Thesis (Ph. D.)--University of Missouri-Columbia, 2004. / Typescript. Vita. Includes bibliographical references (leaves 243-253). Also available on the Internet.

Thesis (M. Phil.)--University of Hong Kong, 2006. / Title proper from title frame. Also available in printed format.

The research presented in this thesis is to evaluate the feasibility of demountable shear connectors as an alternative to welded shear connectors in composite structures through push off tests and composite beam tests. Push off tests were conducted to examine the shear strength, stiffness and ductility of demountable shear connectors in composite structures. The experimental results showed that demountable shear connectors in composite structures have very similar shear capacity to welded shear connectors. The shear capacity was compared against the prediction methods used for the welded shear connections given in Eurocode 4 and AISC 360-10 and the methods used for bolted connections in Eurocode 3 and ACI 318-08. It was found that the AISC 360-10 and ACI 318-08 methods overestimated the shear capacity in some cases. The Eurocode method is conservative and can be utilised to predict the shear capacity of demountable connectors in composite structures. The experimental studies of two identical composite beams using demountable shear connectors and welded shear connectors showed very similar moment capacity. However, the specimen with demountable shear connectors was more ductile compared to the welded specimen. The experimental study suggests that the methods available in Eurocode 4 and BS 5950 for predicting moment capacity and mid span deflection can be adopted for composite beam with demountable shear connectors. In addition, a finite element analysis of push off test and beam test with demountable shear connectors was also conducted for parametric studies and results are used to evaluate the behaviour of composite structures.

In February of 2017 after a period of heavy rainfall, a slope destabilized behind Fremont Hall on the campus of Cal Poly San Luis Obispo. The geology of this slope stability failure is the Franciscan Complex. The Franciscan Complex, when weathered in place, results in clay soil that makes up the typical soil mantle on the hills throughout the region. Peak strength is the typical parameter tested to assess the strength of the soil. For the Franciscan-derived clay, the residual strength is the focus of this study to understand slope failure since the clay is the weakest portion of the matrix in the Franciscan Complex. Both intact and remolded specimens were processed from the samples obtained from the slide for laboratory testing. The tested material is considered representative of the soil found in the Franciscan Complex along the California coast and other similar regions worldwide where the presence of this mélange results in slope instabilities. Three different shearing tests were performed to study the residual strength: direct shear reversal, ring shear, and large-scale direct shear reversal. Sampling soil from the slide took place twice: once in 2017 and once in 2019. A block of soil sampled in 2017 was taken after the toe of the slope was cut for reconstruction which resulted in an exposed slide plane. In 2019, additional samples were retrieved near the toe of the slope after subsequent failure of the slope. Although the material was assumed to be from the slide plane, there is a possibility it may have originated from the surrounding matrix. Intact and remolded specimens were tested in direct shear reversal tests, and remolded specimens were tested in ring shear tests. The 2019 source was tested in the large-scale direct shear reversal tests because the material obtained during 2017 was not enough to replicate the large specimen. Remolded specimens were prepared by passing through sieve No. 40. A secondary set of tests were performed on specimens prepared by passing through sieve No. 200. When comparing remolded against intact specimens, the clasts within the intact material exhibited an influence on the residual strength by an approximate difference of 20%. The results also indicated the liquid limit (LL) had an impact on the residual strength; higher value LL exhibited lower residual strength, and lower value LL exhibited higher residual strength. When comparing the laboratory results against in situ CPT tests, the values from the CPT fell within the range of the laboratory residual strength corresponding to the slide’s depth of movement. The results from testing these specimens showed the soil obtained directly from the slide failure exhibited a residual strength represented as friction angle of 14° ± 2° for intact soil specimens, 11° ± 3° for remolded specimens of the 2017 failure plane passing through No. 40 sieve, and 22° ± 2° for remolded specimens of the 2019 sample location passing though No. 40 sieve. The remolded specimens passing through sieve No. 200 produced even lower results. However, since all clasts were removed by the No. 200 sieve, those results are not considered representative of field conditions. Based on the test results, and the infinite slope limit equilibrium slope stability analysis, a median range of residual strength for this slide is approximately 12.5 to 14.0°.

The research presented in this thesis is to evaluate the feasibility of demountable shear connectors as an alternative to welded shear connectors in composite structures through push off tests and composite beam tests. Push off tests were conducted to examine the shear strength, stiffness and ductility of demountable shear connectors in composite structures. The experimental results showed that demountable shear connectors in composite structures have very similar shear capacity to welded shear connectors. The shear capacity was compared against the prediction methods used for the welded shear connections given in Eurocode 4 and AISC 360-10 and the methods used for bolted connections in Eurocode 3 and ACI 318-08. It was found that the AISC 360-10 and ACI 318-08 methods overestimated the shear capacity in some cases. The Eurocode method is conservative and can be utilised to predict the shear capacity of demountable connectors in composite structures. The experimental studies of two identical composite beams using demountable shear connectors and welded shear connectors showed very similar moment capacity. However, the specimen with demountable shear connectors was more ductile compared to the welded specimen. The experimental study suggests that the methods available in Eurocode 4 and BS 5950 for predicting moment capacity and mid span deflection can be adopted for composite beam with demountable shear connectors. In addition, a finite element analysis of push off test and beam test with demountable shear connectors was also conducted for parametric studies and results are used to evaluate the behaviour of composite structures. / EPSRC and the University of Bradford

