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  • About
  • The Global ETD Search service is a free service for researchers to find electronic theses and dissertations. This service is provided by the Networked Digital Library of Theses and Dissertations.
    Our metadata is collected from universities around the world. If you manage a university/consortium/country archive and want to be added, details can be found on the NDLTD website.

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Carbon Dioxide-Mediated Preparation of Amine-Boranes

Daniel O'Neal Reddy (8893829) 15 June 2020 (has links)
<p>Since their discovery by Burg and Schlesinger in 1937, amine-boranes have enjoyed a rich preparative history and have experienced reinvigorated interest as valuable reagents for organic syntheses. Previously, the Herbert C. Brown Center for Borane Research has reported their synthesis from NaBH<sub>4</sub> and amines via the intermediacy of (NH<sub>4</sub>)<sub>2</sub>SO4 or NaHCO<sub>3</sub>. Described herein is a CO<sub>2</sub>-mediated amine-borane synthesis that accommodates all classes of amines, particularly long-chain trialkyl- and pyridine-like heteroarylamines.</p>
Organic Chemistry
amine-boranes
carbon dioxide (CO2)
synthetic chronology

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