The laser-induced holographic gratings in the Azo dye-doped PMMA thin films with liquid crystal were investigated by changing the temperature of the sample, the angle of two writing beams and the rubbing. The high power Q-switch pulse laser has been used as the writing beams and the He-Ne cw laser has been used as a real-time probe beam to detect the first order diffraction singals. The grating are the results of photo-isomerization of azo dye and diffusions of liquid crystal. The model has been established to analyze the first order diffraction signals in order to understand the mechanism of grating and the effect of temperature and angle.

A novel detection technique to estimate the amount of chirp in fiber Bragg gratings (FBGs) is proposed. This method is based on the fact that reflectivity at central wavelength of FBG reflection changes with strain/temperature gradient (linear chirp) applied to the same. Transfer matrix approach was used to vary different grating parameters (length, strength and apodization) to optimize variation of reflectivity with linear chirp. Analysis is done for different sets of ‘FBG length-refractive index strength’ combinations for which reflectivity vary linearly with linear chirp over a decent measurement range. This work acts as a guideline to choose appropriate grating parameters in designing sensing apparatus based on change in reflectivity at central wavelength of FBG reflection. A novel high sensitive FBG strain sensing technique using lasers locked to relative frequency reference is proposed and analyzed theoretically. Static strain on FBG independent of temperature can be measured by locking frequency of diode laser to the mid reflection frequency of matched reference FBG, which responds to temperature similar to that of the sensor FBG, but is immune to strain applied to the same. Difference between light intensities reflected from the sensor and reference FBGs (proportional to the difference between respective pass band gains at the diode laser frequency) is not only proportional to the relative strain between the sensor and reference FBGs but also independent of servo residual frequency errors. Usage of relative frequency reference avoids all complexities involved in the usage of absolute frequency reference, hence, making the system simple and economical. Theoretical limit for dynamic and static strain sensitivities considering all major noise contributions are respectively of the order of 25 pε/ Hz and 1.2nε /

The diploma thesis described the basic principles and characters of the long period fiber gratings (LPFGs). Our concern was to describe basic mathematical description of these gratings needed to their modelation and simulation. Consequently some exact models leading to changes in the shape of the spectrum LPFGs were suggested, these methods were the chirping, apodization and changes in the average refractive index navg. In the Matlab environment, programes for counting the important parametres LPFGs were created and meanwhile each model leading to the change in the shape of the spectrum was simulated.

In this thesis work, a systematic quantitative study has been undertaken, on the performance of etched fiber Bragg Grating (FBG) sensors in the investigation of surface molecular adsorption in real-time; it is shown that the limit of detection (LOD) of FBGs etched below 2 microns diameter, is better compared to prominent optical label-free molecular sensing techniques such as Surface Plasmon Resonance (SPR). Novel fiber optic sensors based on FBG and etched FBG with various nano materials (polyelectrolytes, carbon nanotubes, hydrogel, metals and chalcogenides) coated on the surface of the core or cladding, have been proposed for sensing multi parameters such as pH, protein, humidity, gas, strain, temperature, and light etc. Besides being reproducible and repeatable, the proposed methods are fast, compact, and highly sensitive. A novel optical instrument has also been developed to measure angular deviation, binocular deviation and refractive index of glass slabs, and liquids, based on a shadow casting technique. This method uses the deviation in the geometrical shadow cast by a periodic dot pattern trans-illuminated by a distorted light beam from the transparent test specimen relative to a reference pattern.

