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Hydrogen peroxide is used in various fields, such as food preservative, bleaching, oxidizing, reducing, and chemical reaction reagents. However, inappropriate use may have harmful effects to human health or environment. A number of analytical methods have been developed for the determination of hydrogen peroxide. Herein is described the effort to develop an optical fiber chemical sensor based on the evanescence wave absorbance that can detect the presence of, and measure the concentration of, hydrogen peroxide. For the H2O2 optical fiber sensor, Nafion membrane was coated in the fiber optic. Titanium ions dispersed in a Nafion membrane can form a TiO-H2O2 complex with the H2O2 diffused into the membrane. The complex is shown to absorb light with a maximum absorption near 360 nm. The intensity of the absorbance peak is directly proportional to the concentration of H2O2. At present, this sensor has been tested for detecting H2O2 concentrations ranging from 0.03 ppm to 9 ppm in an aqueous solution at room temperature. Additionally, coating polydimethylsiloxiane (PDMS) outside the fiber optic can detect H2O2 in high concentration 300ppm and high temperature 70oC. Finally, the use of the developed optical fiber chemical sensor allows the direct determination of H2O2 in milk.

Interferometric fiber optic sensors have been extensively used to measure a large variety of physical, chemical and biomedical parameters due to their superior performance. At the Center for Photonics Technology of Virginia Tech, a variety of interferometric fiber optic sensors have been developed in recent years, for efficient oil recovery, partial discharge detection in high voltage transformers, pressure sensing in gas turbine engines, and temperature measurements in gasifiers and boilers. However, interrogating an interferometric sensor involves accurate recovery of a measurand from the phase-modulated lightwaves, and has been a challenge for high performance, high speed, and low-cost, to current white-light interferometry (WLI) techniques, such as the widely used scanning WLI (S-WLI) and spectral-domain WLI (SD-WLI). The performance of a white-light interferometric sensing system depends not only on the design of the probes, but also, to a great extent, on the interrogation strategy to be used. In this Ph.D. research, a tunable optical filter based WLI (TOF-WLI) is proposed and validated as a low cost, yet high performance, solution to the interrogation of various types of interferometric sensors. In addition to the capability of linear/quadrature demodulation, TOF-WLI retains all the features of WLI, is compatible with the SD-WLI, and can be tailored for both static and wideband signals. It also has great potential in surface metrology and biomedical imaging as well as optical spectroscopy. The key, to the success of this new approach in competition with the other available WLI techniques, is that the tunable optical filter (TOF) must be specially designed for sensing and extremely low cost. Therefore, two novel TOFs, a diffraction grating tunable filter (DG-TOF) and an extrinsic Fabry-Perot tunable filter (EFP-TF), are proposed and demonstrated. Laboratory and field test results on using the DG-TOF WLI for partial discharge and thermal fault detection in high voltage power transformers, and the EFP-TF WLI in temperature sensor systems and a turbine engine monitoring system will also be presented to demonstrate the feasibility for efficient sensor interrogation. / Ph. D.

The reason of the essay research find position of leakage point, and design a fiber optical leakage detection system. The research of fiber optical detection system in past year, because property of structure produce SNR smaller, quality of detection system is too bed. The essay brings to a hybrid Mach-Zehnder & Sagnac interferomtric can improve the SNR to 10dB. Therefore, it provides the better SNR. The experiment is added to signal process, such as PTL, PGC structure. To provide the systematic characteristic, such as dynamic range(60dB), percentage error(0.025%). The focal of the essay provide leak detection systematic characteristics how we make use of signal process.

The main frame of the distributed fiber optic leak detection system adopted the hybrid Mach-Zehnder & Sagnac interferomtric. We use the sensing fiber of In-Line frame to detect leak physical field. We can measure the position of the leak physical field through our sensing system and signal process system. In the cause of improving detective ability of leak detection system, we modify three elements of the system, including (1) the choice of the acoustic response of sensing fiber, (2) modification of the PZT phase modulator, and (3) modification of the PGC demodulator. The frame of our experiment is composed of the distributed fiber optic leak detection system and leak system of the fluid pipes. In which leak system of fluid pipes is designed the leaky frame of high-pressure fluid pipes. The main of experiment introduce the leak detection system to measure the leak acoustics of the fluid pipes. Then we can discuss the experimental result. The measurable minimum range of our distributed fiber optic leak detection system is3.3x10^-4(rad/¡ÔHz), and the dynamic range is above 75 dB. The dynamic range of this system can improve the original system to above 15 dB.

[pt] Nesta dissertação são relatadas as etapas que resultam na construção do protótipo de um receptor acústico a Fibra Óptica (RAFO). O trabalho faz parte de um projeto mais amplo visando o desenvolvimento de um medidor de vazão sônico baseado em fibras ópticas. Nesta fase inicial, os esforços foram voltados para a concepção, construção e testes do protótipo do transdutor, responsável pela deteção dos sinais sônicos emitidos por uma fonte, baseado em tecnologia de fibras ópticas. O uso de um sensor extrínseco foi a solução aqui empregada, que adota uma proposta de medição diferente da utilizada em medidores de vazão sônicos convencionais. O sistema de medição de vazão proposto na linha de pesquisa na qual este trabalho está inserido, baseia-se em medidas de tempo de transito para daí inferir a vazão volumétrica do fluido que escoa pelo duto. O sistema foi concebido para operar apenas numa banda estreita de frequências, casada com o sinal senoidal emitido pela fonte sonora. Neste trabalho um receptor acústico a fibra óptica foi projetado, montado e testado, tendo seu funcionamento sido demonstrado para freqüências de operação em torno de 3,2 kHz. A escolha desta faixa de frequências deveu-se basicamente a limitações do sistema de leitura optoeletronico utilizado nos testes de medição. Entretanto, uma vez que o princípio de funcionamento foi demonstrado com sucesso, não existem limitações para o re-dimensionamento do sensor de forma que este possa vir a operar em bandas de freqüência mais elevadas. / [en] This thesis reports the steps that have led to the assemblage and testing of na optical fiber microphone. This is part of a greater effort directed towards the development a sonic flowmeter based on optical fiber technology. In this first phase of the project, focus has been placed on the conception, construction, and testing, of the acoustic receiver first prototype. This transducer will be responsible for capturing the acouustical signails sent by an emitter, also based on optical fiber technology, and which is yet to be developed. In constrast with conventional sonic flowmeters, in which time of flight of acoustical pulses is the measured quantity related to flow rate, we are proposing a system based on measurement of phase difference between emitted and received sinusoidal signals.Hence, the acoustic receiver has been conceived to operate in a narrow frequency band. In particular, the developed prototype has been designed to operate in a frequency band centered at 3.2 kHz. This choice has been dictated by the response of the optoeletronic circuit employed in tests performed with the receiver operating in air and water. Nevertheless, since the principle of operation has been measurement of acoustical signails in higher frequency bands.

