Estudos mostram que ocorre uma compactação superficial após alguns anos de utilização do sistema plantio direto (SPD), podendo interferir no desenvolvimento das plantas. A escarificação tem sido utilizada para amenizar os efeitos da compactação sob SPD, porém há evidências de que seus efeitos são de curta duração. O objetivo deste trabalho foi avaliar o comportamento de alguns parâmetros físicos após a escarificação em curto prazo (um ano) nas seguintes profundidades: 0,0-0,10 m; 0,10-0,20 m; 0,20-0,30 m; 0,30-0,40 m. A densidade do solo (Ds) e o grau de compactação (Gc) foram analisados em área de plantio direto por 16 anos (PD), imediatamente após a escarificação (ESC), seis meses (ESC6M) e um ano após a escarificação (ESC12M). Nas camadas superiores a densidade do solo apresentou variação semelhante, com redução significativa em ESC e um aumento expressivo em ESC6M, sendo que a Ds retornou aos valores registrados antes da mobilização em ESC12M. Nos períodos ESC, ESC6M e ESC12M foi observado um aumento da Ds na camada 0,30-0,40 m em comparação com o PD. A escarificação provocou redução do grau de compactação nas camadas 0,0-0,10 m e 0,10-0,20 m, com o Gc retornando aos valores originais um ano após a escarificação. Os maiores valores de Gc foram observados seis meses após a escarificação, porém o solo apresentou grande recuperação visto que em ESC12M o grau de compactação apresentou tendência de retorno aos valores originais em todas as profundidades, possivelmente devido à alta resiliência do solo. Os efeitos da escarificação avaliados pela Ds e Gc apresentaram duração inferior a um ano, sugerindo que neste solo não é necessária esta operação. / Studies show that a surface compaction occurs after some years adoption of no-tillage (NT), which may interfere in plant development. Chiseling has been used to alleviate the effects of soil compaction under NT, but studies show that this operation has short-term effects. The aim of this study was to evaluate the behavior of some physical parameters after chiseling in shortterm (one year) in the following depths: 0.0 to 0.10 m, 0.10-0.20 m, 0.20-0, 30 m, 0.30 to 0.40 m. Soil bulk density (BD) and the degree of compactness (DC) were analyzed in long-term (16 years) no-tillage (NT), chiseling of the long-term no-tillage (CHI), six months (CHI6M) and one year after chiseling (CHI12M). In top layers bulk density showed similar variation, with significant reduction in CHI and a marked increase in CHI6M, returning to the values recorded before mobilization in CHI12M. In periods CHI, CHI6M and CHI12M was an increase in the BD 0.30-0.40 m layer in comparison with NT. Chiseling caused a reduction the degree of compaction in the layers 0.0-0.10 m and 0.10-0.20 m, with DC returning to the original values one year after chiseling. The greatest DC values were observed six months after chiseling, nevertheless the soil showed great recovery whereas in CHI12M the degree of compactness tended to return to the original values in all layers, possibly due the high soil resilience. The duration of chiseling effects measured by BD and DC was less than one year, suggesting in this soil is not necessary this operation.

Estudos mostram que ocorre uma compactação superficial após alguns anos de utilização do sistema plantio direto (SPD), podendo interferir no desenvolvimento das plantas. A escarificação tem sido utilizada para amenizar os efeitos da compactação sob SPD, porém há evidências de que seus efeitos são de curta duração. O objetivo deste trabalho foi avaliar o comportamento de alguns parâmetros físicos após a escarificação em curto prazo (um ano) nas seguintes profundidades: 0,0-0,10 m; 0,10-0,20 m; 0,20-0,30 m; 0,30-0,40 m. A densidade do solo (Ds) e o grau de compactação (Gc) foram analisados em área de plantio direto por 16 anos (PD), imediatamente após a escarificação (ESC), seis meses (ESC6M) e um ano após a escarificação (ESC12M). Nas camadas superiores a densidade do solo apresentou variação semelhante, com redução significativa em ESC e um aumento expressivo em ESC6M, sendo que a Ds retornou aos valores registrados antes da mobilização em ESC12M. Nos períodos ESC, ESC6M e ESC12M foi observado um aumento da Ds na camada 0,30-0,40 m em comparação com o PD. A escarificação provocou redução do grau de compactação nas camadas 0,0-0,10 m e 0,10-0,20 m, com o Gc retornando aos valores originais um ano após a escarificação. Os maiores valores de Gc foram observados seis meses após a escarificação, porém o solo apresentou grande recuperação visto que em ESC12M o grau de compactação apresentou tendência de retorno aos valores originais em todas as profundidades, possivelmente devido à alta resiliência do solo. Os efeitos da escarificação avaliados pela Ds e Gc apresentaram duração inferior a um ano, sugerindo que neste solo não é necessária esta operação. / Studies show that a surface compaction occurs after some years adoption of no-tillage (NT), which may interfere in plant development. Chiseling has been used to alleviate the effects of soil compaction under NT, but studies show that this operation has short-term effects. The aim of this study was to evaluate the behavior of some physical parameters after chiseling in shortterm (one year) in the following depths: 0.0 to 0.10 m, 0.10-0.20 m, 0.20-0, 30 m, 0.30 to 0.40 m. Soil bulk density (BD) and the degree of compactness (DC) were analyzed in long-term (16 years) no-tillage (NT), chiseling of the long-term no-tillage (CHI), six months (CHI6M) and one year after chiseling (CHI12M). In top layers bulk density showed similar variation, with significant reduction in CHI and a marked increase in CHI6M, returning to the values recorded before mobilization in CHI12M. In periods CHI, CHI6M and CHI12M was an increase in the BD 0.30-0.40 m layer in comparison with NT. Chiseling caused a reduction the degree of compaction in the layers 0.0-0.10 m and 0.10-0.20 m, with DC returning to the original values one year after chiseling. The greatest DC values were observed six months after chiseling, nevertheless the soil showed great recovery whereas in CHI12M the degree of compactness tended to return to the original values in all layers, possibly due the high soil resilience. The duration of chiseling effects measured by BD and DC was less than one year, suggesting in this soil is not necessary this operation.

The phenomenon called soil aggregate coalescence occurs at contact-points between aggregates and causes soil strength to increase to values that can inhibit plant root exploration and thus potential yield. During natural wetting and drying, soil aggregates appear to ‘weld’ together with little or no increase in dry bulk density. The precise reasons for this phenomenon are not understood, but it has been found to occur even in soils comprised entirely of water stable aggregates. Soil aggregate coalescence has not been widely observed and reported in soil science and yet may pose a significant risk for crops preventing them from achieving their genetic and environmental yield potentials. This project used soil penetrometer resistance and an indirect tensile-strength test to measure the early stages of aggregate coalescence and to evaluate their effects on the early growth of tomato plants. The early stages of aggregate coalescence were thought to be affected by a number of factors including: the matric suction of water during application and subsequent drainage, the overburden pressure on moist soil in the root zone, the initial size of soil aggregates prior to wetting, and the degree of sodicity of the soil aggregates. Seven mainexperiments were conducted to evaluate these factors. The matric suction during wetting of a seedbed affects the degree of aggregate slaking that occurs, and the strength of the wetted aggregates. The matric suction during draining affects the magnitude of ‘effective stresses’ that operate to retain soil structural integrity as the soil drains and dries out. An experiment was conducted to evaluate the influence of matric suction (within a range of suctions experienced in the field) on aggregate coalescence using soils of two different textures. Sieved aggregates (0.5 to 2 mm diameter) from a coarse-textured and two fine-textured (swelling) soils were packed into cylindrical rings (4.77 cm i.d., 5 cm high) and subjected to different suctions on wetting (near-saturation, and 1 kPa), and on draining (10 kPa on sintered-glass funnels, and 100 kPa on ceramic pressure plates). After one-week of drainage, penetrometer resistance was measured as a function of depth to approximately 45 mm (penetrometer had a recessedshaft, cone diameter = 2 mm, advanced at a rate of 0.3 mm/min). Tensile strength of other core-samples was measured after air-drying using an indirect “Brazilian” crushing test. For the coarse-textured soil, penetrometer resistance was significantly greater for samples wet to near-saturation, despite there being no significant increase in dry bulk density; this was not the case for the finer-textured soils, and it was difficult to distinguish the effects of variable bulk density upon drying from those of the imposed wetting treatments. In both coarse- and fine-textured soils, the tensile strength was significantly greater for samples wet to near-saturation. Thus wetting- and draining-suctions were both found to influence the degree of soil aggregate coalescence as measured by penetrometer resistance and tensile strength. Aggregate coalescence in irrigated crops is known to develop as the growing season progresses. It was therefore thought to be linked to the repeated occurrence of matric suctions that enhance the phenomenon during cycles of wetting and draining. An experiment was conducted to determine the extent of aggregate coalescence in a coarsetextured and two fine-textured (swelling clay) soils during 8 successive cycles of wetting and draining. Sieved aggregates (0.5 to 2 mm diameter) from each soil were packed into cylindrical rings (4.77 cm i.d., 5 cm high) and wetted to near saturation for 24 h. They were then drained on ceramic pressure plates to a suction of 100 kPa for one week, after which penetrometer resistance and tensile strength were measured as described above. The degree of expression of aggregate coalescence depended on soil type. For the coarse-textured soil, repeated wetting and draining significantly increased bulk density, penetrometer resistance and tensile strength. For the fine-textured soil, penetrometer resistance and bulk density did not vary significantly with repeated wetting and draining; on the contrary, there was evidence in these swelling clay soils to suggest bulk density and penetrometer resistance decreased. However, there was a progressive increase in tensile strength as cycles of wetting and draining progressed. The expansive nature of the fine-textured soil appears to have masked the development of aggregate coalescence as measured by penetrometer resistance, but its expression was very clear in measurements of tensile strength despite the reduction in bulk density with successive wetting and draining. Field observations have indicated