This dissertation is focused on the design, fabrication, and characterization of novel metamaterials in microwave and terahertz regions with the following outcomes: A planar &micro / -negative metamaterial structure, called double-sided SRR (DSRR), is proposed in the first part of this study. DSRR combines the features of a conventional split ring resonator (SRR) and a broadside-coupled SRR (BC-SRR) to obtain much better miniaturization at microwave frequencies for a given physical cell size. In addition to DSRR, double-sided multiple SRR (DMSRR), double-sided spiral resonator (DSR), and double-sided U-spiral resonator (DUSR) have been shown to provide smaller electrical sizes than their single-sided versions under magnetic excitation. In the second part of this dissertation, a novel multi-band tunable metamaterial topology, called micro-split SRR (MSSRR), is proposed. In addition to that, a novel magnetic resonator structure named single loop resonator (SLR) is suggested to provide two separate magnetic resonance frequencies in addition to an electric resonance in microwave region. In the third part, two different frequency tunable metamaterial topologies called BC-SRR and gap-to-gap SRR are designed, fabricated and characterized at terahertz frequencies with electrical excitation for the first time. In those designs, frequency tuning based on variations in near field coupling is obtained by in-plane horizontal or vertical displacements of the two SRR layers. The values of frequency shifts obtained for these tunable metamaterial structures are reported to be the highest values obtained in literature so far. Finally, in the last part of this dissertation, novel double-sided metamaterial based sensor topologies are suggested and their feasibility studies are presented.