Steam exploded fibers from Yellow Poplar (Liriodendron tulipifera) wood were assessed in terms of (a) their impact on torque during melt processing of a thermoplastic cellulose ester (plasticized CAB); (b) their fiber incorporation and dispersion characteristics in a CAB-based composite by SEM and image analysis, respectively; and (c) their impact on the mechanical properties (under tension) of CAB-based composites having fiber contents of between 10 and 40% by weight. The fibers included water-washed steam exploded fibers (WEF), alkali-extracted fibers (AEF), acetylated fibers (AAEF), all from Yellow poplar (log Ro = 4.23), and oat fillers (COF) as control. The stepwise increase in cellulose content by extraction, and especially the (surface) modification by acetylation, contributed to increased torque during melt processing, and to improved interfacial adhesion as well as fiber dispersion. As compared to pure CAB, AAEF generated the highest increase in torque (+ 421%) followed by AEF (+ 260%) and WEF (+ 190%) at 40% fiber content by weight. AAEF was also found to enhance the tensile properties of the resulting composites. SEM studies of the tensile fracture surfaces indicated significant interfacial delamination and also pull - out of fibers when WEF, AEF, and COF were used to reinforce the CAB matrix. Composites with AAEF, by contrast, revealed fracture surfaces with reduced interfacial delamination and with significant fiber fracturing during failure. Image analysis was used to determine fiber dispersion within the resulting composites quantitatively. Significant improvement in fiber dispersion was achieved when the matrix was reinforced with acetylated fibers (AAEF). Fiber addition to the matrix resulted in loss of strain at break (- 80 to - 93%) and slight or significant increases in modulus (+ 47 to + 103%) depending on fiber type at 40% fiber content. Maximum stress declined for all fibers except AAEF at all fiber contents. AAEF-based composites revealed a decline in maximum stress when fiber content rose to 10%, and this reversed when fiber content increased beyond 10%. This increase in strength is consistent with the rule of mixtures that stipulates reinforcement of the matrix by fibers that are capable of transferring stresses across the fiber-matrix interface. All fibers suffered length decreases during melt processing. / Master of Science

Understanding and predicting the consequences of dangerous phenomena linked to the industrial activity is critical to ensure the highest safety level possible. Explosions represent a high risk of fatalities and economic loss and even though the phenomenon is studied in the literature, accidents still occur.The explosion in air of a heterogeneous charge (i.e. an explosive charge surrounded or mixed with a gaseous, solid, or liquid pollutant) has various consequences. While the presence of buildings around the explosion will reduce considerably the impact of most of them, it will affect in more complex ways the propagation of the pressure released, also called bast wave, and the pollutant dispersion. Simplified models to characterize the blast propagation and the dispersion following an explosion are necessary tools for industries to access a first estimation of the risks related to their activities. However, the existing models do not take into account the effect of the urban environment.The global objective of the project is to improve the understanding of the blast propagation and the dispersion inside an urban environment by generating a quantitative database. In parallel to the project, simplified models are being developed by the Commissariat à l’Energie Atomique et aux Energies Alternatives (CEA) Gramat (center from the Direction des Applications Militaires (DAM)) and will be validated by the generated experimental database. To achieve this goal, experimental techniques are developed and applied to a controlled reduced-scale urban environment, and a CFD approach is used to facilitate the understanding of the blast experimental results. The challenges associated with the creation of a new experimental system led to innovative solutions in response to technical issues. The main originality of the project is the investigation of explosively driven dispersion under a controlled atmospheric boundary layer, which represents a novelty in the area from the author's knowledge. Existing experimental techniques have been extended and validated for the large dynamic ranges involved in the explosive dispersion. The research is separated into two parts: the investigation of the blast, and the investigation of the dispersion driven by an explosion, both inside an urban environment in a 1:200 reduced scale.In the first part, the blast propagation has been first investigated in free field to characterize the energy, the geometry, and the repeatability of each studied explosives. Then the blast has been studied inside four selected typical urban configurations. To help the understanding of the blast path, a numerical model has been developed in OpenFoam to simulate the propagation and a good overlap between the experimental and numerical results has been observed. The second part of the research focuses on the investigation of the explosively driven dispersion. Micro-sized talc particles have been added around the explosives to simulate the pollutant dispersion. Large-Scale Particle Image Velocimetry (LS-PIV) and Mie-Scattering techniques have been first investigated and validated on a supersonic jet. They have been thereafter applied to the explosively driven dispersion. Three atmospheric conditions, two masses of talc, and two diameters of powder have been investigated, both in free field and inside a T-junction.The experimental techniques used to characterize the explosion of a heterogeneous charge show promising results. They are powerful tools to investigate complex large-scale and large dynamic range flows. / Doctorat en Sciences de l'ingénieur et technologie / info:eu-repo/semantics/nonPublished