that aggregate coalescence is first expressed at the bottom of the seedbed and that it develops progressively upward to the soil surface during the growing season. This suggests that overburden pressures may enhance the onset of the phenomenon by increasing the degree of inter-aggregate contact. Soils containing large quantities of particulate organic matter were known to resist the onset of aggregate coalescence to some extent. An experiment was conducted to evaluate the effects of soil organic matter and overburden pressures, by placing brass cylinders of various weights (equivalent to static load pressures of 0, 0.49, 1.47 and 2.47 kPa) on the top of dry soil aggregates (0.5 – 2 mm diameter) having widely different soil organic carbon contents placed in steel rings 5 cm high and 5 cm i.d. With the weights in place, the aggregates were wetted to near-saturation for 24 h and then drained on ceramic pressure plates to a suction of 100 kPa for one week. Bulk density, penetrometer resistance and tensile strength were measured when the samples were removed from the pressure plates and they all increased significantly with increasing overburden pressure in the soil with low organic matter content, but not in the soil with high organic matter content. The amount of tillage used to prepare seedbeds influences the size distribution of soil aggregates produced – that is, more tillage produces finer seedbeds. The size distribution of soil aggregates affects the number of inter-aggregate contact points and this was thought to influence the degree of aggregate coalescence that develops in a seedbed. Previous work has shown that soil organic matter reduces aggregate coalescence and so an experiment was conducted to evaluate the effects of aggregate size and organic matter on the phenomenon. For soils with high and low organic matter contents, aggregate size fractions of < 0.5, 0.5 – 2, 2 – 4, and < 4 mm were packed into soil cores (as above) and wetted to near-saturation then drained to 100 kPa suction as described above. Penetrometer resistance and tensile strength were measured and found to increase directly with the amount of fine material present in the soil cores – being greater in the < 0.5 mm and < 4 mm fractions, and being less in the 0.5 – 2 mm and 2 – 4 mm fractions. In all cases, penetrometer resistance and tensile strength were lower in the samples containing more organic matter. The rate at which soil aggregates are wetted in a seedbed affects the degree of slaking and densification that occurs, and the extent to which aggregates are wetted influences the overall strength of a seedbed. Both wetting rate and the extent of wetting were believed to influence the onset of aggregate coalescence and were thought to be affected by soil organic matter and irrigation technique. An experiment was therefore designed to separate these effects so that improvements to management could be evaluated for their greatest efficacy – that is, to determine whether management should focus on improving irrigation technique or increasing soil organic matter content, or both. The rate of wetting was controlled by spraying (or not spraying) soil aggregates (0.5 – 2 mm diameter) with polyvinyl alcohol (PVA). Samples of coarse- and fine-textured soils were packed into steel rings (as above) and subjected to different application rates of water (1, 10 and 100 mm/h) using a dripper system controlled by a peristaltic pump. Samples were brought to either a near-saturated state or to a suction of 10 kPa for 24 h, and then drained on a pressure plate at a suction of 100 kPa for one week. Measurements of penetrometer resistance and tensile strength were then made as described above. As expected, penetrometer resistance was lower in samples treated with PVA before wetting (slower wetting rates) and in samples held at a greater suction (10 kPa) after initial wetting (greater inter-aggregate strength). The effects were more pronounced in the coarse-textured soil. In both coarse- and fine-textured soils, tensile strengths increased with increasing wetting rate (greatest for 100 mm/h) and extent of wetting (greater when held at near-saturated conditions). The rate of wetting was found to be somewhat more important for promoting aggregate coalescence than the extent of wetting. Because aggregate coalescence often occurs with little or no increase in bulk density, an explanation for the increase in penetrometer resistance and tensile strength is unlikely to be explained by a large increase in the number of inter-aggregate contacts. An increase in the strength of existing points of inter-aggregate contact was therefore considered in this work. For inter-aggregate bond strengths to increase, it was hypothesized that small increases in the amount of mechanically (or spontaneously) dispersed clay particles, and subsequent deposition at inter-aggregate contact points could increase aggregate coalescence as measured by penetrometer resistance and tensile strength. An experiment was devised to manipulate the amount of spontaneously dispersed clay in coarse- and fine-textured soils of high and low organic matter content. The degree of sodicity of each soil was manipulated by varying the exchangeable sodium percentage (ESP) of soil aggregates (0.5 – 2mm) above and below a nominal threshold value of 6. Dry aggregates were then packed into steel rings (as above) and subjected to wetting near saturation, then draining to a suction of 100 kPa for one week as described above. Measurements were then taken of penetrometer resistance and tensile strength, both of which were affected by ESP in different ways. In the coarse-textured soil, sodicity enhanced aggregate slaking and dispersion, which increased bulk density. While penetrometer resistance also increased, its effect on aggregate coalescence could not be separated from a simple effect of increased bulk density. Similarly, the effect of sodicity on aggregate coalescence in the fine-textured soil was confounded by the higher water contents produced by greater swelling, which produced lower-than-expected penetrometer resistance. Measurements of tensile strength were conducted on air-dry samples, and so the confounding effects of bulk density and water content were eliminated and it was found that tensile strength increased with sodicity in both coarse- and fine-textured soils. The presence of dispersed clay was therefore implicated in the development of aggregate coalescence in this work. Finally, a preliminary evaluation of how the early stages of aggregate coalescence might affect plant growth was attempted using tomatoes (Gross lisse) as a test plant. Seeds were planted in aggregates (0.5 – 4 mm) of a coarse- or fine-textured soil packed in steel rings. These were wetted at a rate of 1 mm/h to either near-saturation (for maximum coalescence) or to a suction of 10 kPa (for minimum coalescence) and held under these conditions for 24 h. All samples were then transferred to a ceramic pressure plate for drainage to 100 kPa suction for one week. Samples were then placed in a growth-cabinet held at 20C with controlled exposure to 14 h light/day. Germination of the seeds, plant height, and number and length of roots were observed. Germination of the seeds held at near-saturation in both coarse- and fine-textured soils was delayed by 24 h compared with seeds held at 10 kPa suction. Neither the number nor the length of tomato roots differed significantly between the different treatments and soils. In the coarse-textured soil, however, the total root length over a period of 14 days was somewhat greater in the uncoalesced samples than in the coalesced samples, but this difference was not statistically significant. These results suggest that aside from delaying germination, aggregate coalescence may not have a large effect on early growth of tomato plants. However, this is not to say that detrimental effects may not be manifest at later stages of plant growth, and this certainly needs to be evaluated, particularly because aggregate coalescence increase with repeated cycles of wetting and draining. In conclusion, the primary findings of the work undertaken in this thesis were: • Rapid wetting of soil aggregates to near-saturation enhanced the onset of soil aggregate coalescence as measured by (in some cases) penetrometer resistance at a soil water suction of 100 kPa, and (in most cases) tensile strength of soil cores in the air-dry state. The rate of wetting appeared to be more important in bringing on aggregate coalescence than how wet the soil eventually became during wetting. This means reducing the rate at which irrigation water is applied to soils may reduce the onset of aggregate coalescence more effectively than controlling the total amount of water applied – though both are important. The literature reports that aggregate coalescence occurs in the field over periods of up to several months, involving multiple wetting and draining cycles, but the work here demonstrated that this can occur over much shorter time periods depending on conditions imposed. • Aggregate coalescence occurred in coarse-textured soils regardless of whether the bulk density increased during wetting and draining. In finer-textured soils, the response to wetting conditions varied and was complicated by changes in bulk density and water content due to swelling. • Small overburden pressures enhanced the onset of aggregate coalescence, but these effects were diminished in the presence of high soil organic matter contents. • Finer aggregate size distributions (which are often produced in the field by excessive tillage during seedbed preparation) invariably led to greater aggregate coalescence than coarser aggregate size distributions. The effects of aggregate size were mitigated to some extent by higher contents of soil organic matter. • Sodicity enhanced aggregate coalescence as measured by tensile strength, but when penetrometer resistance was measured in the moist state, the effects were masked to some extent by higher water contents generated by swelling and dispersion. This work suggests that tensile strength (in the air dry state) may be a more effective measure of aggregate coalescence than penetrometer resistance. • Early plant response to aggregate coalescence was not large, but the response may become magnified during later stages of growth. / http://proxy.library.adelaide.edu.au/login?url= http://library.adelaide.edu.au/cgi-bin/Pwebrecon.cgi?BBID=1297583 / Thesis (Ph.D.) -- School of Earth and Environmental Sciences, 2007

