Poverty Point is a monumental earthwork center dating to the Late Archaic Period (ca. 3700-3100 Cal BP). The site is well known for its diverse collection of foreign lithic materials indicative of a wide-ranging acquisition network. Among the extra-local items recovered from the site are lithic raw materials that were used for bifaces in the form of projectile points and/or knives (PP/Ks). Here, I determined the atomic and molecular composition of 847 bifaces from the Alexander Collection using Visible/Near-Infrared Reflectance (VNIR) and Fourier-Transform Infrared Reflectance (FTIR) spectroscopy. The combined wavelength spectra datasets were compared to a raw material database to determine the location of the parent formations from which the raw materials were obtained. The PP/K raw materials analyzed were sourced to outcrops stretching across the Southeast, Mid-South and Mid-West.

Scholars of the Late Pleistocene in Southern Africa have recently sought to develop models explaining long-term variation between Middle Stone Age and Late Stone Age assemblages in terms of variability between “macrolithic” vs. “microlithic” toolmaking systems associated with shifts in hunter-gatherer ecology and land use patterns. While it has often proven extremely difficult to actually test many models, recently developed methods allow us to do so in novel ways. In this dissertation, I use new archaeological data from excavations of two sites in the Namib Desert, as well as new approaches to sourcing lithic artifacts to examine the hypothesis that contrasts between terminal Pleistocene (ca. 15-20 ka BP) and early Holocene (ca. 6-12 ka BP) occupation phases at the two sites represent adaptive responses primarily driven by changes in fluvial regimes and the resource productivity of riparian corridors. Analyzing the lithic assemblage compositions and locating probable source areas for raw materials suggests that terminal Pleistocene groups likely centered land use strategies more toward upland areas east of the study sites and periodically followed broad riparian corridors into the desert itself. Early Holocene groups expanded their ranges and more intensively targeted resources on the open desert plains, dunes, and beaches of the coastal lowlands. My results suggest environmental change may be partially responsible for driving this shift, but new data and methodological tools are needed to address factors like fluctuations in regional population size that may have been driving shifts in the late Pleistocene record of this unique region of Southern Africa.