Engineering industries usually require nondestructive evaluation (NDE) methods to ensure quality control, safety, and optimized use of resources. Among potential NDE techniques, ultrasonic wave methods are widely used because of their versatility and affordability. For applications to layered structures, ultrasonic guided waves are naturally excited and detected, so these guided waves are the preferred choice when compared to conventional bulk waves. The main advantage of guided waves over bulk waves for layered structures is that these guided waves can propagate a much farther distance, and thus they enable long range inspection. It is important to note that guided waves are multi-mode, so a preferred mode can be selectively used, although it is sometimes more efficient to use multiple wave modes. The characteristics of guided waves, namely dispersive propagation and attenuation, are directly related to the properties of the system in which they are propagating, so the measurement of these wave characteristics can be used for material characterization and condition monitoring. Despite a number of successful techniques to experimentally measure propagation characteristics of guided waves, there is a lack of a standard procedure to obtain attenuation characteristics. This research develops such a quantitative and systematic procedure to extract attenuation characteristics from real guided wave time-domain signals. This research considers multiple wave-modes, and focuses on broadband attenuation measurements with laser ultrasonic techniques. The analytical model of guided waves with attenuation is studied in general cases, and a numerical simulation is developed to model the point source/receiver laser measurement system. The attenuation extraction technique is developed using synthetic signals generated by the simulation. Finally, this research demonstrates the use of experimentally-measured attenuation data for material characterization and condition monitoring by developing an inversion scheme to back-calculate material properties for a number of practical cases.

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Measurements of the mechanical properties of lithium-ion battery electrode films can be used to quantify and improve manufacturing processes and to predict the mechanical and electrochemical performance of the battery. This thesis demonstrates the use of acoustic resonances to distinguish among commercial-grade battery films with different active electrode materials, thicknesses, and densities. Resonances are excited in a clamped circular area of the film using a pulsed infrared laser or speaker and responses are measured using an electret condenser microphone. A numerical model is used to quantify the sensitivity of resonances to changes in mechanical properties. When the numerical model is compared to simple analytical models for thin plates and membranes, the battery films measured here trend more similarly to the membrane model. Resonance measurements are also used to monitor the drying process. Results from a scanning laser Doppler vibrometer verify the modes excited in the films, and a combination of experimental and simulated results is used to estimate the Young's modulus of the battery electrode coating layer.

Indiana University-Purdue University Indianapolis (IUPUI) / Material jetting (MJ) additive manufacturing (AM) has experienced an increased adoption in several industry areas and as well as research applications. One of MJ’s distinct benefits is the ability to print tunable composites, digital materials (DM) by carefully adjusting the ratio of droplets of heterogeneous base-polymeric inks. However, the lack of material information usable in computer simulations has hampered its acceptance in some end-use applications. For these materials to be used in Finite Element Analysis (FEA) simulations the mechanical properties of the DMs need to be characterized into usable material models. DMs printable with an MJ printer has a wide variety of materials properties, ranging from flexible silicone rubber to rigid Acrylonitrile Butadiene Styrene (ABS). Therefore, to cohesively express the mechanical behavior of the DMs it is necessary to utilize non-linear material models. The objective this research is to conduct physical testing to characterize the mechanical behavior of DMs printable with an MJ. Subsequently, to validate the effectiveness of the material models for multi-DM prints. Utilizing the newly characterized material models two use cases were investigated, with the goal of improving the performance of printed parts through simulation. In this study, an MJ printer was used to fabricate the test specimens as well as the components used in the use case studies. The study was focused on the family of six DMs printable from the mixture of the base polymers Tango Black+ (TB+) and Vero White+ (VW+). To characterize the mechanical properties of the materials a tensile test was conducted utilizing the KS-M6518 standard as a basis. The mechanical properties of the DMs were then fitted into four non-linear models and the results compared. The fitted models were, the Neo Hookean model, a two-parameter, three-parameter, and a five-parameter Mooney Rivlin model. To confidently use the material models for multi-DM prints FEA simulations need to validate the accuracy to which they can predict the deformation of the samples under load. To compare the results of the computer simulations and the physical test, strain maps for both results were analyzed. Four different test specimens were printed and tested. A baseline single material samples were compared to three multi-material samples with different embedded structures. The results confirmed the validity of the material models even when used for multi-DM prints. The recently characterized models are utilized in two use case studies which showcase the potential of DMs. The first use case was focused on printing multi-DM substrates for the use of stretchable electronics. The second use case investigated the benefits of utilizing multiple materials to create 3D conductive traces utilizing a new method, the “swollen-off” method. Both case studies showed the benefits of utilizing DMs as well as the applicability of the material models in predictive simulations.

