Finite element models could be used for this purpose, provided model accuracy is verified first. In Chapter 4 a technique is developed which facilitates the extraction of sub-micron resolution strain data from correlation images obtained during in-situ tensile deformation. By comparing image correlation results with a crystal plasticity finite element code it is found that good agreement between the two exists. The method outlined is material independent and could be applied to most metallurgical studies. Chapter 5 reviews the findings of each case study and makes suggestions as to the direction of future research. / Thesis (Master, Mechanical and Materials Engineering) -- Queen's University, 2013-09-30 16:05:52.934

In the structural engineering community, a need exists for a non-contact two-dimensional measurement system which could provide information for field monitoring and greatly enhance the accuracy of numerical structural models. Recent advances have enabled the use of digital image correlation (DIC) to calculate the surface displacements of chosen targets in a series of digital images with a high degree of accuracy. Images are recorded during an experiment and are afterwards post-processed to find relevant information including, but not limited to, a) global displacement, b) relative displacement and c) changes in strain. In this research, a series of experiments were conducted to create measurement techniques for monitoring steel and reinforced concrete (RC) structures utilizing DIC. However, to ensure accurate DIC measurements, the addition of artificial texture from lightly applied spray paint on finished concrete was investigated and was determined to noticeably improve results. Furthermore, the placement of the digital camera relative to the structure being monitored was shown to control not only the desired field of view in the region of interest, but also the resulting image texture and DIC measurement accuracy. The DIC technique was applied to monitor and understand two important aspects of structural evaluation: a) the movement along shear planes and b) the evaluation of changes in strain due to curvature in beam elements. To monitor the change in crack width and slip, a method was created and validated on a series of artificial and reinforced concrete images for the cases of pure shear, pure flexure and combine flexure and shear. Curvature was found to impact the crack slip measurement, but its effect can be removed by using an innovative averaging technique. The curvature of a steel HSS and RC beams was found by using virtual DIC strain gauges and the horizontal strain profile. Results matched well with the curvature from electrical foil gauges and numerical models when the gauge length was maximized and selected so that the effects of cracking were accounted for. / Thesis (Master, Civil Engineering) -- Queen's University, 2012-09-28 09:36:04.274

Gamma titanium aluminide alloys are emerging as a lightweight replacement to nickel superalloys, with current application in turbine stages of aero-engines, as well as in high performance automobiles and potentially the nuclear industry. The lack of toughness of its two constitutive intermetallic phases, γ-TiAl and α2-Ti3Al, prevents a conventional damage tolerant approach to fatigue lifing. To gain confidence in the use of γ-TiAl alloys and extend the temperature-stress envelope of applicability, the present work aims to achieve an understanding of the development of plasticity and flaw formation during cyclic loading. The general plasticity of a γ-TiAl alloy, Ti-45Al-2Nb-2Mn(at.%)-0.8vol.%TiB2, in compression was investigated by mapping the development of localised strain at the specimen surface. Methods were developed to produce speckle patterns for high resolution digital image correlation that were stable at test temperatures of 700 °C in air, in order to study the extent of plasticity generated by differing deformation mechanisms at application-relevant temperatures, with nano-scale resolution. At the colony scale (i.e. single stacks of co-planar α2-Ti3Al and γ-TiAl lamellae, where each stack is formed from a single high temperature disordered α-TiAl grain), macroscopic deformation bands were observed to develop at only a few percent strain. Within such bands, which propagated across many colonies of differing lamellar orientations, considerable lattice curvature and localised slip and twin operation occurred. This correlated with colony boundary failure in such bands. Twinning of the γ-TiAl phase parallel to the lamellar interfaces, longitudinal twinning, has rarely been studied, despite generalised twinning in equiaxed γ-TiAl grains being known to cause boundary decohesion. Here, the occurrence of longitudinal twinning in both microcompression and polycrystalline testpieces was investigated up to 700 °C by electron backscatter diffraction. The strength of constraint by surrounding lamellar domains was found to be the determining factor in the increased prominence of twinning at 700 °C, and hence determined whether twinning shear-induced flaws formed at colony boundaries. Using the high temperature digital image correlation strain mapping and electron backscatter diffraction techniques developed, along with transmission electron microscopy, the onset of plasticity at temperatures up to 700 °C was studied in both micro-scale and macro-scale test specimens for different lamellar thicknesses. Testpieces were loaded below the macroscopic yield stress in both monotonic and high cycle fatigue regimes, to 107 cycles, at a tensile stress ratio of R = 0.1. Longitudinal plasticity occurred in most colonies with soft mode lamellar orientations, and was located just 30 - 50 nm from lamellar interfaces. Lamellar refinement caused an increased number of slip bands to develop. In most cases, plastic strains decreased to zero by the colony boundary and strain transfer across such boundaries in high cycle fatigue was rare. At room temperature, the maximum applied stress was found to influence the number of slip bands more than the number of loading cycles.