Soil is extremely important for providing food, biomass and raw materials, water and nutrient storage; supporting biodiversity and providing foundations for man-made structures. However, its health is threatened by human activities, which can greatly affect the potential of soils to fulfil their functions and, consequently, result in environmental, economic and social damage. These issues require the characterisation of the impact and spatial extent of the problems. This can be achieved through the creation of detailed and comprehensive soil maps that describe both the spatial and vertical variability of key soil properties. Detailed three-dimensional (3D) digital soil maps can be readily used and embedded into environmental models. Three-dimensional soil mapping is not a new concept. However, only with the recent development of more powerful computers has it become feasible to undertake such data processing. Common techniques to estimate soil properties in the three-dimensional space include geostatistical interpolation, or a combination of depth functions and geostatistics. However, these two methods are both partially flawed. Geostatistical interpolation and kriging in particular, estimate soil properties in unsampled locations using a weighted average of the nearby observations. In order to produce the best possible estimate, this form of interpolation minimises the variance of each weighted average, thus decreasing the standard deviation of the estimates, compared to the soil observations. This appears as a smoothing effect on the data and, as a consequence, kriging interpolation is not reliable when the dataset is not sampled with a sampling designs optimised for geostatistics. Depth function approaches, as they are generally applied in literature, implement a spline regression of the soil profile data that aims to better describe the changes of the soil properties with depth. Subsequently, the spline is resampled at determined depths and, for each of these depths, a bi-dimensional (2D) geostatistical interpolation is performed. Consequently, the 3D soil model is a combination of a series of bi-dimensional slices. This approach can effectively decrease or eliminate any smoothing issues, but the way in which the model is created, by combining several 2D horizontal slices, can potentially lead to erroneous estimations. The fact that the geostatistical interpolation is performed in 2D implies that an unsampled location is estimated only by considering values at the same depth, thus excluding the vertical variability from the mapping, and potentially undermining the accuracy of the method. For these reasons, the literature review identified a clear need for developing, a new method for accurately estimating soil properties in 3D – the target of this research, The method studied in this thesis explores the concept of soil specific depth functions, which are simple mathematical equations, chosen for their ability to describe the general profile pattern of a soil dataset. This way, fitting the depth function to a particular sample becomes a diagnostic tool. If the pattern shown in a particular soil profile is dissimilar to the average pattern described by the depth function, it means that in that region there are localised changes in the soil profiles, and these can be identified from the goodness of fit of the function. This way, areas where soil properties have a homogeneous profile pattern can be easily identified and the depth function can be changed accordingly. The application of this new mapping technique is based on the geostatistical interpolation of the depth function coefficients across the study area. Subsequently, the equation is solved for each interpolated location to create a 3D lattice of soil properties estimations. For this way of mapping, this new methodology was denoted as top-down mapping method. The methodology was assessed through three case studies, where the top-down mapping method was developed, tested, and validated. Three datasets of diverse soil properties and at different spatial extents were selected. The results were validated primarily using cross-validation and, when possible, by comparing the estimates with independently sampled datasets (independent validation). In addition, the results were compared with estimates obtained using established literature methods, such as 3D kriging interpolation and the spline approach, in order to define some basic rule of application. The results indicate that the top-down mapping method can be used in circumstances where the soil profiles present a pattern that can be described by a function with maximum three coefficients. If this condition is met, as it was with key soil properties during the research, the top-down mapping method can be used for obtaining reliable estimates at different spatial extents.

The use of fossil derived products and the environmental and economic problems associated with them have made a shift to abundant renewable resources such as forest biomass more attractive. However before forest biomass can be used as a resource, its properties must be known. This study determined the physical properties of heterogeneous biomass residues produced during harvesting on two operational forest sites within the Great Lakes-St Lawrence forest of south-eastern Ontario. Properties measured were moisture content, size distribution, bulk density, and wood-to-bark ratio; also thermo-chemical properties including elemental composition, thermal reactivity and energy content were measured. The effects of forest site and harvest type, storage and position in storage pile, on the properties of biomass were also investigated. Results of the study showed that the various heterogeneous forest harvest residues differed more physically than thermo-chemically for the different variables, and this affected biomass procurement more than the potential utilization options.

The phenomenon called soil aggregate coalescence occurs at contact-points between aggregates and causes soil strength to increase to values that can inhibit plant root exploration and thus potential yield. During natural wetting and drying, soil aggregates appear to ‘weld’ together with little or no increase in dry bulk density. The precise reasons for this phenomenon are not understood, but it has been found to occur even in soils comprised entirely of water stable aggregates. Soil aggregate coalescence has not been widely observed and reported in soil science and yet may pose a significant risk for crops preventing them from achieving their genetic and environmental yield potentials. This project used soil penetrometer resistance and an indirect tensile-strength test to measure the early stages of aggregate coalescence and to evaluate their effects on the early growth of tomato plants. The early stages of aggregate coalescence were thought to be affected by a number of factors including: the matric suction of water during application and subsequent drainage, the overburden pressure on moist soil in the root zone, the initial size of soil aggregates prior to wetting, and the degree of sodicity of the soil aggregates. Seven mainexperiments were conducted to evaluate these factors. The matric suction during wetting of a seedbed affects the degree of aggregate slaking that occurs, and the strength of the wetted aggregates. The matric suction during draining affects the magnitude of ‘effective stresses’ that operate to retain soil structural integrity as the soil drains and dries out. An experiment was conducted to evaluate the influence of matric suction (within a range of suctions experienced in the field) on aggregate coalescence using soils of two different textures. Sieved aggregates (0.5 to 2 mm diameter) from a coarse-textured and two fine-textured (swelling) soils were packed into cylindrical rings (4.77 cm i.d., 5 cm high) and subjected to different suctions on wetting (near-saturation, and 1 kPa), and on draining (10 kPa on sintered-glass funnels, and 100 kPa on ceramic pressure plates). After one-week of drainage, penetrometer resistance was measured as a function of depth to approximately 45 mm (penetrometer had a recessedshaft, cone diameter = 2 mm, advanced at a rate of 0.3 mm/min). Tensile strength of other core-samples was measured after air-drying using an indirect “Brazilian” crushing test. For the coarse-textured soil, penetrometer resistance was significantly greater for samples wet to near-saturation, despite there being no significant increase in dry bulk density; this was not the case for the finer-textured soils, and it was difficult to distinguish the effects of variable bulk density upon drying from those of the imposed wetting treatments. In both coarse- and fine-textured soils, the tensile strength was significantly greater for samples wet to near-saturation. Thus wetting- and draining-suctions were both found to influence the degree of soil aggregate coalescence as measured by penetrometer resistance and tensile strength. Aggregate coalescence in irrigated crops is known to develop as the growing season progresses. It was therefore thought to be linked to the repeated occurrence of matric suctions that enhance the phenomenon during cycles of wetting and draining. An experiment was conducted to determine the extent of aggregate coalescence in a coarsetextured and two fine-textured (swelling clay) soils during 8 successive cycles of wetting and draining. Sieved aggregates (0.5 to 2 mm diameter) from each soil were packed into cylindrical rings (4.77 cm i.d., 5 cm high) and wetted to near saturation for 24 h. They were then drained on ceramic pressure plates to a suction of 100 kPa for one week, after which penetrometer resistance and tensile strength were measured as described above. The degree of expression of aggregate coalescence depended on soil type. For the coarse-textured soil, repeated wetting and draining significantly increased bulk density, penetrometer resistance and tensile strength. For the fine-textured soil, penetrometer resistance and bulk density did not vary significantly with repeated wetting and draining; on the contrary, there was evidence in these swelling clay soils to suggest bulk density and penetrometer resistance decreased. However, there was a progressive increase in tensile strength as cycles of wetting and draining progressed. The expansive nature of the fine-textured soil appears to have masked the development of aggregate coalescence as measured by penetrometer resistance, but its expression was very clear in measurements of tensile strength despite the reduction in bulk density with successive wetting and draining. Field observations have indicated that aggregate coalescence is first expressed at the bottom of the seedbed and that it develops progressively upward to the soil surface during the growing season. This suggests that overburden pressures may enhance the onset of the phenomenon by increasing the degree of inter-aggregate contact. Soils containing large quantities of particulate organic matter were known to resist the onset of aggregate coalescence to some extent. An experiment was conducted to evaluate the effects of soil organic matter and overburden pressures, by placing brass cylinders of various weights (equivalent to static load pressures of 0, 0.49, 1.47 and 2.47 kPa) on the top of dry soil aggregates (0.5 – 2 mm diameter) having widely different soil organic carbon contents placed in steel rings 5 cm high and 5 cm i.d. With the weights in place, the aggregates were wetted to near-saturation for 24 h and then drained on ceramic pressure plates to a suction of 100 kPa for one week. Bulk density, penetrometer resistance and tensile strength were measured when the samples