O presente trabalho tem por objetivo desenvolver um aparato experimental para estudar, em modelo físico de escala reduzida, o comportamento mecânico de um duto enterrado submetido a variações do estado de tensões da massa de solo circundante e a um potencial movimento de massa gravitacional, com avaliação concomitante das deformações desenvolvidas no solo por meio da técnica de correlação de imagens digitais. A alteração do estado de tensão no maciço foi feita por meio da aplicação de incrementos de inclinação ao modelo. Foram realizados ensaios com o duto nas posições transversal e longitudinal no interior da caixa de ensaios, enterrado em areia pura e seca, com razão entre altura de cobertura e diâmetro do duto de 3,55. A compacidade do maciço, controlada por meio da utilização da técnica de chuva de areia, foi avaliada nas situações densa (D = 111,5 %) e fofa (Dr = 58,2%). O comportamento mecânico do duto foi avaliado por meio de instrumentação para medição da deformação específica e deflexão da parede, sendo verificado efeito de flexão lateral no duto disposto na transversal, com maiores deformações observadas na situação de maciço fofo. Para o duto disposto na longitudinal, maiores deformações específicas foram observadas para a seção instrumentada central na situação de maciço denso, contudo verificou-se a necessidade de realização de ensaios adicionais para elucidação dos resultados, em termos da interação solo/tubo ao longo do comprimento do elemento. Para a utilização da técnica de correlação de imagens digitais, as imagens foram adquiridas em um ambiente com iluminação padronizada e resolução de partícula igual a 4. A qualidade da textura da imagem foi garantida por meio da preparação de material com adição de 20% de areia colorida. O refinamento da malha de análise, avaliado por meio da alteração do tamanho dos subsets e espaçamento entre subsets, não exerceu grande influência nos campos de deslocamentos obtidos, porém maiores refinamentos permitiram extrair observações mais detalhadas do campo de deformações. A utilização da técnica permitiu ainda avaliar a evolução dos vetores de deslocamento ao longo das etapas de inclinação e a influência do duto enterrado, na posição transversal, nos deslocamentos das partículas de solo circundante. / The present work aims the development of an experimental apparatus to study the behavior of a buried pipe under different soil stress states and potential landslides in a small-scale physical model. Digital image correlation technique is also used to evaluate soil deformation. A controlled slope increment squeme were responsible for soil stress state changes. The tests were performed with the model pipe buried in pure dry sand with a buried depth ratio of 3.55. A series of four tests involving two pipe configurations inside the test box (transversal and longitudinal) and two relative density (111.5% and 58.2%) was conducted. Soil density was controlled by pluviation method. The model pipe was instrumented in order to evaluate its behavior in terms of linear strain and deflection of the pipe wall. For the transversely disposed pipe, it was observed lateral bending effect and larger strains when buried in loose sand. For the longitudinally diposed pipe, the largest strains occurred in the pipe central cross section and in the tests conducted in dense sand. Nevertheless, additional testing is needed to better clarify the results, in terms of soil/pipe interaction along the pipe length. Daily digital images were acquired under standardized conditions of illumination for the use of digital image correlation technique. The particle/pixel size ratio was set equal to 4. Image texture quality was improved by adding 20% colored sand to the material used in the investigation. The level of refinement of the analysis mesh, evaluated by varying the subset size and the spacing of subsets, did not shown significant effect in the displacement fields. However, finer meshes allowed more detailed observations in the engineering shear strain fields obtained. Additionally, the digital image correlation technique allowed the evaluation of the displacement vectors evolution along the different slope stages considered. Moreover, this technique also captured the effect of the transversely disposed pipe on surrounding soil particles displacements.

This research project on the campus of Southern Illinois University Carbondale is an extension to the inquiry into the feasibility and reliability of the technology known as Digital Laser Speckle Image Correlation (DiLSIC). This is a hybrid approach of combining two existing technologies. The first being Digital Image Correlation (DIC) which is a nondestructive evaluation commonly used to find displacement, in-plane strain, as well as deformation. The second being the of laser speckle patterns. This hybrid has achieved level of resolution measured to be 3.4μ. DiLSIC increases the application ability of the DIC technique to situations that generally would not be an option to use. DiLSIC needs no artifact speckle patterns to be applied to the specimen as a preparation for nondestructive testing. In DIC testing, the surface of a specimen must artifact speckles applied to the subject surface. Often the application of artifact speckles is not desirable or possible. DiLSIC is an acceptable alternative to the previously discussed industry-wide practice. This method broadens the usage of the DIC technique to situations which previously were not possible. This technology can identify, quantify, and detect the distribution of strain and stress concentrations in composite structures. For this study, a honeycomb-backed glass fiber reinforced polymer (GFRP) panel from a Cessna aircraft exterior luggage door was obtained and a defect panel is created. The panel is constructed with one area containing a repair compliant with manufacturer standardized methods and a repair area is not compliant and consists of multiple incorrect repair steps. An area with no repair is also tested to act as a control for comparison and quantification. The results for the inspected areas showed a linear strain increase in the noncompliant repair. The data plot for the compliant repair showed a trend of following the same basic curve as the no repair area. A verification process follows the DiLSIC testing consisting of using Infrared Thermography, Air-coupled ultrasonic, and white light artifact speckle DIC. These tests show DiLSIC is a viable alternative to the testing that is available in the industry. DiLSIC can detect defect location, size, geometry and map strain to determine the difference between compliant and noncompliant repairs when compared to a base level non-repair area

