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Super Duplex Stainless Steels have superior corrosion resistance properties and strength compared to conventional steels. However, these properties are influenced by the different phases that precipitate during the heat treatment process. The conventional way of studying the time and temperature effects on the properties and micro-structure of SDSS is to prepare many samples at different temperatures and holding times. The welding research group at Production Technology Center, Trollhättan, Sweden, has recently developed a unique heat treatment method to produce a wide range of temperature by using a stationary TIG arc heat source. It results in a graded micro-structure in a single sample at a specific time period. The accuracy of the results ob-ained from this process is highly related to the accuracy of the temperature field model next to weld pool. In this work, a model was developed by using OpenFOAM CDF code, to predict the temperature field of the super duplex stainless steel samples that have been subjected to this novel TIG arc heat treatment process. The developed model was able to capture the trend in the overall temperature field in the heat affected zone. However, there was some mismatch between the modelled and experimental temperature profiles in certain locations in the heat affected zone. Further improvements have to be done to the developed model in order to take the phase transformation effect into account. A preliminary investigation has been carried out on how to implement this in the current model and reported in the thesis.

With increasing miniaturization in microelectronics the wirebonds used in IC packages are witnessing a thrust towards fine pitch wirebonding. To have a precise control over loop height of the wirebond for fine pitch wirebonding, it is imperative to do mechanical characterization of the wirebond. The present work studies the mechanical properties of gold wire and wirebond using nanoindentation. The wirebond specimen surface was planarized using mechanical polishing. The loop height of the gold wirebond is directly proportional to the length of the heat affected zone (HAZ) above the ball of gold wirebond. Metallographic preparation of gold wirebond cross section reveals the presence of undesirable coarse grain structure in HAZ due to recrystallization and grain growth in the gold wire adjacent to the ball. The recrystallization temperature of our gold wire was found using D.S.C. to be 340.66°C. The doping elements present in the gold wire used, were identified using TOF-SIMS. Nanoindentation of the gold wire was done at different maximum loads to observe the hardness variation with load. The nanoindentation of gold wirebond has confirmed a v-shaped hardness profile in the HAZ. The hardness minima for the particular gold wire used with a ball size ratio of 2.4 was observed at distance of 160-170 µm from the neck of the ball. The elastic modulus was found to vary randomly and to be independent of the microstructure in the wirebond. A yield stress profile based on empirical hardness-yield strength correlation has been predicted for the gold wirebond. / Singapore-MIT Alliance (SMA)

The heat-affected zone (HAZ) is the most common region of weld failures. The weld failures are directly related to the microstructure. Microstructure control of the HAZ is crucial to weld quality and prevention of weld failures. However, publications on modeling the development of the HAZ are relatively limited. Moreover, no efforts have been made to predict the HAZ microstructures in real-time. The primary goal of this research is to present a methodology to enable real-time predictions of microstructure evolution in the HAZ and its mechanical properties. This goal was achieved by an approach based on materials science principles and real-time sensing techniques. In this study, the entire welding process was divided into a series of sub-processes. Real-time multiple measurements from multiple sensors were incorporated into the sub-processes. This resulted in an integrated welding system upon which the predictions for the final HAZ microstructure are based. As part of the integrated system, the microstructural model was used to predict the TTT curves, volume fractions of the decomposition products, and hardness numbers of the heat-affected zones of steel alloys. Actual welds were performed under two different sets of conditions, and the resulting experimental data were compared with predictions made using the microstructural model. The predicted and experimental microstructure and hardness are found to be in good agreement, indicating that the microstructural model can be used in real applications. This research can act as an important component of future research to enable physics-based flexible control of welding. / text