were removed from the pressure plates and they all increased significantly with increasing overburden pressure in the soil with low organic matter content, but not in the soil with high organic matter content. The amount of tillage used to prepare seedbeds influences the size distribution of soil aggregates produced – that is, more tillage produces finer seedbeds. The size distribution of soil aggregates affects the number of inter-aggregate contact points and this was thought to influence the degree of aggregate coalescence that develops in a seedbed. Previous work has shown that soil organic matter reduces aggregate coalescence and so an experiment was conducted to evaluate the effects of aggregate size and organic matter on the phenomenon. For soils with high and low organic matter contents, aggregate size fractions of < 0.5, 0.5 – 2, 2 – 4, and < 4 mm were packed into soil cores (as above) and wetted to near-saturation then drained to 100 kPa suction as described above. Penetrometer resistance and tensile strength were measured and found to increase directly with the amount of fine material present in the soil cores – being greater in the < 0.5 mm and < 4 mm fractions, and being less in the 0.5 – 2 mm and 2 – 4 mm fractions. In all cases, penetrometer resistance and tensile strength were lower in the samples containing more organic matter. The rate at which soil aggregates are wetted in a seedbed affects the degree of slaking and densification that occurs, and the extent to which aggregates are wetted influences the overall strength of a seedbed. Both wetting rate and the extent of wetting were believed to influence the onset of aggregate coalescence and were thought to be affected by soil organic matter and irrigation technique. An experiment was therefore designed to separate these effects so that improvements to management could be evaluated for their greatest efficacy – that is, to determine whether management should focus on improving irrigation technique or increasing soil organic matter content, or both. The rate of wetting was controlled by spraying (or not spraying) soil aggregates (0.5 – 2 mm diameter) with polyvinyl alcohol (PVA). Samples of coarse- and fine-textured soils were packed into steel rings (as above) and subjected to different application rates of water (1, 10 and 100 mm/h) using a dripper system controlled by a peristaltic pump. Samples were brought to either a near-saturated state or to a suction of 10 kPa for 24 h, and then drained on a pressure plate at a suction of 100 kPa for one week. Measurements of penetrometer resistance and tensile strength were then made as described above. As expected, penetrometer resistance was lower in samples treated with PVA before wetting (slower wetting rates) and in samples held at a greater suction (10 kPa) after initial wetting (greater inter-aggregate strength). The effects were more pronounced in the coarse-textured soil. In both coarse- and fine-textured soils, tensile strengths increased with increasing wetting rate (greatest for 100 mm/h) and extent of wetting (greater when held at near-saturated conditions). The rate of wetting was found to be somewhat more important for promoting aggregate coalescence than the extent of wetting. Because aggregate coalescence often occurs with little or no increase in bulk density, an explanation for the increase in penetrometer resistance and tensile strength is unlikely to be explained by a large increase in the number of inter-aggregate contacts. An increase in the strength of existing points of inter-aggregate contact was therefore considered in this work. For inter-aggregate bond strengths to increase, it was hypothesized that small increases in the amount of mechanically (or spontaneously) dispersed clay particles, and subsequent deposition at inter-aggregate contact points could increase aggregate coalescence as measured by penetrometer resistance and tensile strength. An experiment was devised to manipulate the amount of spontaneously dispersed clay in coarse- and fine-textured soils of high and low organic matter content. The degree of sodicity of each soil was manipulated by varying the exchangeable sodium percentage (ESP) of soil aggregates (0.5 – 2mm) above and below a nominal threshold value of 6. Dry aggregates were then packed into steel rings (as above) and subjected to wetting near saturation, then draining to a suction of 100 kPa for one week as described above. Measurements were then taken of penetrometer resistance and tensile strength, both of which were affected by ESP in different ways. In the coarse-textured soil, sodicity enhanced aggregate slaking and dispersion, which increased bulk density. While penetrometer resistance also increased, its effect on aggregate coalescence could not be separated from a simple effect of increased bulk density. Similarly, the effect of sodicity on aggregate coalescence in the fine-textured soil was confounded by the higher water contents produced by greater swelling, which produced lower-than-expected penetrometer resistance. Measurements of tensile strength were conducted on air-dry samples, and so the confounding effects of bulk density and water content were eliminated and it was found that tensile strength increased with sodicity in both coarse- and fine-textured soils. The presence of dispersed clay was therefore implicated in the development of aggregate coalescence in this work. Finally, a preliminary evaluation of how the early stages of aggregate coalescence might affect plant growth was attempted using tomatoes (Gross lisse) as a test plant. Seeds were planted in aggregates (0.5 – 4 mm) of a coarse- or fine-textured soil packed in steel rings. These were wetted at a rate of 1 mm/h to either near-saturation (for maximum coalescence) or to a suction of 10 kPa (for minimum coalescence) and held under these conditions for 24 h. All samples were then transferred to a ceramic pressure plate for drainage to 100 kPa suction for one week. Samples were then placed in a growth-cabinet held at 20C with controlled exposure to 14 h light/day. Germination of the seeds, plant height, and number and length of roots were observed. Germination of the seeds held at near-saturation in both coarse- and fine-textured soils was delayed by 24 h compared with seeds held at 10 kPa suction. Neither the number nor the length of tomato roots differed significantly between the different treatments and soils. In the coarse-textured soil, however, the total root length over a period of 14 days was somewhat greater in the uncoalesced samples than in the coalesced samples, but this difference was not statistically significant. These results suggest that aside from delaying germination, aggregate coalescence may not have a large effect on early growth of tomato plants. However, this is not to say that detrimental effects may not be manifest at later stages of plant growth, and this certainly needs to be evaluated, particularly because aggregate coalescence increase with repeated cycles of wetting and draining. In conclusion, the primary findings of the work undertaken in this thesis were: • Rapid wetting of soil aggregates to near-saturation enhanced the onset of soil aggregate coalescence as measured by (in some cases) penetrometer resistance at a soil water suction of 100 kPa, and (in most cases) tensile strength of soil cores in the air-dry state. The rate of wetting appeared to be more important in bringing on aggregate coalescence than how wet the soil eventually became during wetting. This means reducing the rate at which irrigation water is applied to soils may reduce the onset of aggregate coalescence more effectively than controlling the total amount of water applied – though both are important. The literature reports that aggregate coalescence occurs in the field over periods of up to several months, involving multiple wetting and draining cycles, but the work here demonstrated that this can occur over much shorter time periods depending on conditions imposed. • Aggregate coalescence occurred in coarse-textured soils regardless of whether the bulk density increased during wetting and draining. In finer-textured soils, the response to wetting conditions varied and was complicated by changes in bulk density and water content due to swelling. • Small overburden pressures enhanced the onset of aggregate coalescence, but these effects were diminished in the presence of high soil organic matter contents. • Finer aggregate size distributions (which are often produced in the field by excessive tillage during seedbed preparation) invariably led to greater aggregate coalescence than coarser aggregate size distributions. The effects of aggregate size were mitigated to some extent by higher contents of soil organic matter. • Sodicity enhanced aggregate coalescence as measured by tensile strength, but when penetrometer resistance was measured in the moist state, the effects were masked to some extent by higher water contents generated by swelling and dispersion. This work suggests that tensile strength (in the air dry state) may be a more effective measure of aggregate coalescence than penetrometer resistance. • Early plant response to aggregate coalescence was not large, but the response may become magnified during later stages of growth. / http://proxy.library.adelaide.edu.au/login?url= http://library.adelaide.edu.au/cgi-bin/Pwebrecon.cgi?BBID=1297583 / Thesis (Ph.D.) -- School of Earth and Environmental Sciences, 2007