Several sensor technologies have been developed and experimented over the last few decades to cater various needs of medical diagnostics. Among these, fiber optic sensors, in particular, Fiber Bragg Grating (FBG) based sensors have attracted considerable attention due to their inherent advantages such electrical passiveness, immunity to Electro Magnetic Interference (EMI), chemical inertness, etc. The present research work focuses on design, development and validation of FBG sensor based devices for measurement of certain healthcare parameters in the context of foot function/gait cycle, cardiac and breathing activity, nostril dominance, hand grip/wrist angle force function, etc. The experimental work presented here emphasizes on the effectiveness and competitiveness of the FBG devices developed, in comparison with standard tools such as Accelerometer, Load cell, Electronic Stethoscope, Electromyogram and Dynamometer. In the field of human balance, stability and geriatrics, two independent FBG devices namely, Fiber Bragg Grating based Stability Assessment Device (FBGSAD) and Optical Sensor Ground Reaction Force measurement Platform (OSGRFP) have been designed, developed and experimented for postural stability assessment and gait analysis respectively. The result of these studies have significant implications in understanding of the mechanism of plantar strain distribution, identifying issues in gait cycles, detecting foot function discrepancies, identifying individuals who are susceptible to falls and to qualify subjects for balance and stability. In the field of ergonomic assessment, Fiber Braggs Grating based Hand Grip Device (FBGHGD) is designed and developed for the measurement of hand grip force which helps in the understanding of several important biomechanical aspects such as neuromuscular system function, overall upper-limb strength, vertebral fracture, skeletal muscle function, prediction of disability, incapacity, mortality and bone mass density (forearm, skeletal sites, spine, hip etc.). Further as an extension of this work, the FBGHGD is used for measurement of force generated by the wrist in different positions of the flexion and extension which relates to the wrist muscle activity and its enactment. In the field of cardiac activity monitoring, a novel, in-vivo, non-invasive and portable device named Fiber Bragg Grating based Heart Beat Device (FBGHBD) is developed for the simultaneous measurement of respiratory and cardiac activities. The work involves designing FBGHBD, validating its performance against traditional diagnostic systems like electronic stethoscope, exploration of its clinical relevance and the usage of FBGHBD in studies involving normal persons and patients with myocardial infarction. The unique design of FBGHBD provides critical information such as nascent morphology of cardiac and breathing activity, heart rate variability, heart beat rhythm, etc., which can assist in early clinical diagnosis of many conditions associated to heart and lung malfunctioning. Further, the scope of this work extends towards evaluating several signal processing algorithms and demonstrating a suitable signal processing architecture for real-time extraction of heart beat and respiratory rates along with its nascent morphologies for critical health care application. In the area of breath monitoring, a Nostril Pressure and Temperature Device (NPTD) is designed and developed which aims at simultaneous, accurate and real-time measurement of nostril air flow pressure and temperature to aid in clinical diagnosis of nasal dysfunction and associated nose disorders. The results of NPTD can offer certain vital features like breathing pattern, respiratory rate, changes in individual nostril temperature/pressure, nostrils dominance, body core temperature etc., which can assist in early clinical diagnosis of breathing problems associated with heart, brain and lung malfunctioning. Since the research work in this thesis involve experiments engaging human subjects, necessary approvals from the ethical committee is obtained before the experiments and required ethical procedures are followed during all the experimental trials.