The use of optical fiber sensors is increasing widely in civil, industrial, and military applications mainly due to their, (a) miniature size, (b) high sensitivity, (c) immunity from electro-magnetic interference, (d) resistance to harsh environments, (e) remote signal processing ability, and, (f) multiplexing capabilities. Because of these advantages a variety of optical fiber sensing techniques have evolved over the years having potentials for myriad of applications. One very challenging job, for any of these optical fiber sensing techniques, is to implement a stand alone system with the design and development of all the signal processing models along with the necessary hardware, firmware, and software satisfying the real-time signal processing requirements. In this work we first develop the equations for the system model of the wavelength modulated extrinsic Fabry-Perot interferometric (EFPI) optical fiber sensor, and then design and build all the hardware and software necessary to implement a stand-a / Ph. D.

Structural health monitoring (SHM) has become a strong national interest because of the need of reliable and accurate damage detection methods for aerospace, civil and mechanical engineering infrastructure. Health monitoring of these structures usually requires the sensors to have such features as large area coverage, maintenance free or minimum maintenance, ultra-low cost per measurement point, and capability of operation in harsh environments. Fiber Bragg grating (FBG) has attracted considerable interest for this application because of its compactness, electromagnetic immunity, and excellent multiplexing capability. Several FBG multiplexing techniques have been developed to increase the multiplexing number and further reduce the unit cost. To the author's best knowledge, the current demonstrated maximum multiplexing number are 800 FBG sensors in a single array using optical frequency domain reflectometry (OFDR), whose maximum fiber span is limited by the coherence length of light source. In this work, we proposed and demonstrated a wavelength-scanning time-division multiplexing (WSTDM) of 1000 ultra-weak FBGs for distributed temperature sensing. In comparison with the OFDR method, the WSTDM method distinguishes the sensors by different time delays, and its maximum operation distance, which is limited by the transmission loss of the fiber, can be as high as tens of kilometers. The strong multiplexing capability and low crosstalk of the ultra-weak FBG sensors was investigated through both theoretical analysis and experiment. An automated FBG fabrication system was developed for fast FBG fabrication. With this WSTDM method, we multiplexed 1000 ultra-weak FBGs for distributed temperature sensing. Besides the demonstrated temperature measurement, the reported method can also be applied to measure other parameters, such as strain, pressure. / Ph. D.

Several techniques for measuring humidity are presented. The goal of the study is to use the electrostatic self-assembled monolayer synthesis process to fabricate a Fabry-Parot Cavity based optical fiber humidity sensor. The sensing scheme bases on the refractive index change with relative humidity of the film applied to the end of optical fiber. That is, the change in reflected optical power indicates certain humidity. To achieve this, some chemicals induce on specific coating materials were applied at the end of optical fiber. In this thesis, experimental results are given to prove that the humidity sensor has high sensitive and fast response time. Furthermore, we investigate the potential for the use of human breathing monitoring and air flow rate detection. Results from preliminary tests of each are given. / Master of Science

A slab-coupled optical fiber sensor (SCOS) falls into a narrow class of all-dielectric optical fiber electric field sensors, which makes it a perfect candidate for measurements of high electric fields in environments where presence of conductors is highly perturbing to the system under test. Its nonlinear response to high fields requires a new nonlinear calibration technique. A nonlinear calibration method is explained and demonstrated to successfully measure high electric fields, as well as high voltages with dynamic range up to 50 dB. Furthermore, a SCOS can be fitted into narrow spaces and make highly localized measurements due to its small size. This allows a SCOS to be integrated inside a standard high voltage coaxial cable, such as RG-218. Effects of partial discharge and arcing is minimized by development of a fabrication method to avoid introduction of impurities, especially air-bubbles, into the cable during SCOS insertion. Low perturbation of the measured voltage is shown by simulating the introduced voltage reflections to be on the order of –50 dB. It is also shown that a SCOS can be inserted into other cables without significant perturbation to the voltage. A complete high voltage and high electric field measurement system is built based on the high-voltage modifications of the SCOS technology. The coaxial SCOS is enhanced for robustness. Enhancements include packaging a SCOS into stronger ceramic trough, strengthening the fiber with kevlar reinforced furcation tubing and protecting the sensor with metal braces and protective shells. The interrogator is protected from electromagnetic interference with an RF-shielded box. Reduction in power losses introduced by the new PANDA-SCOS technology allows interrogator bandwidths to be increased up to 1.2 GHz. The whole measurement process is streamlined with dedicated software, developed specifically for high voltage and electric field measurements with support for the nonlinear calibration.