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  • About
  • The Global ETD Search service is a free service for researchers to find electronic theses and dissertations. This service is provided by the Networked Digital Library of Theses and Dissertations.
    Our metadata is collected from universities around the world. If you manage a university/consortium/country archive and want to be added, details can be found on the NDLTD website.

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Spelling suggestions: "subject:"hydridisation"" "subject:"dehydroiodination""

1

Simple Synthesis of Fresh Alkyl Iodides Using Alcohols and Hydriodic Acid

Klein, Suzane, Zhang, Cungen, Jiang, Yu Lin 14 April 2008 (has links)
A simple synthesis of fresh alkyl iodides using alcohols and hydriodic acid (HI) is reported. The alkyl iodides were obtained in quick and easy work-up with good to excellent yields (66-94%) and very high purities (97-99%). Freshly prepared iodomethane and 1-iodobutane were applied to synthesize biologically relevant 3,7-dimethyladenine and 9-butyladenine, which were characterized thoroughly using 1D and 2D NMR, individually.
alcohols
alkyl bromides
alkyl iodides
hydriodic acid
hydriodination
hydrobromination
hydrogen bromide

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