Phenol formaldehyde (PF) is the oldest known synthetic polymer. This polymer has seen many applications throughout history, including jewelry, electric wire insulation, and resins used to make adhesives. Today, PF resins are still crucial components used in the wood products industry. These PF resins are formulated into adhesives used to make plywood and various other wood composite products. For example, in the United States, 90 % of the homes are still frame homes that use plywood for construction. The PF adhesives used to make these composites are formulated using agricultural waste products like walnut shells and corn-cob residue. These organic waste products act as fillers that reduce the cost, increase the viscosity, and affect the rheology of the fillers. Wheat flour is added as an extender to reduce cost and affect the tack of the adhesive. These organic fillers are lignocellulosic materials that are made of lignin, cellulose, and hemicellulose. Not much is known about the interactions of these organic fillers and the polymer resin. Rheological studies in our lab have shown that not all of the additions to the adhesive formulation are inert components in the adhesive. The steady-state flow curve analysis of PF adhesives revealed that there is a liquid structure change that occurs at high shear rate. This structure change is observed as a viscosity increase that occurs after applying a maximum shear rate of 4000 1/s. A rheological analysis was conducted to determine the source of this change, with individual components added to the resin. The PF base resin (with nothing added) has a Newtonian rheological behavior. When wheat flour is added to the resin, the overall viscosity increases, and shear thinning occurs at highe shear rates. There is no final viscosity change observed on with the addition of wheat flour. Adding corn-cob residue to the resin increased viscosity, led to some shear thinning at higher shear rates, and allowed the viscosity changes observed in the fully formulated adhesives. These experiments showed that the liquid structural changes that occur in the adhesives are attributed to the organic fillers. All organic fillers used in our studies, including corn-cob residue, walnut shell, almond shell, and Alder bark produce different levels of viscosity change in the PF adhesive formulations. These biomass materials have varying amounts of lignocellulosic content, particle size distributions, and particle shape. Among the fillers, corn-cob residue was shown to cause the most viscosity change compared to any of the fillers. Corn-cob residue is unique compared to the others because it has undergone acid digestion to convert its xylans to furfural. During the viscoelastic oscillation studies, the corn-cob residue filled adhesives showed that they developed network structures in response to a high shear rate that were not observed using the other fillers. With the discovery of these network structures, the next goal of this research was to correlate the effects observed on the rheometer to relevant adhesive application technology like high shear spraying. The corn-cob residue adhesive was sprayed at approximately 70,000 1/s compared to the 4000 1/s of rotational shear on the rheometer. The viscoelastic oscillation studies revealed that there was no network structure formation after high-shear spraying. Further, there was no change observed in the flow curve analysis after spraying the adhesive. This study showed that there are limitations when trying to correlate changes that happen in adhesives during spraying, where extensional forces dominate compared to shear forces. In future research, there is the opportunity to explore the effects of extensional deformation that occurs during the atomization of the adhesive, which will be more reflective of the changes that occur during spraying. / Doctor of Philosophy / Phenol-formaldehyde adhesives are crucial products in the home construction industry. These adhesives are used to make plywood that is used to build frame homes, which represent approximately 90 % of the homes in the United States. These phenol-formaldehyde adhesives are made using organic materials repurposed from agricultural waste products like corn cobs, walnut shells, almond shells, and tree bark. These products help to enhance the properties of the adhesive, reduce the cost, and reduce the amount of resin used. The goal of this research is to understand better the interactions between the adhesive and the organic fillers using rheology. Rheology is a field that studies how materials change and flow with applied external forces. This is an important field because it provides information on viscosity and viscoelastic behavior. Our research has shown that in response to high shear rates, the viscosity of these phenol-formaldehyde adhesives increases. Studying these changes can lead to a better understanding of how these materials change during industrial spraying. This understanding could lead to improved building adhesive materials in the home construction industry.

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The behavior and strength of welded shear studs are subjects of ongoing study. In recent years, research has shown that the American Institute of Steel Construction (AISC) specification equations for shear stud strength are unconservative for studs placed in deck with ribs transverse to the steel beam. Twenty-four solid slab push-out tests, 93 composite slab push-out tests, and bare stud tests were performed to study the effects on stud strength of friction, normal load, position of studs in the ribs of steel deck, concrete strength, and stud properties. Stud diameters ranged from 3/8 in. to 7/8 in., deck heights ranged from 2 in. to 6 in., and both single and pairs of studs were tested. The push-out test results from this study were combined with other studies to propose a new stud strength prediction model. Three new beam tests were performed to study the effect of the stud position in the ribs of the steel deck. The results of these tests, along with 61 other beam tests, were used to verify the new stud strength prediction model. A reliability study was performed to determine resistance factors for stud strength and beam strength. / Ph. D.