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In this dissertation, we examine mechanics of rhythmic tracheal compression (RTC) in the darkling beetle, Zophobas morio. In Chapter 2, we studied the relationship between hemolymph pressure and tracheal collapse to test the hypothesis that pressure is a driving mechanism for RTC. We found that tracheae collapse as pressure increases, but other physiological factors in the body may be affecting tracheal compression in live beetles. Additionally, as the tracheae compress, they do so in varying spatial patterns across the insect body. In chapter 3, we examined spatial variations in the taenidial spacing, stiffness, and tracheal thickness along the length of the tracheae. We related variations in Young's modulus and taenidial spacing with measurements of collapse dimples and found that spatial patterns of Young's modulus correlate with dimensions of collapse dimples. This correlation suggests an intuitive link between tracheal stiffness variations and the unique patterns observed in compressing tracheae. Lastly, in chapter 4, we studied the non-uniform collapse patterns in 3-D. By manually pressurizing the hemocoel and imaging using synchrotron microcomputed tomography (SR-µCT), we reconstructed the tracheal system in its compressed state. While previous studies used 2-D x-ray images to examine collapse morphology, ours is the first to quantify collapse patterns in 3-D and compare with previous 2-D quantification methods. Our method is also the first to make a direct measure of tracheal volume as the tracheal system compresses, similar to the phenomenon that occurs during rhythmic tracheal compression. / Doctor of Philosophy / Insects have long been a source of curiosity and inspiration for scientists and engineers. The insect respiratory system stands as an example of a seemingly complex oxygen delivery system that operates with relative simplicity. As opposed to mammals and other vertebrates, the insect respiratory system does not deliver oxygen using blood. Instead, insects possess a massive network of hollow tracheal tubes that are distributed throughout the body. Air enters spiracular valves along the length of the insect body, travels through the tracheal tube network, and is delivered directly to the tissues. In some insects, the tracheae compress and expand, driving flow of respiratory gasses. However, unlike vertebrate lungs, there are no muscles directly associated with the tracheal system that would drive this tracheal compression, and exactly how this behavior occurs is not fully understood. In this dissertation, we examined pulsatory increases in blood pressure as a possible mechanism that underlies these tracheal compressions in the darkling beetle, Zophobas morio. Additionally, as the tracheae compress, they do so with varying spatial patterns across the insect body. Because tracheae are complex and non-uniform composite tubes, we examined spatial variations in the microstructure, stiffness, and tracheal thickness along the length of the trachea. Lastly, we visualized the variable collapse patterns in three dimensions using synchrotron micro-computed tomography combined with manual pressurization of the hemocoel. While previous studies used two-dimensional x-ray images to quantify tracheal collapse patterns, this work represents the first three-dimensional study. Understanding tracheal collapse mechanics, material properties, and their relationships with the circulatory system can help to gain an understanding of how insects create complex fluid flows within the body using relatively simple mechanisms.