Au cours des dernières deux décennies, la modélisation micromécanique a été largement développée afin de relier directement la microstructure réelle d’un matériau à ses propriétés macroscopiques (mécanique, thermique, électrique, etc.). Les lois de plasticité cristalline visent à prédire les comportements locaux et macroscopiques et/ou les changements de la microstructure lors d’un chargement thermomécanique. Cependant, étant donné l’échelle des mécanismes que ces modèles décrivent, les mesures sont difficiles à réaliser et l’identification des paramètres devient délicate. Il est également nécessaire d’utiliser des données expérimentales à l’échelle du grain. L’objectif de l’étude présentée ici est de développer une procédure robuste pour obtenir au moins deux réponses mécaniques locales distinctes d’un matériau à l’échelle du grain.Les champs total et élastique ont été sélectionnés et ensuite mesurés en même temps à chaque niveau de chargement successif lors d’essais de traction avec décharges. Le champ total a été déterminé par Corrélation d’Images Numériques (CIN) et le champ élastique a été calculé à partir de la mesure de Diffraction des Rayons X (DRX). Deux échantillons oligo-cristallins en alliage d’aluminium (5052) ont été utilisés dans cette étude. Le dispositif et méthode expérimental a été développé pour effectuer simultanément la CIN, la DRX et l’essai de traction in-situ dans un diffractomètre à rayons X. En plus des résultats et des analyses, les incertitudes ont également été quantifiées. / Micromechanical modelling was widely developed during the past 20 years as they enable ones to make direct links between the actual microstructure of a material and its macroscopic properties such as mechanical, thermal, electrical, etc. Crystal plasticity models aim at predicting local and macroscopic behaviours and/or changes of the microstructure during thermomechanical loading. However, the parameters of these models are difficult to identify, because the mechanisms they describe are at a small scale and are thus complicated to measure. For this reason, the crystalline model identification requires the use of experimental data at the grain scale. The objective of the study presented here is to develop a robust procedure to obtain at least two distinct local mechanical responses of a material at the grain scale.The total and elastic strain fields have been chosen to be characterised referring to the research interest and the adaptability of experimental methodologies. When samples were subjected to simple tensile loadings and unloadings, strain fields were measured on the sample surface simultaneously at each successive level. Total strain fields were determined by the Digital Image Correlation technique (DIC) while elastic strain fields were calculated from the X-ray diffraction (XRD) measurements. Two oligo-crystalline samples of an aluminium alloy (5052) has been prepared and used in this study. The experimental device and methodology was designed and developped to perform DIC, XRD and tensile tests in-situ in an X-ray diffractometer. The total and elastic strain fields of two samples through in situ tension experiments were obtained. Besides results and analysis, the corresponding uncertainties during each measurement were quantified as well.