The phenomenon called soil aggregate coalescence occurs at contact-points between aggregates and causes soil strength to increase to values that can inhibit plant root exploration and thus potential yield. During natural wetting and drying, soil aggregates appear to ‘weld’ together with little or no increase in dry bulk density. The precise reasons for this phenomenon are not understood, but it has been found to occur even in soils comprised entirely of water stable aggregates. Soil aggregate coalescence has not been widely observed and reported in soil science and yet may pose a significant risk for crops preventing them from achieving their genetic and environmental yield potentials. This project used soil penetrometer resistance and an indirect tensile-strength test to measure the early stages of aggregate coalescence and to evaluate their effects on the early growth of tomato plants. The early stages of aggregate coalescence were thought to be affected by a number of factors including: the matric suction of water during application and subsequent drainage, the overburden pressure on moist soil in the root zone, the initial size of soil aggregates prior to wetting, and the degree of sodicity of the soil aggregates. Seven mainexperiments were conducted to evaluate these factors. The matric suction during wetting of a seedbed affects the degree of aggregate slaking that occurs, and the strength of the wetted aggregates. The matric suction during draining affects the magnitude of ‘effective stresses’ that operate to retain soil structural integrity as the soil drains and dries out. An experiment was conducted to evaluate the influence of matric suction (within a range of suctions experienced in the field) on aggregate coalescence using soils of two different textures. Sieved aggregates (0.5 to 2 mm diameter) from a coarse-textured and two fine-textured (swelling) soils were packed into cylindrical rings (4.77 cm i.d., 5 cm high) and subjected to different suctions on wetting (near-saturation, and 1 kPa), and on draining (10 kPa on sintered-glass funnels, and 100 kPa on ceramic pressure plates). After one-week of drainage, penetrometer resistance was measured as a function of depth to approximately 45 mm (penetrometer had a recessedshaft, cone diameter = 2 mm, advanced at a rate of 0.3 mm/min). Tensile strength of other core-samples was measured after air-drying using an indirect “Brazilian” crushing test. For the coarse-textured soil, penetrometer resistance was significantly greater for samples wet to near-saturation, despite there being no significant increase in dry bulk density; this was not the case for the finer-textured soils, and it was difficult to distinguish the effects of variable bulk density upon drying from those of the imposed wetting treatments. In both coarse- and fine-textured soils, the tensile strength was significantly greater for samples wet to near-saturation. Thus wetting- and draining-suctions were both found to influence the degree of soil aggregate coalescence as measured by penetrometer resistance and tensile strength. Aggregate coalescence in irrigated crops is known to develop as the growing season progresses. It was therefore thought to be linked to the repeated occurrence of matric suctions that enhance the phenomenon during cycles of wetting and draining. An experiment was conducted to determine the extent of aggregate coalescence in a coarsetextured and two fine-textured (swelling clay) soils during 8 successive cycles of wetting and draining. Sieved aggregates (0.5 to 2 mm diameter) from each soil were packed into cylindrical rings (4.77 cm i.d., 5 cm high) and wetted to near saturation for 24 h. They were then drained on ceramic pressure plates to a suction of 100 kPa for one week, after which penetrometer resistance and tensile strength were measured as described above. The degree of expression of aggregate coalescence depended on soil type. For the coarse-textured soil, repeated wetting and draining significantly increased bulk density, penetrometer resistance and tensile strength. For the fine-textured soil, penetrometer resistance and bulk density did not vary significantly with repeated wetting and draining; on the contrary, there was evidence in these swelling clay soils to suggest bulk density and penetrometer resistance decreased. However, there was a progressive increase in tensile strength as cycles of wetting and draining progressed. The expansive nature of the fine-textured soil appears to have masked the development of aggregate coalescence as measured by penetrometer resistance, but its expression was very clear in measurements of tensile strength despite the reduction in bulk density with successive wetting and draining. Field observations have indicated that aggregate coalescence is first expressed at the bottom of the seedbed and that it develops progressively upward to the soil surface during the growing season. This suggests that overburden pressures may enhance the onset of the phenomenon by increasing the degree of inter-aggregate contact. Soils containing large quantities of particulate organic matter were known to resist the onset of aggregate coalescence to some extent. An experiment was conducted to evaluate the effects of soil organic matter and overburden pressures, by placing brass cylinders of various weights (equivalent to static load pressures of 0, 0.49, 1.47 and 2.47 kPa) on the top of dry soil aggregates (0.5 – 2 mm diameter) having widely different soil organic carbon contents placed in steel rings 5 cm high and 5 cm i.d. With the weights in place, the aggregates were wetted to near-saturation for 24 h and then drained on ceramic pressure plates to a suction of 100 kPa for one week. Bulk density, penetrometer resistance and tensile strength were measured when the samples were removed from the pressure plates and they all increased significantly with increasing overburden pressure in the soil with low organic matter content, but not in the soil with high organic matter content. The amount of tillage used to prepare seedbeds influences the size distribution of soil aggregates produced – that is, more tillage produces finer seedbeds. The size distribution of soil aggregates affects the number of inter-aggregate contact points and this was thought to influence the degree of aggregate coalescence that develops in a seedbed. Previous work has shown that soil organic matter reduces aggregate coalescence and so an experiment was conducted to evaluate the effects of aggregate size and organic matter on the phenomenon. For soils with high and low organic matter contents, aggregate size fractions of < 0.5, 0.5 – 2, 2 – 4, and < 4 mm were packed into soil cores (as above) and wetted to near-saturation then drained to 100 kPa suction as described above. Penetrometer resistance and tensile strength were measured and found to increase directly with the amount of fine material present in the soil cores – being greater in the < 0.5 mm and < 4 mm fractions, and being less in the 0.5 – 2 mm and 2 – 4 mm fractions. In all cases, penetrometer resistance and tensile strength were lower in the samples containing more organic matter. The rate at which soil aggregates are wetted in a seedbed affects the degree of slaking and densification that occurs, and the extent to which aggregates are wetted influences the overall strength of a seedbed. Both wetting rate and the extent of wetting were believed to influence the onset of aggregate coalescence and were thought to be affected by soil organic matter and irrigation technique. An experiment was therefore designed to separate these effects so that improvements to management could be evaluated for their greatest efficacy – that is, to determine whether management should focus on improving irrigation technique or increasing soil organic matter content, or both. The rate of wetting was controlled by spraying (or not spraying) soil aggregates (0.5 – 2 mm diameter) with polyvinyl alcohol (PVA). Samples of coarse- and fine-textured soils were packed into steel rings (as above) and subjected to different application rates of water (1, 10 and 100 mm/h) using a dripper system controlled by a peristaltic pump. Samples were brought to either a near-saturated state or to a suction of 10 kPa for 24 h, and then drained on a pressure plate at a suction of 100 kPa for one week. Measurements of penetrometer resistance and tensile strength were then made as described above. As expected, penetrometer resistance was lower in samples treated with PVA before wetting (slower wetting rates) and in samples held at a greater suction (10 kPa) after initial wetting (greater inter-aggregate strength). The effects were more pronounced in the coarse-textured soil. In both coarse- and fine-textured soils, tensile strengths increased with increasing wetting rate (greatest for 100 mm/h) and extent of wetting (greater when held at near-saturated conditions). The rate of wetting was found to be somewhat more important for promoting aggregate coalescence than the extent of wetting. Because aggregate coalescence often occurs with little or no increase in bulk density, an explanation for the increase in penetrometer resistance and tensile strength is unlikely to be explained by a large increase in the number of inter-aggregate contacts. An increase in the strength of existing points of inter-aggregate contact was therefore considered in this work. For inter-aggregate bond strengths to increase, it was hypothesized that small increases in the amount of mechanically (or spontaneously) dispersed clay particles, and subsequent deposition at inter-aggregate contact points could increase aggregate coalescence as measured by penetrometer resistance and tensile strength. An experiment was devised to manipulate the amount of spontaneously dispersed clay in coarse- and fine-textured soils of high and low organic matter content. The degree of sodicity of each soil was manipulated by varying the exchangeable sodium percentage (ESP) of soil aggregates (0.5 – 2mm) above and below a nominal threshold value of 6. Dry aggregates were then packed into steel rings (as above) and subjected to wetting near saturation, then draining to a suction of 100 kPa for one week as described above. Measurements were then taken of penetrometer resistance and tensile strength, both of which were affected by ESP in different ways. In the coarse-textured soil, sodicity enhanced aggregate slaking and dispersion, which increased bulk density. While penetrometer resistance also increased, its effect on aggregate coalescence could not be separated from a simple effect of increased bulk density. Similarly, the effect of sodicity on aggregate coalescence in the fine-textured soil was confounded by the higher water contents produced by greater swelling, which produced lower-than-expected penetrometer resistance. Measurements of tensile strength were conducted on air-dry samples, and so the confounding effects of bulk density and water content were eliminated and it was found that tensile strength increased with sodicity in both coarse- and fine-textured soils. The presence of dispersed clay was therefore implicated in the development of aggregate coalescence in this work. Finally, a preliminary evaluation of how the early stages of aggregate coalescence might affect plant growth was attempted using tomatoes (Gross lisse) as a test plant. Seeds were planted in aggregates (0.5 – 4 mm) of a coarse- or fine-textured soil packed in steel rings. These were wetted at a rate of 1 mm/h to either near-saturation (for maximum coalescence) or to a suction of 10 kPa (for minimum coalescence) and held under these conditions for 24 h. All samples were then transferred to a ceramic pressure plate for drainage to 100 kPa suction for one week. Samples were then placed in a growth-cabinet held at 20C with controlled exposure to 14 h light/day. Germination of the seeds, plant height, and number and length of roots were observed. Germination of the seeds held at near-saturation in both coarse- and fine-textured soils was delayed by 24 h compared with seeds held at 10 kPa suction. Neither the number nor the length of tomato roots differed significantly between the different treatments and soils. In the coarse-textured soil, however, the total root length over a period of 14 days was somewhat greater in the uncoalesced samples than in the coalesced samples, but this difference was not statistically significant. These results suggest that aside from delaying germination, aggregate coalescence may not have a large effect on early growth of tomato plants. However, this is not to say that detrimental effects may not be manifest at later stages of plant growth, and this certainly needs to be evaluated, particularly