With increasing frequency up to the THz frequency range and the desire to optimize performance of modern applications, precise knowledge of the dielectric material parameters of a substrate being used in a planar application is crucial: High performance of the desired device or circuit can often be achieved only by properly designing it, using specific values for the material properties. Especially the integration of planar devices for very broadband applications at high frequencies often demands specific dielectric properties such as a low permittivity, dispersion and loss, assuring a predictable performance over a broad frequency range. Therefore, material characterization at these frequencies is of interest to the developing THz community, although not a lot of methods suitable in terms of frequency range and measurement setup exist yet. In this work, a comprehensive method for dielectric material parameter determination from S-Parameter measurements of unloaded and loaded planar transmission lines up to THz frequencies is developed. A measurement setup and methodology based on wafer prober measurements is established, which allows for characterization of planar substrates and bulk material samples alike. In comparison with most existing methods, no specialized measurement cell or cumbersome micro-machining of material samples is necessary. The required theory is developed, including a discussion of effective parameter extraction methods from measurement, identification of and correction for undesired transmission line effects such as higher order modes, internal inductance and surface roughness, as well as mapping and modelling procedures based on physical permittivity models and electromagnetic simulations. Due to the general approach and modular structure of the developed method, new models to cover additional aspects or enhance its performance even further are easily implementable. Measurement results from 100 MHz to 500 GHz for planar substrates and from 100 MHz to 220 GHz for bulk material samples emphasize the general applicability of the developed method. It is inherently broadband, while the upper frequency limit is only subject to the fabrication capabilities of modern planar technology (i.e. minimum planar dimensions of transmission lines and height of substrate) and thus is easily extendable to higher frequencies. Furthermore, the developed method is not bound to a specific measurement setup and applicable with other measurement setups as well, as is exemplary presented for a free-space setup using antennas, enabling measurement of large, flat material samples not fitting on the wafer prober. Several substrate and bulk material samples covering a wide range of permittivities and material classes are characterized and compared with reference values from literature and own comparison measurements. The uncertainties for both planar substrate as well as bulk material sample measurements are estimated with a single-digit percentage. For all measurements, the order of magnitude of the dielectric loss tangent can be determined, while the lower resolution boundary for bulk material sample measurements is estimated to 0.01. Concerning measurements in the wafer prober environment, fixture-related issues are a main cause of measurement uncertainty. This topic is discussed as well as the design of on-wafer probe pads and custom calibration standards required for broadband operation at THz frequencies. / Mit zunehmender Erschließung des THz-Frequenzbereichs und der zugehörigen Optimierung moderner Anwendungen ist eine genaue Kenntnis der dielektrischen Materialparameter verwendeter planarer Substrate unabdingbar: Eine hohe Performance angestrebter Bauteile oder Schaltungen kann nur durch einen präzisen Entwurf sichergestellt werden, wofür spezifische Werte für die Materialeigenschaften bekannt sein müssen. Insbesondere die Integration planarer Bauelemente für sehr breitbandige Anwendungen bei hohen Frequenzen bedingt spezifische dielektrische Materialeigenschaften, wie bspw. geringe Permittivität, Dispersion und Verluste, sodass eine vorhersagbare Performance über einen breiten Frequenzbereich sichergestellt werden kann. Materialcharakterisierung bei diesen Frequenzen ist folglich von Interesse für die sich entwickelnde THz-Forschungslandschaft, wenngleich derzeit kaum Verfahren existieren, die geeignet in Bezug auf den Frequenzbereich oder Messaufbau sind. Im Rahmen dieser Arbeit wird ein umfassendes Verfahren zur Bestimmung der dielektrischen Materialparameter aus S-Parameter-Messungen unbelasteter und belasteter planarer Leitungen bis in den THz-Bereich entwickelt. Ein Messaufbau mitsamt Messmethodik basierend auf Wafer Prober-Messungen wird entworfen, welcher die Charakterisierung von planaren Substraten und losen Materialproben ermöglicht. Im Vergleich zu existierenden Verfahren ist weder eine spezielle Messzelle noch eine umständliche Mikrobearbeitung der Materialproben notwendig. Die Entwicklung der hierfür notwendigen Theorie beinhaltet eine Diskussion von Methoden zur Extraktion effektiver Parameter aus Messungen, die Identifikation und Korrektur unerwünschter Leitungseffekte wie bspw. höherer Moden, interner Induktivität und Oberflächenrauhigkeit sowie