Residual stresses are generally considered to be the driving forces for the failure of APS TBCs. In this thesis, the residual stress distribution as a function of depth in APS TBC has been measured by synchrotron XRD and explained by image based modelling based on the microstructure detailed studied by SEM and CT. The residual stress/ strain distribution as a function of depth was measured by synchrotron XRD in transmission and reflection geometry. The residual stress/ strain values were analysed using full pattern Rietveld refinement, the sin square psi method and XRD2 method. For the reflection geometry, a new method was developed to deconvolute the residual stress value in each depth from the measured averaged values. Two types of residual stress/strain distribution were observed. The first kind of residual stress was found to be compressive and followed a non-linear trend, which increased from the surface to the interface, decreased slightly and increased again to the interface. This trend showed a jump feature near the interface. The second kind of residual stress distribution possessed two jump features: one near the interface similar to the first kind and another jump feature near the sample surface. The residual stress in both beta and gama phase in the bond coat were also investigated which showed a tensile stress state. The stress trend predicted by our analytical model followed a linear relationship. Comparing this with the first kind of residual stress distribution, two main differences were shown. Firstly the jump feature near the interface and secondly the much larger overall stress gradient. The 3D and 2D microstructure of the sample with the first kind of residual stress distribution was observed by X-ray CT and SEM. The effect of pores, inter-splat cracks and the rumpling interface on the residual stress distribution was investigated by image based modelling. It was proved that the pores and the inter-splat cracks had no large influence on the stress distribution and the jump feature near the interface was a result of the rumpling interface. The much larger stress gradient observed in the measured residual stress distribution was an indication of the stress relaxation in the coating which was proved by a specially designed mechanical test. To explain the jump feature near the sample surface in the second kind of stress distribution. 3D microstructures of the measured samples were observed using X-ray CT. The effect of vertical and the side cracks on the stress distribution were investigated by image based modelling. It was found that the vertical crack had no large influence on the residual stress distribution and the jump feature in the stress trend near the surface could be attributed to the side crack. The effect of other kinds of cracks that were not directly observed in our samples, such as middle or through side cracks, were also investigated. These results were used to develop a semi-destructive method to determine the existence and distribution of cracks in APS TBC.

Les pièces de structure aéronautique utilisées dans l’aéronautique sont fabriquées en plusieurs étapes. Des étapes, comme le traitement thermique, génèrent des contraintes résiduelles. Les enlèvements de matière réalisés par les opérations d’usinage peuvent alors conduire à la réorganisation des contraintes résiduelles dans la matière et ainsi à la déformation de la pièce. La mesure in-situ de ces déformations devient nécessaire lorsque ce phénomène est étudié. Ces travaux de thèse abordent cette problématique dans le cadre du projet SIMP-Aero. L’objectif de ces travaux de thèse est d’adapter la méthode de corrélation d’images numériques à la mesure de la déformation de pièce pendant l’usinage, c’est-à-dire dans un centre d’usinage. Pour cela, plusieurs améliorations sont apportées à la méthode. Premièrement, les mouvements du système optique sont pris en compte afin que ceux-ci n’altère pas la qualité des mesures. Ensuite, les copeaux présents sur les images sont détectés et filtrés par un algorithme. Au final, la méthode développée permet de mesurer des champs de déplacement durant toute la séquence d’usinage, sans devoir l’interrompre, avec une incertitude de mesure de l’ordre du centième de millimètre. / Structural aluminum alloy parts used in aeronautics are manufactured in several steps, from forming processes and heat treatments to final machining. Some of the process steps induce residual stresses. The material removal during machining release these residual stresses and thus, leads to the part deformation. The in-situ measurement of these deformations becomes necessary when this phenomenon is studied. The present work address this problematic in the context of the ANR SIMP-Aero Project. It aims to define a reliable experimental technique dedicated to the measurement of part deformations during machining of large aeronautical parts. The backbone of the technique relies on Digital Image Correlation (DIC). Mainly as a consequence of the harsh constraints environment of machining, the customization of DIC is required. First, movements of the optical system are quantified and compensated for the proper measurement of the workpiece displacement. Then, the metal chips that fly between the observed surface and the acquisition system are detected and filtered by the algorithm. Finally, the developed method enables the measurement of displacement fields throughout the whole machining sequence, without interrupting it, and a measurement uncertainty of around one hundredth of a millimeter is ensured.

Digital Image Correlation (DIC) is a technique which uses images taken before and after deformation to determine displacement and strain data over the surface of the sample. In order to obtain this data for both in-plane as well as out-of-plane direction, multiple views of the sample are required. Typically, this is accomplished using multiple cameras, but it is possible to use diffraction gratings to bend the light coming from the specimen in order to allow a single camera to capture multiple views. This technique is referred to as Diffraction Assisted Image Correlation (DAIC) and has been previously demonstrated at room temperature. This work expands this method for use at high temperatures by incorporating the use of ultraviolet (UV) lights for illumination and filtering out the light in the visible spectrum. This increases the temperature at which useful images can be captured by reducing the glow that specimens produce at elevated temperatures. When not filtered out, this glow saturates the camera sensor making DIC impossible. This new technique is referred to as Ultraviolet Diffraction Assisted Image Correlation (UV-DAIC).