because aggregate coalescence increase with repeated cycles of wetting and draining. In conclusion, the primary findings of the work undertaken in this thesis were: • Rapid wetting of soil aggregates to near-saturation enhanced the onset of soil aggregate coalescence as measured by (in some cases) penetrometer resistance at a soil water suction of 100 kPa, and (in most cases) tensile strength of soil cores in the air-dry state. The rate of wetting appeared to be more important in bringing on aggregate coalescence than how wet the soil eventually became during wetting. This means reducing the rate at which irrigation water is applied to soils may reduce the onset of aggregate coalescence more effectively than controlling the total amount of water applied – though both are important. The literature reports that aggregate coalescence occurs in the field over periods of up to several months, involving multiple wetting and draining cycles, but the work here demonstrated that this can occur over much shorter time periods depending on conditions imposed. • Aggregate coalescence occurred in coarse-textured soils regardless of whether the bulk density increased during wetting and draining. In finer-textured soils, the response to wetting conditions varied and was complicated by changes in bulk density and water content due to swelling. • Small overburden pressures enhanced the onset of aggregate coalescence, but these effects were diminished in the presence of high soil organic matter contents. • Finer aggregate size distributions (which are often produced in the field by excessive tillage during seedbed preparation) invariably led to greater aggregate coalescence than coarser aggregate size distributions. The effects of aggregate size were mitigated to some extent by higher contents of soil organic matter. • Sodicity enhanced aggregate coalescence as measured by tensile strength, but when penetrometer resistance was measured in the moist state, the effects were masked to some extent by higher water contents generated by swelling and dispersion. This work suggests that tensile strength (in the air dry state) may be a more effective measure of aggregate coalescence than penetrometer resistance. • Early plant response to aggregate coalescence was not large, but the response may become magnified during later stages of growth. / http://proxy.library.adelaide.edu.au/login?url= http://library.adelaide.edu.au/cgi-bin/Pwebrecon.cgi?BBID=1297583 / Thesis (Ph.D.) -- School of Earth and Environmental Sciences, 2007

The phenomenon called soil aggregate coalescence occurs at contact-points between aggregates and causes soil strength to increase to values that can inhibit plant root exploration and thus potential yield. During natural wetting and drying, soil aggregates appear to ‘weld’ together with little or no increase in dry bulk density. The precise reasons for this phenomenon are not understood, but it has been found to occur even in soils comprised entirely of water stable aggregates. Soil aggregate coalescence has not been widely observed and reported in soil science and yet may pose a significant risk for crops preventing them from achieving their genetic and environmental yield potentials. This project used soil penetrometer resistance and an indirect tensile-strength test to measure the early stages of aggregate coalescence and to evaluate their effects on the early growth of tomato plants. The early stages of aggregate coalescence were thought to be affected by a number of factors including: the matric suction of water during application and subsequent drainage, the overburden pressure on moist soil in the root zone, the initial size of soil aggregates prior to wetting, and the degree of sodicity of the soil aggregates. Seven mainexperiments were conducted to evaluate these factors. The matric suction during wetting of a seedbed affects the degree of aggregate slaking that occurs, and the strength of the wetted aggregates. The matric suction during draining affects the magnitude of ‘effective stresses’ that operate to retain soil structural integrity as the soil drains and dries out. An experiment was conducted to evaluate the influence of matric suction (within a range of suctions experienced in the field) on aggregate coalescence using soils of two different textures. Sieved aggregates (0.5 to 2 mm diameter) from a coarse-textured and two fine-textured (swelling) soils were packed into cylindrical rings (4.77 cm i.d., 5 cm high) and subjected to different suctions on wetting (near-saturation, and 1 kPa), and on draining (10 kPa on sintered-glass funnels, and 100 kPa on ceramic pressure plates). After one-week of drainage, penetrometer resistance was measured as a function of depth to approximately 45 mm (penetrometer had a recessedshaft, cone diameter = 2 mm, advanced at a rate of 0.3 mm/min). Tensile strength of other core-samples was measured after air-drying using an indirect “Brazilian” crushing test. For the coarse-textured soil, penetrometer resistance was significantly greater for samples wet to near-saturation, despite there being no significant increase in dry bulk density; this was not the case for the finer-textured soils, and it was difficult to distinguish the effects of variable bulk density upon drying from those of the imposed wetting treatments. In both coarse- and fine-textured soils, the tensile strength was significantly greater for samples wet to near-saturation. Thus wetting- and draining-suctions were both found to influence the degree of soil aggregate coalescence as measured by penetrometer resistance and tensile strength. Aggregate coalescence in irrigated crops is known to develop as the growing season progresses. It was therefore thought to be linked to the repeated occurrence of matric suctions that enhance the phenomenon during cycles of wetting and draining. An experiment was conducted to determine the extent of aggregate coalescence in a coarsetextured and two fine-textured (swelling clay) soils during 8 successive cycles of wetting and draining. Sieved aggregates (0.5 to 2 mm diameter) from each soil were packed into cylindrical rings (4.77 cm i.d., 5 cm high) and wetted to near saturation for 24 h. They were then drained on ceramic pressure plates to a suction of 100 kPa for one week, after which penetrometer resistance and tensile strength were measured as described above. The degree of expression of aggregate coalescence depended on soil type. For the coarse-textured soil, repeated wetting and draining significantly increased bulk density, penetrometer resistance and tensile strength. For the fine-textured soil, penetrometer resistance and bulk density did not vary significantly with repeated wetting and draining; on the contrary, there was evidence in these swelling clay soils to suggest bulk density and penetrometer resistance decreased. However, there was a progressive increase in tensile strength as cycles of wetting and draining progressed. The expansive nature of the fine-textured soil appears to have masked the development of aggregate coalescence as measured by penetrometer resistance, but its expression was very clear in measurements of tensile strength despite the reduction in bulk density with successive wetting and draining. Field observations have indicated that aggregate coalescence is first expressed at the bottom of the seedbed and that it develops progressively upward to the soil surface during the growing season. This suggests that overburden pressures may enhance the onset of the phenomenon by increasing the degree of inter-aggregate contact. Soils containing large quantities of particulate organic matter were known to resist the onset of aggregate coalescence to some extent. An experiment was conducted to evaluate the effects of soil organic matter and overburden pressures, by placing brass cylinders of various weights (equivalent to static load pressures of 0, 0.49, 1.47 and 2.47 kPa) on the top of dry soil aggregates (0.5 – 2 mm diameter) having widely different soil organic carbon contents placed in steel rings 5 cm high and 5 cm i.d. With the weights in place, the aggregates were wetted to near-saturation for 24 h and then drained on ceramic pressure plates to a suction of 100 kPa for one week. Bulk density, penetrometer resistance and tensile strength were measured when the samples were removed from the pressure plates and they all increased significantly with increasing overburden pressure in the soil with low organic matter content, but not in the soil with high organic matter content. The amount of tillage used to prepare seedbeds influences the size distribution of soil aggregates produced – that is, more tillage produces finer seedbeds. The size distribution of soil aggregates affects the number of inter-aggregate contact points and this was thought to influence the degree of aggregate coalescence that develops in a seedbed. Previous work has shown that soil organic matter reduces aggregate coalescence and so an experiment was conducted to evaluate the effects of aggregate size and organic matter on the phenomenon. For soils with high and low organic matter contents, aggregate size fractions of < 0.5, 0.5 – 2, 2 – 4, and < 4 mm were packed into soil cores (as above) and wetted to near-saturation then drained to 100 kPa suction as described above. Penetrometer resistance and tensile strength were measured and found to increase directly with the amount of fine material present in the soil cores – being greater in the < 0.5 mm and < 4 mm fractions, and being less in the 0.5 – 2 mm and 2 – 4 mm fractions. In all cases, penetrometer resistance and tensile strength were lower in the samples containing more organic matter. The rate at which soil aggregates are wetted in a seedbed affects the degree of slaking and densification that occurs, and the extent to which aggregates are wetted influences the overall strength of a seedbed. Both wetting rate and the extent of wetting were believed to influence the onset of aggregate coalescence and were thought to be affected by soil organic matter and irrigation technique. An experiment was therefore designed to separate these effects so that improvements to management could be evaluated for their greatest efficacy – that is, to determine whether management should focus on improving irrigation technique or increasing soil organic matter content, or both. The rate of wetting was controlled by spraying (or not spraying) soil aggregates (0.5 – 2 mm diameter) with polyvinyl alcohol (PVA). Samples of coarse- and fine-textured soils were packed into steel rings (as above) and subjected to different application rates of water (1, 10 and 100 mm/h) using a dripper system controlled by a peristaltic pump. Samples were brought to either a near-saturated state or to a suction of 10 kPa for 24 h, and then drained on a pressure plate at a suction of 100 kPa for one week. Measurements of penetrometer resistance and tensile strength were then made as described above. As expected, penetrometer resistance was lower in samples treated with PVA before wetting (slower wetting rates) and in samples held at a greater