Haynes alloy 282 is a new gamma prime (γ’) precipitation strengthened nickel-base superalloy developed for high temperature applications in land-based and aero turbine engines. Joining is a crucial process both during the manufacturing of new components and repair of service-damaged turbine parts. Unfortunately, the new superalloy cracks during laser beam welding (LBW), which is an attractive technique for joining superalloys components due to its low heat input characteristic that preclude the geometrical distortion of welded components. This research is therefore initiated with the goal of studying and developing an effective approach for preventing or minimizing cracking during LBW of the new superalloy Haynes 282. Careful and detailed electron microscopy and spectroscopy study reveal, for the first time, the formation of sub-micron grain boundary M5B3 particles, in the material. Microstructural study of welded specimens coupled with Gleeble thermo-mechanical physical simulations shows that the primary cause of weld heat affected zone (HAZ) cracking in the alloy is the sub-solidus liquation reaction of intergranular M5B3 borides in the material. Further weldability study showed that the HAZ liquation cracking problem worsens with reduction in welding heat input, which is normally necessary to produce the desired weld geometry with minimum distortion. In order to minimize the HAZ cracking during low heat input laser welding, microstructural modification of the alloy by heat treatment at 1080 - 1100oC has been developed. The pre-weld heat treatment minimizes cracking in the alloy by reducing the volume fraction of the newly identified M5B3 borides, while also minimizing non-equilibrium grain boundary segregation of boron liberated during dissociation of the boride particles. Further improvement in resistance to cracking was produced by subjecting the material to thermo-mechanically induced grain refinement coupled with a pre-weld heat treatment at 1080oC. This approach produces, for the first time, crack-free welds in this superalloy, and the benefit of this procedure in preventing weld cracking in the new material is preserved after post-weld heat treatment (PWHT), as additional cracking was not observed in welded specimens subjected to PWHT.

Haynes alloy 282 is a new gamma prime (γ’) precipitation strengthened nickel-base superalloy developed for high temperature applications in land-based and aero turbine engines. Joining is a crucial process both during the manufacturing of new components and repair of service-damaged turbine parts. Unfortunately, the new superalloy cracks during laser beam welding (LBW), which is an attractive technique for joining superalloys components due to its low heat input characteristic that preclude the geometrical distortion of welded components. This research is therefore initiated with the goal of studying and developing an effective approach for preventing or minimizing cracking during LBW of the new superalloy Haynes 282. Careful and detailed electron microscopy and spectroscopy study reveal, for the first time, the formation of sub-micron grain boundary M5B3 particles, in the material. Microstructural study of welded specimens coupled with Gleeble thermo-mechanical physical simulations shows that the primary cause of weld heat affected zone (HAZ) cracking in the alloy is the sub-solidus liquation reaction of intergranular M5B3 borides in the material. Further weldability study showed that the HAZ liquation cracking problem worsens with reduction in welding heat input, which is normally necessary to produce the desired weld geometry with minimum distortion. In order to minimize the HAZ cracking during low heat input laser welding, microstructural modification of the alloy by heat treatment at 1080 - 1100oC has been developed. The pre-weld heat treatment minimizes cracking in the alloy by reducing the volume fraction of the newly identified M5B3 borides, while also minimizing non-equilibrium grain boundary segregation of boron liberated during dissociation of the boride particles. Further improvement in resistance to cracking was produced by subjecting the material to thermo-mechanically induced grain refinement coupled with a pre-weld heat treatment at 1080oC. This approach produces, for the first time, crack-free welds in this superalloy, and the benefit of this procedure in preventing weld cracking in the new material is preserved after post-weld heat treatment (PWHT), as additional cracking was not observed in welded specimens subjected to PWHT.

Developed thesis compares MAG welding and plasma welding, with the same input parameters. Based on the literature was reviewed weldability and welding of both methods. It was experimentally for both technologies specifically designed heat input, evaluation and macrostructure of the weld dilution, the dimensions of the heat affected zone and finally test the hardness in the transverse direction Vickers.