This thesis examines the influences of five factors on the strain energy at failure of metallic alloy plates during a shock wave impact. The five factors are material type, initial damage, boundary conditions, plate thickness, and plate temperature. The finite element simulation matrix was developed using a statistical design of experiments (DOE) technique. The Eulerian hydrocode CTH was used to develop the pressure histories that were input into the finite element code Abaqus/Explicit, which implemented the Mississippi State University internal state variable (ISV) plasticity-damage model (DMG). The DMG model is based on the Bammann-Chiesa-Johnson (BCJ) ISV plasticity formulation with the addition of porosity and the void nucleation, growth, and coalescence rate equations that admit heterogeneous microstructures. Material type and thickness were the primary influences on the strain energy at failure, and the materials studied, magnesium and aluminum, showed two different failure mechanisms, tearing at the boundaries and spalling, respectively.

One of the principal challenges of primary blast injury research is imitation of shock waves accurately and consistently in a safe and tunable platform. Existing simulators have been effective in these goals but have not been conducive for in vitro models due to their large size and air-mediated wave propagation. In this thesis, a redesigned benchtop shock wave generator (SWG) has provided a platform for in vitro models. A pulsed power generator charges a capacitor and discharges the capacitor through a bridge wire. The discharge causes the bridge wire to experience phase changes, momentarily becoming a gas or plasma. In this moment, the bridge wire expands radially and creates a pressure wave in the surrounding water. As the wave propagates, it forms a shock wave and strikes the cell platform at the far end of the conical tank. Current design efforts are focused on the tunability of the SWG, by varying the bridge wire material and diameter. Five materials at three bridge wire diameters have been tested. Each bridge wire was inserted into the SWG via a pinching mechanism. Either side of the pinching mechanism was connected to either terminal of the capacitor. When the pulsed power generator was cycled, the bridge wire was vaporized and generated a shock wave. A piezoelectric sensor near the wide end of the tank recorded the passing of the shock wave, which was used to derive various pressure metrics that correlate to injury. The sample size for each combination of diameter and material was five, with a grand total of seventy-five samples run. Two-way ANOVAs measuring the impacts of bridge wire material and diameter on a variety of shock wave metrics found that the diameter played a significant role in determining the peak overpressure and positive impulse generated while the main effect of material played a much smaller role. The interaction between material and diameter was also found to be significant. The tunable benchtop SWG provides a platform for exploration of primary blast injury using in vitro models. By adjusting the bridge wire diameter, the SWG can generate waves with a variety of shock wave metrics, providing an opportunity for researchers to address various degrees of injury. With the addition of this technology to the efforts to understand primary blast injury, development of treatments and protective equipment can be expedited. / Master of Science / Primary blast injury, the injury caused by the blast wave moving through the body, has been affecting those exposed to blast for nearly a century, since the regular use of conventional explosives in World War I. As equipment and war has changed in the past two decades, there has been heightened interest in understanding the effects of blast waves on the body. To assist in this research, blast wave simulators have been developed to recreate the blast wave in a controlled environment. However, current designs are not conducive to experiments on cultured cells. A new blast wave simulator, called the shock wave generator (SWG), has been designed as a platform for cultured cell-based experiments. The simulator generates a shock wave by exploding a thin bridge wire using high electrical current. The explosion occurs underwater, generating a shock wave capable of injuring cells at the opposite end of the tank. A platform such as this provides multiple opportunities to tune the pressure metrics related to the shock waves. Bridge wire material and volume play critical roles in the resulting shock wave, working together to define the amount of energy required to vaporize the bridge wire. Five materials and three diameters, a derivative of the wire volume, were investigated to determine their impacts on the resulting peak pressure, positive duration, and positive impulse. While wire material was not found to have a significant impact on peak pressure, wire diameter had a significant effect on the resulting overpressures. The thickest wire generated the lowest peak pressure while the thinner wires generated higher peak pressures. The thinner wires were not significantly different from one another. A similar result was found for positive duration and impulse. Overall, the use of an exploding wire to generate shock waves is applicable as an injury mechanism for cell cultures in primary blast injury research. This work along with future work will provide a tunable and controlled platform that has opened a new frontier for investigating the primary blast injury.

No description available.

This work deals with evaluating the effectiveness of a new verification algorithm called slice--n--dice. In order to evaluate the effectiveness of slice--n--dice, a vector clock POR was implemented to compare it against. The first paper contained in this work was published in ACM SIGSOFT Software Engineering Notes and discusses the implementation of the vector clock POR. The results of this paper show the vector clock POR performing better than the POR in Java Pathfinder by at least a factor of two. The second paper discusses the implementation of slice--n--dice and compares it against other verification techniques. The results show that slice--n--dice performs better than the other verification methods in terms of states explored and runtime when there is no error in the program or little thread interaction is needed in order for the error to manifest.

