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Liquid-liquid extraction in a spray column

A study was made on the back mixing or circulation in the continuous phase of a spray type liquid-liquid extraction tower. Concentration profiles of both continuous and dispersed phases were obtained by internal sampling.
Mass transfer data are presented for the transfer of acetic acid between water and methyl isobutyl ketone in the 1.5-in. I.D. columns of three different heights. Considerable circulation
in the continuous water phase was observed which resulted
in the reduction of the driving force for mass transfer. A driving force correction factor, F(m), was obtained from the H.T.U. data using a simplified picture of behaviour at the interface.
The height of the tower did not seem to have any effect on F(m). The overall H.T.U. values, obtained from the experimental
profiles, were correlated with the flow rates.
The end effect due to the agitation and coalescence of the drops at the interface was measured. This end effect was correlated with the overall capacity coefficients and the dispersed
phase flow rates. / Applied Science, Faculty of / Chemical and Biological Engineering, Department of / Graduate

Identiferoai:union.ndltd.org:UBC/oai:circle.library.ubc.ca:2429/40923
Date January 1959
CreatorsRai Choudhury, Prosenjit
PublisherUniversity of British Columbia
Source SetsUniversity of British Columbia
LanguageEnglish
Detected LanguageEnglish
TypeText, Thesis/Dissertation
RightsFor non-commercial purposes only, such as research, private study and education. Additional conditions apply, see Terms of Use https://open.library.ubc.ca/terms_of_use.

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