Zuordnungs- und Modellierungsverfahren basierend auf physikalischen Permittivitätsmodellen und elektromagnetischen Simulationen. Durch den allgemeinen, modularen Ansatz des entwickelten Verfahrens lassen sich neue Modelle zur Berücksichtigung zusätzlicher Effekte oder weiteren Verbesserung der Performance einfach einarbeiten. Messergebnisse von 100 MHz bis 500 GHz für planare Substrate und von 100 MHz bis 220 GHz für lose Materialproben unterstreichen die allgemeine Anwendbarkeit des entwickelten Verfahrens. Es ist inhärent breitbandig, wobei eine obere Frequenzgrenze nur durch die Fertigungstoleranzen moderner planarer Technologien gegeben ist (minimale Leitungsdimensionen und Substrathöhe), sodass es einfach zu höheren Frequenzen hin erweiterbar ist. Weiterhin ist das entwickelte Verfahren nicht an einen bestimmten Messaufbau gebunden und auch mit weiteren Aufbauten anwendbar, wie beispielhaft an einem Freiraum-Aufbau mit Antennen präsentiert wird. Eine Vielzahl planarer Substrate und loser Materialproben, die ein weites Spektrum an Permittivitäten und Materialklassen abdecken, werden charakterisiert und mit Referenzdaten aus der Literatur sowie eigenen Messungen verglichen. Die Messunsicherheiten der Permittivitätsmessungen werden im einstelligen Prozentbereich abgeschätzt und der dielektrische Verlustwinkel kann in seiner Größenordnung bestimmt werden. Aufbaubezogene Einflüsse als eine Hauptursache für Messunsicherheiten am Wafer Prober werden adressiert, ebenso wie der Entwurf von On-Wafer Probe Pads und selbsterstellter Kalibrierstandards, die notwendig sind für den Einsatz bei THz-Frequenzen.

There is a need to monitor the existence and effects of damage in structural materials. Aircraft components provide a much publicized example, but the need exists in a variety of other structures, such as layered materials used in food packaging industries. While several techniques and models have been proposed for material characterization and condition monitoring of bulk materials, less attention has been devoted to thin sheets having no flexural rigidity. This study is therefore devoted to the development of a new method for acoustic Non-Destructive Testing (NDT) and material characterization of thin sheets used in food packaging materials or similar structures. A method for assessing the strength in the presence of crack of thin sheets used in food packaging is first presented using a modified Strip Yield Model (SYM). Resonance frequency measurement is then introduced and it is shown, at low frequency range (less than 2kHz), that a change in the physical properties such as a reduction in stiffness resulting from the onset of cracks or loosening of a connection causes detectable changes in the modal properties, specifically the resonance frequency. This observation leads to the implementation of a simple method for damage severity assessment on sheet materials, supported by a new theory illustrating the feasibility of the detection of inhomogeneity in form of added mass, as well as damage severity assessment, using a measurement of the frequency shift. A relationship is then established between the resonance frequency and the material’s elastic property, which yields a new modality for sheet materials remote characterization. The result of this study is the groundwork of a low-frequency vibration-based method with remote acoustic excitation and laser detection, for nondestructive testing and material characterization of sheet materials. The work also enhances the feasibility of the testing and condition monitoring of real structures in their operating environment, rather than laboratory tests of representative structures. The sensitivity of the new experimental approach used is liable to improvement while being high because the frequency measurement is one of the most accurate measurements in physics and metrology.

The development of modern digital communication systems has been entered a new era with faster signal transmission and processing capability, called high-speed circuit systems. As their clock frequencies have increased and rise times of signals have decreased, the signal integrity of interconnects in the packaging and printed circuit boards plays a more and more important role. In high-speed circuit systems, the well-designed logic functions most likely will not work well if their interconnects are not taken into account.This dissertation addresses to profoundly understand the signal integrity knowledge, be proficient in calculation, simulation and measurements, and be capable of solving related signal integrity problems. The research mainly emphasizes on three aspects. First of all, the impact of on-wafer calibration methods on the measured results of coplanar waveguide circuits is comprehensively investigated, with their measurement repeatability and accuracy. Furthermore, a method is presented to characterize the physically-consistent broadband material properties for both rigid and flexible dielectric materials. Last but not least, a hybrid method for efficient modeling of three dimensional via structures is developed, in order to simplify the traditional 3D full-length via simulations and dramatically reduce the via build and simulation time and complexity.