suction (10 kPa) after initial wetting (greater inter-aggregate strength). The effects were more pronounced in the coarse-textured soil. In both coarse- and fine-textured soils, tensile strengths increased with increasing wetting rate (greatest for 100 mm/h) and extent of wetting (greater when held at near-saturated conditions). The rate of wetting was found to be somewhat more important for promoting aggregate coalescence than the extent of wetting. Because aggregate coalescence often occurs with little or no increase in bulk density, an explanation for the increase in penetrometer resistance and tensile strength is unlikely to be explained by a large increase in the number of inter-aggregate contacts. An increase in the strength of existing points of inter-aggregate contact was therefore considered in this work. For inter-aggregate bond strengths to increase, it was hypothesized that small increases in the amount of mechanically (or spontaneously) dispersed clay particles, and subsequent deposition at inter-aggregate contact points could increase aggregate coalescence as measured by penetrometer resistance and tensile strength. An experiment was devised to manipulate the amount of spontaneously dispersed clay in coarse- and fine-textured soils of high and low organic matter content. The degree of sodicity of each soil was manipulated by varying the exchangeable sodium percentage (ESP) of soil aggregates (0.5 – 2mm) above and below a nominal threshold value of 6. Dry aggregates were then packed into steel rings (as above) and subjected to wetting near saturation, then draining to a suction of 100 kPa for one week as described above. Measurements were then taken of penetrometer resistance and tensile strength, both of which were affected by ESP in different ways. In the coarse-textured soil, sodicity enhanced aggregate slaking and dispersion, which increased bulk density. While penetrometer resistance also increased, its effect on aggregate coalescence could not be separated from a simple effect of increased bulk density. Similarly, the effect of sodicity on aggregate coalescence in the fine-textured soil was confounded by the higher water contents produced by greater swelling, which produced lower-than-expected penetrometer resistance. Measurements of tensile strength were conducted on air-dry samples, and so the confounding effects of bulk density and water content were eliminated and it was found that tensile strength increased with sodicity in both coarse- and fine-textured soils. The presence of dispersed clay was therefore implicated in the development of aggregate coalescence in this work. Finally, a preliminary evaluation of how the early stages of aggregate coalescence might affect plant growth was attempted using tomatoes (Gross lisse) as a test plant. Seeds were planted in aggregates (0.5 – 4 mm) of a coarse- or fine-textured soil packed in steel rings. These were wetted at a rate of 1 mm/h to either near-saturation (for maximum coalescence) or to a suction of 10 kPa (for minimum coalescence) and held under these conditions for 24 h. All samples were then transferred to a ceramic pressure plate for drainage to 100 kPa suction for one week. Samples were then placed in a growth-cabinet held at 20C with controlled exposure to 14 h light/day. Germination of the seeds, plant height, and number and length of roots were observed. Germination of the seeds held at near-saturation in both coarse- and fine-textured soils was delayed by 24 h compared with seeds held at 10 kPa suction. Neither the number nor the length of tomato roots differed significantly between the different treatments and soils. In the coarse-textured soil, however, the total root length over a period of 14 days was somewhat greater in the uncoalesced samples than in the coalesced samples, but this difference was not statistically significant. These results suggest that aside from delaying germination, aggregate coalescence may not have a large effect on early growth of tomato plants. However, this is not to say that detrimental effects may not be manifest at later stages of plant growth, and this certainly needs to be evaluated, particularly because aggregate coalescence increase with repeated cycles of wetting and draining. In conclusion, the primary findings of the work undertaken in this thesis were: • Rapid wetting of soil aggregates to near-saturation enhanced the onset of soil aggregate coalescence as measured by (in some cases) penetrometer resistance at a soil water suction of 100 kPa, and (in most cases) tensile strength of soil cores in the air-dry state. The rate of wetting appeared to be more important in bringing on aggregate coalescence than how wet the soil eventually became during wetting. This means reducing the rate at which irrigation water is applied to soils may reduce the onset of aggregate coalescence more effectively than controlling the total amount of water applied – though both are important. The literature reports that aggregate coalescence occurs in the field over periods of up to several months, involving multiple wetting and draining cycles, but the work here demonstrated that this can occur over much shorter time periods depending on conditions imposed. • Aggregate coalescence occurred in coarse-textured soils regardless of whether the bulk density increased during wetting and draining. In finer-textured soils, the response to wetting conditions varied and was complicated by changes in bulk density and water content due to swelling. • Small overburden pressures enhanced the onset of aggregate coalescence, but these effects were diminished in the presence of high soil organic matter contents. • Finer aggregate size distributions (which are often produced in the field by excessive tillage during seedbed preparation) invariably led to greater aggregate coalescence than coarser aggregate size distributions. The effects of aggregate size were mitigated to some extent by higher contents of soil organic matter. • Sodicity enhanced aggregate coalescence as measured by tensile strength, but when penetrometer resistance was measured in the moist state, the effects were masked to some extent by higher water contents generated by swelling and dispersion. This work suggests that tensile strength (in the air dry state) may be a more effective measure of aggregate coalescence than penetrometer resistance. • Early plant response to aggregate coalescence was not large, but the response may become magnified during later stages of growth. / http://proxy.library.adelaide.edu.au/login?url= http://library.adelaide.edu.au/cgi-bin/Pwebrecon.cgi?BBID=1297583 / Thesis (Ph.D.) -- School of Earth and Environmental Sciences, 2007

The phenomenon called soil aggregate coalescence occurs at contact-points between aggregates and causes soil strength to increase to values that can inhibit plant root exploration and thus potential yield. During natural wetting and drying, soil aggregates appear to ‘weld’ together with little or no increase in dry bulk density. The precise reasons for this phenomenon are not understood, but it has been found to occur even in soils comprised entirely of water stable aggregates. Soil aggregate coalescence has not been widely observed and reported in soil science and yet may pose a significant risk for crops preventing them from achieving their genetic and environmental yield potentials. This project used soil penetrometer resistance and an indirect tensile-strength test to measure the early stages of aggregate coalescence and to evaluate their effects on the early growth of tomato plants. The early stages of aggregate coalescence were thought to be affected by a number of factors including: the matric suction of water during application and subsequent drainage, the overburden pressure on moist soil in the root zone, the initial size of soil aggregates prior to wetting, and the degree of sodicity of the soil aggregates. Seven mainexperiments were conducted to evaluate these factors. The matric suction during wetting of a seedbed affects the degree of aggregate slaking that occurs, and the strength of the wetted aggregates. The matric suction during draining affects the magnitude of ‘effective stresses’ that operate to retain soil structural integrity as the soil drains and dries out. An experiment was conducted to evaluate the influence of matric suction (within a range of suctions experienced in the field) on aggregate coalescence using soils of two different textures. Sieved aggregates (0.5 to 2 mm diameter) from a coarse-textured and two fine-textured (swelling) soils were packed into cylindrical rings (4.77 cm i.d., 5 cm high) and subjected to different suctions on wetting (near-saturation, and 1 kPa), and on draining (10 kPa on sintered-glass funnels, and 100 kPa on ceramic pressure plates). After one-week of drainage, penetrometer resistance was measured as a function of depth to approximately 45 mm (penetrometer had a recessedshaft, cone diameter = 2 mm, advanced at a rate of 0.3 mm/min). Tensile strength of other core-samples was measured after air-drying using an indirect “Brazilian” crushing test. For the coarse-textured soil, penetrometer resistance was significantly greater for samples wet to near-saturation, despite there being no significant increase in dry bulk density; this was not the case for the finer-textured soils, and it was difficult to distinguish the effects of variable bulk density upon drying from those of the imposed wetting treatments. In both coarse- and fine-textured soils, the tensile strength was significantly greater for samples wet to near-saturation. Thus wetting- and draining-suctions were both found to influence the degree of soil aggregate coalescence as measured by penetrometer resistance and tensile strength. Aggregate coalescence in irrigated crops is known to develop as the growing season progresses. It was therefore thought to be linked to the repeated occurrence of matric suctions that enhance the phenomenon during cycles of wetting and draining. An experiment was conducted to determine the extent of aggregate coalescence in a coarsetextured and two fine-textured (swelling clay) soils during 8 successive cycles of wetting and draining. Sieved aggregates (0.5 to 2 mm diameter) from each soil were packed into cylindrical rings (4.77 cm i.d., 5 cm high) and wetted to near saturation for 24 h. They were then drained on ceramic pressure plates to a suction of 100 kPa for one week, after which penetrometer resistance and tensile strength were measured as described above. The degree of expression of aggregate coalescence depended on soil type. For the coarse-textured soil, repeated wetting and draining significantly increased bulk density, penetrometer resistance and tensile strength. For the fine-textured soil, penetrometer resistance and bulk density did not vary significantly with repeated wetting and draining; on the contrary, there was evidence in these swelling clay soils to suggest bulk density and penetrometer resistance decreased. However, there was a progressive increase in tensile strength as cycles of wetting and draining