Les propriétés mécaniques des alliages de fer sont largement conditionnées par leur microstructure et la population de défauts locaux qu’elle contient. Comme il s'agit d'un moment de forte interaction entre ces deux éléments, l'étude des transformations α-γ et γ-α du fer mérite une attention particulière. Outre le passage d'une structure cristalline cubique centrée à une structure cubique faces centrées – donc de compacités différentes –,elles sont associées à une réduction des paramètres de maille. Le changement de volume correspondant est responsable de déformations mécaniques locales autour des sites de germination. La technique de corrélation d'images numériques(CIN) s'est montrée fiable pour ce qui est de calculer des champs cinématiques à l'échelle de quelques grains. Dans ce travail, elle est adaptée à la capture de localisations de la déformation pendant les transformations allotropiques. Un banc expérimental est conçu pour obtenir des images haute résolution avec un contrôle fin des sollicitations thermiques. Des essais de validation sont d'abord effectués sur du fer industriel. Puis des échantillons de fer haute pureté sont ensuite soumis à des cycles de transformation α-γ-α et les champs de déformation correspondant sont calculés par CIN. Associés à l'acquisition des orientations initiales et finales, ils sont utilisés pour valider les mécanismes de transformation proposés dans la littérature. En parallèle, un modèle, écrit en petites déformations, est construit en incorporant des composants liés à la transformation dans une fonctionnelle dont les conditions de stationnarité sont équivalentes au problème thermomécanique à résoudre. Les incréments des variables internes, incluant glissements plastiques et fractions volumique transformées, sont obtenus en minimisant cette fonctionnelle. / Mechanical properties of iron-based alloys are largely conditioned by their microstructure and the population of local defects inside this microstructure. As it is a moment of massive interplay between these two elements, the study of the α-γ and γ-α transformations in iron is of particular interest. Besides a change from a body-centered cubic to a face-centered cubic crystal structure – and thus a change in compacity –, they lead to a lattice parameter reduction. The corresponding change in volume is responsible for local mechanical deformations around transformation sites. Digital Image Correlation (DIC) technique has been proven reliable to compute kinematic fields at the scale of a few grains. In the present work, an adaptation of this technique to the observation of strain localizations induced by the formation of a new phase is proposed. A home-made device is designed to obtain high resolution images and to control heating and cooling. Tests are first conducted on industrial iron to assess the viability of the procedure. High-purity iron samples are then submitted to α-γ-α transformation cycles and the associated strain fields are computed. In combination with the acquisition of initial and final orientations they are used to validate transformation mechanisms proposed in the literature. In parallel, a model, written under the small strain format, is built by incorporating transformation related components into a power functional whose stationarity conditions are equivalent to the thermomechanical problem. In accordance with variational principles, the evolution of internal variables,including plastic slip increments and fraction of the material locally transformed, are computed through the minimization of the functional.