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Termisk modellring av hårdhet genom beräkning och simulering av den värmepåverkade zonen i en lasersvetsad stålplatta är en omfattande process. Dock är analysen viktig då mikrostrukturella fastransformationer förorsakade av svetsningen kan ge oönskade hårdhetsnivåer av den värmepåverkade zonen jämfört med hårdeheten i basmaterialet. I denna avhandling har analytiska ekvationer implementerats och testats för validitet mot simuleringar gjorda av andra författare och mot experimentella värden.Eftersom termisk modellering av svetsar är ett omfattande område var avhandlingen tvungen att smalnas av för att göra analysen mer fokuserad. Begränsningar gjordes för den matematiska modelleringen genom att endast titta på två-dimensionellt värmeflöde i svetsade plattor där endast den analytiska lösningen är av intresse. Arbetet har också inriktats mot stål då detta material är vida använt över hela världen. Då lasersvetsning är en snabb och kostnadseffektiv process så är hårdhetsanalysen av största vikt. Avhandlingen är uppdelad i tre övergripande delar; den första är att ta fram och förstå arbetet som gjorts inom termisk modellering av svetsar, alltså förstå matematiken bakom problemet. Modelleringen är till för att producera diagram parametrar från en termisk cykel, för att kunna fortgå med korrekt hårdhets analys. För det andra så sätts den matematiska modelleringen på prov i ett antal situationer som var och en simulerar olika förutsättningar. Detta gjordes i ett grafiskt användargränssnitt av ren bekvämlighet. Detta gör att ingenjörer lätt kan implementera olika egenskaper för materialet och få fram diagram och kurvor.Sist, ett liknande grafisk användargränssnitt för att simulera hårdheten i valfri punkt i den värmepåverkade zonen programmerades och därigenom implementerades ekvationerna som denna avhandling handlar om i grund och botten. En teoretisk bakgrund till fasomvandlingen är också inkluderad som förklaring till grundproblemet med oönskad hårdhet i den värmepåverkade zonen i lasersvetsat stål.Huvudslutsatser i avhandlingen:•Matematisk modellering av värmeöverföring i svetsar genomförd av Rosenthal är fortfarande applicerbar på modern lasersvetsningsapparatur. •Den empiriska modellen från Ion et al. (1984) är ej applicerbar med godkänt resultat för hårdhetsuppskattning.•Ekvationerna från Ion (2005) är statistiskt godkända för att simulera hårdhet.•Den analytiska lösningen är överlägsen den numeriska när det gäller snabb och enkel implementering för att simulera termiska cykler och hårdhet, medan den numeriska lösningen kan ta i beaktning mera avancerade egenskaper.•Förvärming av stålet innan svetsning kan vara mycket fördelaktigt för hårdheten i den värme-påverkade zonen, speciellt vid högre kolekvivalent. / Thermal modelling of hardness in the heat-affected zone (HAZ) in a laser welded steel plate is a cumbersome process both in calculation and simulation. The analysis is however important as the microstructural phase transformations induced by welding may cause unwanted hardness levels in the HAZ compared with that of the parent material. In this thesis analytical equations have been implemented and checked for validity against simulations made by other authors and against experimental values.With such a large field as thermal modelling, the thesis had to be narrowed down to make the analysis more subject focused. Limitations made were for mathematical modelling only looking at a two-dimensional heat flow in welded plates; in this thesis only the analytical solution to the heat flow is considered. The work was also directed towards steel; such a material as used largely all over the globe. As laser welding is a fast and cost-effective process, an analysis of hardness is of great importance. Work was divided into three overlapping parts; the first was to derive and understand the work done in the field of thermal modelling of welds, thus understanding the mathematics behind the basic problem. This modelling provides a number of curves and parameters from a thermal cycle, thus enabling one to do the hardness analysis correctly. Secondly, this mathematical modelling was applied to a number of cases, simulating different circumstances. This was done using self-programmed Graphical User Interfaces (GUI) for convenience. This enables engineers to easily plug in the materials and processing properties and thus simulate the required parameters and curves for further analysis.Lastly, a GUI for simulating the hardness of any point in the HAZ was programmed and used, thus implementing and validating the equations. A theoretical introduction of the phases induced in the HAZ is also included, in order of understanding the problems of unwanted hardness in the HAZ of laser-welded steel.Main conclusions of this thesis:•Mathematical modelling of heat transfer in welds by Rosenthal (1946) is still applicable for modern laser welding apparatus.•The empirical model presented by Ion et al. (1984) is not applicable with experimental results of hardness in the HAZ of the steels investigated here.•Equations by Ion (2005) are accurate for simulating the hardness.•The analytical solutions investigated are superior to numerical solutions with regard to quick, simple simulations of thermal cycles and hardness. Numerical solutions allows for more advanced modelling, which can be lengthy.•Preheating the steel prior to welding is favourable in reducing hardness levels, especially with steel of higher carbon equivalent.