progressed. The expansive nature of the fine-textured soil appears to have masked the development of aggregate coalescence as measured by penetrometer resistance, but its expression was very clear in measurements of tensile strength despite the reduction in bulk density with successive wetting and draining. Field observations have indicated that aggregate coalescence is first expressed at the bottom of the seedbed and that it develops progressively upward to the soil surface during the growing season. This suggests that overburden pressures may enhance the onset of the phenomenon by increasing the degree of inter-aggregate contact. Soils containing large quantities of particulate organic matter were known to resist the onset of aggregate coalescence to some extent. An experiment was conducted to evaluate the effects of soil organic matter and overburden pressures, by placing brass cylinders of various weights (equivalent to static load pressures of 0, 0.49, 1.47 and 2.47 kPa) on the top of dry soil aggregates (0.5 – 2 mm diameter) having widely different soil organic carbon contents placed in steel rings 5 cm high and 5 cm i.d. With the weights in place, the aggregates were wetted to near-saturation for 24 h and then drained on ceramic pressure plates to a suction of 100 kPa for one week. Bulk density, penetrometer resistance and tensile strength were measured when the samples were removed from the pressure plates and they all increased significantly with increasing overburden pressure in the soil with low organic matter content, but not in the soil with high organic matter content. The amount of tillage used to prepare seedbeds influences the size distribution of soil aggregates produced – that is, more tillage produces finer seedbeds. The size distribution of soil aggregates affects the number of inter-aggregate contact points and this was thought to influence the degree of aggregate coalescence that develops in a seedbed. Previous work has shown that soil organic matter reduces aggregate coalescence and so an experiment was conducted to evaluate the effects of aggregate size and organic matter on the phenomenon. For soils with high and low organic matter contents, aggregate size fractions of < 0.5, 0.5 – 2, 2 – 4, and < 4 mm were packed into soil cores (as above) and wetted to near-saturation then drained to 100 kPa suction as described above. Penetrometer resistance and tensile strength were measured and found to increase directly with the amount of fine material present in the soil cores – being greater in the < 0.5 mm and < 4 mm fractions, and being less in the 0.5 – 2 mm and 2 – 4 mm fractions. In all cases, penetrometer resistance and tensile strength were lower in the samples containing more organic matter. The rate at which soil aggregates are wetted in a seedbed affects the degree of slaking and densification that occurs, and the extent to which aggregates are wetted influences the overall strength of a seedbed. Both wetting rate and the extent of wetting were believed to influence the onset of aggregate coalescence and were thought to be affected by soil organic matter and irrigation technique. An experiment was therefore designed to separate these effects so that improvements to management could be evaluated for their greatest efficacy – that is, to determine whether management should focus on improving irrigation technique or increasing soil organic matter content, or both. The rate of wetting was controlled by spraying (or not spraying) soil aggregates (0.5 – 2 mm diameter) with polyvinyl alcohol (PVA). Samples of coarse- and fine-textured soils were packed into steel rings (as above) and subjected to different application rates of water (1, 10 and 100 mm/h) using a dripper system controlled by a peristaltic pump. Samples were brought to either a near-saturated state or to a suction of 10 kPa for 24 h, and then drained on a pressure plate at a suction of 100 kPa for one week. Measurements of penetrometer resistance and tensile strength were then made as described above. As expected, penetrometer resistance was lower in samples treated with PVA before wetting (slower wetting rates) and in samples held at a greater suction (10 kPa) after initial wetting (greater inter-aggregate strength). The effects were more pronounced in the coarse-textured soil. In both coarse- and fine-textured soils, tensile strengths increased with increasing wetting rate (greatest for 100 mm/h) and extent of wetting (greater when held at near-saturated conditions). The rate of wetting was found to be somewhat more important for promoting aggregate coalescence than the extent of wetting. Because aggregate coalescence often occurs with little or no increase in bulk density, an explanation for the increase in penetrometer resistance and tensile strength is unlikely to be explained by a large increase in the number of inter-aggregate contacts. An increase in the strength of existing points of inter-aggregate contact was therefore considered in this work. For inter-aggregate bond strengths to increase, it was hypothesized that small increases in the amount of mechanically (or spontaneously) dispersed clay particles, and subsequent deposition at inter-aggregate contact points could increase aggregate coalescence as measured by penetrometer resistance and tensile strength. An experiment was devised to manipulate the amount of spontaneously dispersed clay in coarse- and fine-textured soils of high and low organic matter content. The degree of sodicity of each soil was manipulated by varying the exchangeable sodium percentage (ESP) of soil aggregates (0.5 – 2mm) above and below a nominal threshold value of 6. Dry aggregates were then packed into steel rings (as above) and subjected to wetting near saturation, then draining to a suction of 100 kPa for one week as described above. Measurements were then taken of penetrometer resistance and tensile strength, both of which were affected by ESP in different ways. In the coarse-textured soil, sodicity enhanced aggregate slaking and dispersion, which increased bulk density. While penetrometer resistance also increased, its effect on aggregate coalescence could not be separated from a simple effect of increased bulk density. Similarly, the effect of sodicity on aggregate coalescence in the fine-textured soil was confounded by the higher water contents produced by greater swelling, which produced lower-than-expected penetrometer resistance. Measurements of tensile strength were conducted on air-dry samples, and so the confounding effects of bulk density and water content were eliminated and it was found that tensile strength increased with sodicity in both coarse- and fine-textured soils. The presence of dispersed clay was therefore implicated in the development of aggregate coalescence in this work. Finally, a preliminary evaluation of how the early stages of aggregate coalescence might affect plant growth was attempted using tomatoes (Gross lisse) as a test plant. Seeds were planted in aggregates (0.5 – 4 mm) of a coarse- or fine-textured soil packed in steel rings. These were wetted at a rate of 1 mm/h to either near-saturation (for maximum coalescence) or to a suction of 10 kPa (for minimum coalescence) and held under these conditions for 24 h. All samples were then transferred to a ceramic pressure plate for drainage to 100 kPa suction for one week. Samples were then placed in a growth-cabinet held at 20C with controlled exposure to 14 h light/day. Germination of the seeds, plant height, and number and length of roots were observed. Germination of the seeds held at near-saturation in both coarse- and fine-textured soils was delayed by 24 h compared with seeds held at 10 kPa suction. Neither the number nor the length of tomato roots differed significantly between the different treatments and soils. In the coarse-textured soil, however, the total root length over a period of 14 days was somewhat greater in the uncoalesced samples than in the coalesced samples, but this difference was not statistically significant. These results suggest that aside from delaying germination, aggregate coalescence may not have a large effect on early growth of tomato plants. However, this is not to say that detrimental effects may not be manifest at later stages of plant growth, and this certainly needs to be evaluated, particularly because aggregate coalescence increase with repeated cycles of wetting and draining. In conclusion, the primary findings of the work undertaken in this thesis were: • Rapid wetting of soil aggregates to near-saturation enhanced the onset of soil aggregate coalescence as measured by (in some cases) penetrometer resistance at a soil water suction of 100 kPa, and (in most cases) tensile strength of soil cores in the air-dry state. The rate of wetting appeared to be more important in bringing on aggregate coalescence than how wet the soil eventually became during wetting. This means reducing the rate at which irrigation water is applied to soils may reduce the onset of aggregate coalescence more effectively than controlling the total amount of water applied – though both are important. The literature reports that aggregate coalescence occurs in the field over periods of up to several months, involving multiple wetting and draining cycles, but the work here demonstrated that this can occur over much shorter time periods depending on conditions imposed. • Aggregate coalescence occurred in coarse-textured soils regardless of whether the bulk density increased during wetting and draining. In finer-textured soils, the response to wetting conditions varied and was complicated by changes in bulk density and water content due to swelling. • Small overburden pressures enhanced the onset of aggregate coalescence, but these effects were diminished in the presence of high soil organic matter contents. • Finer aggregate size distributions (which are often produced in the field by excessive tillage during seedbed preparation) invariably led to greater aggregate coalescence than coarser aggregate size distributions. The effects of aggregate size were mitigated to some extent by higher contents of soil organic matter. • Sodicity enhanced aggregate coalescence as measured by tensile strength, but when penetrometer resistance was measured in the moist state, the effects were masked to some extent by higher water contents generated by swelling and dispersion. This work suggests that tensile strength (in the air dry state) may be a more effective measure of aggregate coalescence than penetrometer resistance. • Early plant response to aggregate coalescence was not large, but the response may become magnified during later stages of growth. / http://proxy.library.adelaide.edu.au/login?url= http://library.adelaide.edu.au/cgi-bin/Pwebrecon.cgi?BBID=1297583 / Thesis (Ph.D.) -- School of Earth and Environmental Sciences, 2007

Thesis (M.S.); Submitted to Iowa State Univ., Ames, IA (US); 12 Dec 2003. / Published through the Information Bridge: DOE Scientific and Technical Information. "IS-T 2608" Maria Ambert Sanchez. 12/12/2003. Report is also available in paper and microfiche from NTIS.