Sensors have become essential elements in human life for safe and comfortable existence in the ever demanding world. Various technologies over decades have contributed in their own way fulfilling innumerable sensing requirements. The discovery of optical sensor technologies has revolutionized the sensing field due to their inherent advantages. Among the large number of fiber optic sensor technologies, FBG based sensors have become widely known and popular within and outside the photonics community and has seen a prominent rise in their utilization. This thesis explores the use of FBG sensors for a wide range of applications scanning across a variety of engineering and medical applications, in the areas of civil engineering, biomechanical engineering, aerospace engineering, geoengineering, etc. It also deals with newer methods of packaging FBG sensors for the measurement of specific engineering parameters like strain, temperature, pressure, displacement and vibration. In the field of civil engineering, FBG sensors are employed for strain sensing on a prism and furthermore tested on a full size brick wallet. During this study, emphasis is made on substituting traditional sensors by specially packaged FBG sensors with the intent of either enhancing the sensing system’s performance or in merging/uniting the inherent advantages of FBG sensors. In the area of biomechanics, a novel sensor methodology using FBG sensors, for measuring surface strains generated on the skin of the calf muscle during various leg exercises is proposed. This methodology is used to address one of the most critical and life threatening issues in long distance air travel, namely the Deep Vein Thrombosis. Further, a FBG sensor based plantar sensing plate, is designed and developed, to measure plantar strain distribution in foot and also to analyze the postural stability. In the field of aerospace engineering, FBG sensors are used for addressing two of the most vital issues; Structural Health Monitoring (SHM) and direct measurement of pressure and temperature on the surface of an aircraft under hypersonic wind flow. Carbon Fiber Composite coupon level testing is carried out to obtain a generic strain calibration factor for the FBG sensor. Further, FBG sensors are exploited for the direct measurement of absolute temperature and pressure on the leeward surface of blunt cone at hypersonic wind speeds. In the domain of geoengineering, the feasibility studies have been undertaken to use a FBG as a seismic sensor and as a bore-well characterizing sensor. A novel FBG seismic sensor package is developed using a single FBG sensor to pick up the seismic waves propagating through the ground generated from earthquakes and ground tremors. Further, FBG sensors are used for measurement of temperature profiles in a bore-well to delineate and characterize the behavior of fractures during seasonal climatic changes. To summarize, the present thesis demonstrates a comprehensive experimental study which bring out the utility of FBG sensors in a variety of challenging applications.

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This thesis describes a detailed study of advanced fibre optic sensors and their applications for label-free biochemical detection. The major contributions presented in this thesis are summarised below. A self-assembly based in-situ layer-by-layer (i-LbL) or multilayer deposition technique has been developed to deposit the 2D material nanosheets on cylindrical fibre devices. This deposition technique is based on the chemical bonding associated with the physical adsorption, securing high-quality 2D materials coating on specific fibre cylindrical surface with strong adhesion as well as a prospective thickness control. Then a " Photonic-nano-bio configuration", which is bioprobes immobilised 2D-(nano)material deposited fibre grating, was built. 2D material overlay provides a remarkable analytical platform for bio-affinity binding interface due to its exceptional optical and biochemical properties. EDC (1-ethyl-3-(3-dimethylaminopropyl)carbodiimide) and NHS (NHydroxysuccinimide) were used to immobilise bioprobes. This kind of configuration is considered to have many advantages such as: enhanced RI sensitivity, enrich immobilisation sites, improved binding efficiency, selective detection. Followed by this configuration, several label-free biosensors were developed. For example, graphene oxide coated dual-peak long period grating (GO-dLPG) based immunosensor has been implemented for ultrasensitive detection of antibody/antigen interaction. The GO-LPG based biosensor has been developed for label-free haemoglobin detection. Apart from biosensors, the black phosphorus (BP) integrated tilted fibre grating (TFG) has been proposed, for the first time, as BP-fibre optic chemical sensor for heavy metal (Pb2+ ions) detection, demonstrating ultrahigh sensitivity, lower limit of detection and wider concentration range. Ultrafast laser micromachining technology has been employed to fabricate long period grating (LPG) and microstructures on optical fibre. The ultrafast laser micromachined polymer optical fibre Bragg grating (POFBG) has been developed for humidity sensing, showing the significant improvement with the reduced response time.

Tese de mestrado integrado. Engenharia Mecânica. Faculdade de Engenharia. Universidade do Porto. 2010

A humidity fiber optic sensor based on phase-shifted (PS) Fiber Bragg gratings (FBG) is demonstrated. Compared to the standard FBG sensors, the peak of the PS-FBG slips into 2 narrow peaks and forms a sharp dip in the middle. As a result, the resolution of the measurement will be higher. The sensors used in the experiments were fabricated by coating the PS-FBG surface with a moisture-sensitive polyimide and is based on the strain effect caused by the swelling of the coating after moisture absorption. The same trend seen in a standard FBG sensor can be achieved, but with higher measurement resolution in environments differing by humidity and temperature. This thesis presents simulation and measurement results, including sensitivity and response time, of the PS-FBG sensor approach for humidity sensing, as compared to the standard FBG sensors. Stability and hysteresis are also discussed.