In this study a modern hydrocode, blastFoam, that was designed for multi-phase compressible flow problems with applications suited for high-explosive detonation was investigated for underwater explosion (UNDEX) events. The problem of over-prediction for long-term UNDEX bubble behavior in modern hydrocodes that is known to be due to neglected secondary energy-loss mechanisms is evaluated. A single secondary energy-loss mechanism is established as the most significant loss mechanism that is being disregarded in current hydrocodes. The leading secondary energy-loss mechanism is formulated into a computational model that modifies the Jones-Wilkins-Lee (JWL) equation of state (EOS). Explanation and guidance for implementing the model in an Finite Volume Method (FVM) Eulerian-based hydrocode is provided. Through this research this thesis aims to improve long-term UNDEX bubble behavior prediction. Which is apart of a larger effort to improve numerical and computational predictions of UNDEX-induced structural ship response. / M.S. / Predicting the bubble dynamics of an underwater explosion (UNDEX) event is of great importance for the survivability of America’s warships. Shock waves from high-energy explosives are destructive to anything and everything nearby. Therefore, the design and development of military machinery rely on the accurate predictions of computational simulations. Computational solvers must be able to simulate the initial propagating shock waves from an underwater explosion, as well as the smaller following shock waves from the oscillating UNDEX bubble. Current incompressible solvers neglect the important compressible effects needed to predict the behavior for the UNDEX bubble oscillation cycle. If America’s Navy cannot predict the long-term damaging effects that a warship may encounter from an UNDEX bubble, then America’s warships and crew could not survive at battle. This study considers the assumptions used to simplify current UNDEX computational solvers in order to investigate and organize a compressible long-term simulation model. This model improves the multi-pulse bubble dynamic predictions for an UNDEX event, and will in return help design a long-term battle-ready warship for America’s future warfare.

This thesis investigates the use of the numerical modeling tools LS-DYNA and USA in modeling general far-field underwater explosions (UNDEX) by modeling a three-dimensional box barge that is subjected to a far-field underwater explosion. Past UNDEX models using these tools have not been validated by experiment and most are limited to very specific problems because of the simplifying assumptions they make. USA is a boundary element code that requires only the structural model of the box barge. LS-DYNA is a dynamic finite element code and requires both the structural model and the surrounding fluid model, which is modeled with acoustic pressure elements. Analysis of the box barge problem results finds that the program USA is a valid tool for modeling the initial shock response of surface ships when cavitation effects are not considered. LS-DYNA models are found to be very dependent on the accuracy of the fluid mesh. The accuracy of the fluid mesh is determined by the ability of the mesh to adequately capture the peak pressure and discontinuity of the shock wave. The peak pressure captured by the model also determines the accuracy of the cavitation region captured in the fluid model. Assumptions made in the formulation of the fluid model causes potential inaccurate fluid-structure interaction and boundary condition problems cause further inaccuracies in the box barge model. These findings provide a base of knowledge for the current capabilities of UNDEX modeling in USA and LS-DYNA from which they can be improved in future work. / Master of Science

The far-field underwater explosion (UNDEX) problem is a complicated problem dominated by two phenomena: the shock wave traveling through the fluid and the cavitation in the fluid. Both of these phenomena have a significant effect on the loading of ship structures subjected to UNDEX. An approach to numerically modeling these effects in the fluid and coupling to a structural model is using cavitating acoustic finite elements (CAFE) and more recently cavitating acoustic spectral elements (CASE). The use of spectral elements in CASE has shown to offer the greater accuracy and reduced computational expense when compared to traditional finite elements. However, spectral elements also increase spurious oscillations in both the fluid and structural response. This dissertation investigates the application of CAFE, CASE, and a possible improvement to CAFE in the form of a finite element flux-corrected transport algorithm, to the far-field UNDEX problem by solving a set of simplified UNDEX problems. Specifically we examine the effect of increased oscillations on structural response and the effect of errors in cavitation capture on the structural response which have not been thoroughly explored in previous work. The main contributions of this work are a demonstration of the problem dependency of increased oscillations in the structural response when applying the CASE methodology, the demonstration of how the sensitivity of errors in the structural response changes with changes in the structural model, a detailed explanation of how error in cavitation capture influences the structural response, and a demonstration of the need to accurately capture the shape and magnitude of cavitation regions in the fluid in order to obtain accurate structural response results. / Ph. D.

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