Chaque année, d'innombrables collisions se produisent entre des avions en vol et des oiseaux. L'impact aviaire, menace redoutée par les pilotes, concerne tant l'aviation civile que son pendant militaire. Les statistiques démontrent que, même si fort heureusement le nombre d'accidents graves reste limité, les incidents sont de plus en plus nombreux. Parmi les acteurs qui luttent contre ce danger, les constructeurs d'avions jouent un rôle prépondérant. Contraints par des réglementations internationales, ils s'attachent à produire des éléments de structure qui résistent à l'impact d'oiseaux. Dans la mise au point de leur produits, les avionneurs démontrent cette résistance à l'aide d'essais d'impact : on accélère un simulant d'oiseau jusqu'à la vitesse voulue -- de l'ordre de la vitesse de croisière nominale de l'avion -- et on le projette sur un aileron ou un morceau de fuselage. La présente thèse doctorale, co-dirigée par les professeurs Philippe Bouillard de l'ULB et Marc Pirlot de l'ERM, contribue doublement à l'amélioration de ces techniques d'essais dynamiques. D'une part, elle réalise la mise au point et la validation d'un lanceur pyrotechnique à double étage pour l'accélération du simulant d'oiseau. Un canon de calibre 20 mm est combiné avec un accélérateur de calibre 160 mm. La combustion d'un mélange de poudre propulsive contenu dans une douille adaptée génère les gaz à haute température et à haute pression nécessaires à l'accélération d'un simulant d'oiseau dûment confiné dans un conteneur de protection. Un dispositif de séparation arrête le conteneur afin que seul le simulant d'oiseau percute l'élément d'avion à l'essai. La solution pyrotechnique à double étage mise au point est validée par de nombreux tirs instrumentés en vitesse, en accélération et en pression ; elle se révèle conforme aux exigences de sécurité et de reproductibilité. Le lanceur pyrotechnique présente par rapport aux solutions pneumatiques, utilisées à notre connaissance dans tous les autres centres d'essais, des avantages indéniables de compacité ainsi que de rapidité et de souplesse de mise en oeuvre. D'autre part, la migration des alliages métalliques vers les matériaux composites est amorcée depuis plusieurs années déjà dans le monde de la construction aéronautique. Pour optimiser les structures, une connaissance des caractéristiques de ces matériaux est indispensable. Les modes de rupture font partie des caractéristiques encore mal connues. La mesure du déplacement hors-plan lors du tir sur panneaux plans est une des manières de quantifier le comportement du matériau sous l'action d'un impact. Cette mesure s'opère généralement de manière statique, après le tir. Une méthode de mesure dynamique a été mise au point, basée sur l'emploi de techniques de stéréoscopie par corrélation numérique d'images. Cette technique a été validée au moyen d'une méthode métrologique indépendante d'extensométrie laser. ABSTRACT Countless collisions occur each year between airplanes and birds. Bird strike is a concern to both civilian and militay aircraft. Statistics show that, although the number of serious accidents fortunately remains low, the number of incidents keeps increasing. Amongst the actors tackling this issue, aircraft manufacturers play an important role. In compliance with international regulations, they have to produce structural elements that withstand bird impact. During the development of their products, aircraft manufacturers have to demonstrate this resistance through bird impact trials : a bird surrogate is accelerated to the required velocity - often close to the nominal cruise speed of the aircraft - and launched onto a flap or a piece of fuselage. This PhD thesis has been co-supervised by Professor Philippe Bouillard (ULB) and Professor Marc Pirlot (ERM-KMS). Its contribution to the improvement of the aforementioned dynamic trials is twofold. One one hand, a two-stage pyrotechnical launcher for bird surrogates has been developed and assessed. A 20 mm caliber gun is connected to a 160 mm diameter launcher. The combustion of a propellant mixture in a cartridge case generates high pressure, high temperature gases which accelerate a bird surrogate protected by a cylindrical container. A stripper refrains the container from hitting the target pane. The pyrotechnical solution has been assessed through an important number of firings where pressure, velocity and acceleration have been measured. The solution has proven compliance with both the safety requirements and the repeatability specifications. Its advantages compared to the pneumatic solutions used, as far as we know, in all other test centres, include compactedness as well as flexibility and high firing rate. On the other hand, migration towards composite materials has been initiated years ago in the area of aeronautical constructions. To optimize structures, a thorough knowledge of these new materials is required. Failure modes belong to the still badly known features of carbon reinforced plastics. Measuring the out-of-plane deformation when firing on a flat pane is one way of quantifying the material's behaviour under impact. This measurement is most frequently made in a static way, after completion of the firing. A dynamic measuring method has been developed, based upon stereoscopic digital image correlation techniques. This technique has been validated by means of an independent laser extensometer measuring method.

Commercially available polycrystalline Ni (Ni200; grain size: 32 μm) and electrodeposited nanocrystalline Ni (grain size: 57 nm), Ni-2.6%Fe (grain size: 25 nm) and Ni-8.5%Fe (grain size: 20 nm) were analyzed for the phenomena of stress-induced heat generation and strain localization during plastic deformation at room temperature (i.e. 250C). Tensile specimens according to ASTM E8 standard dimensions were tested at strain rates of 10-2/s and 10-1/s, respectively, to record the amount of heat dissipated and the change of localized strain using a high resolution infrared (IR) detector and digital image correlation (DIC) camera, respectively. Results have shown that the maximum temperatures that were recorded in nanocrystalline Ni and Ni-Fe alloys were at least 300C lower than the onset temperatures for subgrain coalescence previously measured through differential scanning calorimetry. It can be concluded that thermally activated grain growth during tensile testing of nanocrystalline Ni and Ni-Fe alloys is not likely to occur.

Commercially available polycrystalline Ni (Ni200; grain size: 32 μm) and electrodeposited nanocrystalline Ni (grain size: 57 nm), Ni-2.6%Fe (grain size: 25 nm) and Ni-8.5%Fe (grain size: 20 nm) were analyzed for the phenomena of stress-induced heat generation and strain localization during plastic deformation at room temperature (i.e. 250C). Tensile specimens according to ASTM E8 standard dimensions were tested at strain rates of 10-2/s and 10-1/s, respectively, to record the amount of heat dissipated and the change of localized strain using a high resolution infrared (IR) detector and digital image correlation (DIC) camera, respectively. Results have shown that the maximum temperatures that were recorded in nanocrystalline Ni and Ni-Fe alloys were at least 300C lower than the onset temperatures for subgrain coalescence previously measured through differential scanning calorimetry. It can be concluded that thermally activated grain growth during tensile testing of nanocrystalline Ni and Ni-Fe alloys is not likely to occur.