Ultra-wideband (UWB) communication is emerging as a new wireless technology, which promises high data rates with low interference and low power consumption. The development of such UWB systems requires a sufficiently large amount of data to characterize the propagation behavior of UWB signals in indoor environments and develop accurate channel models. This thesis focuses primarily on a frequency-domain approach for propagation measurements and characterization of indoor UWB channels. This approach is based on measurements of the amplitude using a scalar network analyzer and retrieval of the phase from the amplitude data using a Hilbert transform relationship. Extensive propagation data are collected in a frequency range of 1 to 12 GHz in two buildings on Virginia Tech campus. Using the data, channel characterization results are obtained and compared to those based on time-domain measurements. Some statistical results for small-scale fading, path loss exponent, and signal quality are presented. This comparison validates the accuracy of measured results for the UWB measurement campaign. The measured data also reaffirms the immunity of UWB propagation to small-scale fading which is present in narrowband wireless communication systems. In addition to channel propagation measurements, signal distortions in UWB links, due to bandwidth limitations of antenna characteristics as well as the dispersive behavior of building materials, are also examined. In particular, the distortion of radiated signals by TEM horn antennas along off-boresight directions are studied experimentally. Furthermore, pulse distortions resulting from propagation through dispersive walls are demonstrated by simulation. The roles of receive-transmit antennas in a UWB link are examined, and the requirements for gain, input impedance, polarization, and phase of the radiated signal necessary for minimization of signal distortions are pointed out. / Master of Science