Orientadores: Luís Roberto Marcondes Martins, Regina Maria Puppin Rontani / Tese (doutorado) - Universidade Estadual de Campinas, Faculdade de Odontologia de Piracicaba / Made available in DSpace on 2018-08-27T11:06:52Z (GMT). No. of bitstreams: 1 OliveiraJunior_CarlosdaCunha_D.pdf: 1940639 bytes, checksum: dd88a15626c32be08decb32f8ccbf98d (MD5) Previous issue date: 2015 / Resumo: O objetivo do estudo é avaliar in vitro o efeito da ciclagem termo mecânica na resistência de união push out e adaptação marginal em dentina. Para isso, foram confeccionados 60 blocos de dentina bovina, com dimensões 4mmX4mmX2mm e restaurados com diferentes sistemas adesivos: Single Bonde (SB - 3M), Clearfil SE Bond (CB) e Clearfil SE Protect (CP) (Kuraray). Foram feitas cavidades de 2 mm de diâmetro no centro dos blocos, que foram restaurados com compósito resinoso Z350 cor A3,5, e depois de armazenados em 100% de umidade. Foram polidos com discos Sof-lex da série laranja em sequência decrescente de abrasividade. Em seguida, 30 blocos foram aleatorizados para o grupo controle e os outros 30 foram imersos em fucsina 0,5% por 24h, em seguida, imersos em água por 4h e o excesso de fucsina removido. Foram, então, fotografados para o registro de possíveis fendas formadas. Em seguida, estes blocos foram submetidos à ciclagem mecânica (100.000 ciclos) e térmica (1.000 ciclos). Após o processo de fadiga termomecânica, os blocos foram novamente imersos em fuccina e novas imagens foram registradas. Estas foram analisadas através do software Image J, no qual se registrou o percentual de fendas antes e depois da ciclagem termomecânica pela equação: %fenda = l/lt x 100, onde l é o perímetro da fenda e lt é o perímetro da restauração total. Logo depois, os blocos foram levados ao testes de push out, onde se registrou a resistência de união dos sistemas adesivos estudados que foi comparada com o grupo controle. Os dados foram submetidos ao teste estatístico não paramétrico Kruskal-Wallis e Dunn, por meio do teste de Mann-Whitney para os valores de resitência push out e a análise de percentagem de fendas antes e depois da ciclagem termomecânica se deu pela ANOVA 2 fatores. Os resultados não mostraram diferença estatisticamente significativa entre os grupos no percentual de fendas formadas antes e após a ciclagem termomecânica, mas o grupo ciclado mostrou diferença estatística com o grupo controle, o grupo CP não foi estatisticamente diferente do CB e SB, por outro lado, CB e SB foi estatisticamente diferente. Estes achados sugerem que a ciclagem termomecânica diminuiu significativamente os valores de resistência de união push-out / Abstract: The objective of study to evaluate in vitro the effect of mechanical term cycling on the bond strength push out and marginal adaptation in dentin. For this, were made 60 bovine dentin blocks with dimensions 4mmX4mmX2mm and restored with different adhesive systems: Single Bonde (SB - 3M), Clearfil SE Bond (CB) and Clearfil SE Protect (CP) (Kuraray). 2 mm diameter wells were made in the center of the blocks that have been restored with composite resin Z350 A3,5 color and then stored in 100% humidity. They were polished with Sof-Lex discs orange series in decreasing abrasiveness sequence. Then 30 blocks were randomized to the control group and others 30 were immersed in 0.5% fuchsin for 24 hours, then immersed in water for 4 hours and the fuchsin excess removed. They were photographed to record possible gaps formed. Then these blocks were submitted to mechanical (100,000 cycles) and thermal (1,000 cycles) cycling. After the process of thermomechanical fatigue, the blocks were immersed in fuchsin and new images were recorded. They were analyzed using Image J software, on which registered the percentage of gaps before and after the thermomechanical cycling by the equation: % gap = l / l x 100, where L is the perimeter of the gap and Lt is the total perimeter of the restoration. After, the blocks were taken to push out test where the registered the bond strength of adhesive systems was compared with the control group. Data were subjected to statistical nonparametric Kruskal-Wallis and Dunn, using the Mann-Whitney test for bond strenght to push out, and the analysis values of the percentage of gap before and after the thermomechanical cycling was submited for ANOVA 2way. The results showed no statistically significant difference between groups in the percentage of gap formed before and after thermomechanical cycling, but cycling group showed statistical difference with the control group, the CP group was not statistically different from the CB and SB on the other hand, CB and SB were statistically different. These findings suggest that the thermomechanical cycling decreased the bond strength values push out / Doutorado / Materiais Dentarios / Doutor em Materiais Dentários

The effect of dental technical tools on the phase composition and roughness of 3/4/5 yttria-stabilized tetragonal zirconia polycrystalline (3y-/4y-/5y-TZP) for application in prosthetic dentistry was investigated. Additionally, the X-ray diffraction methods of Garvie-Nicholson and Rietveld were compared in a dental restoration context. Seven plates from two manufacturers, each fabricated from commercially available zirconia (3/4/5 mol%) for application as dental restorative material, were stressed by different dental technical tools used for grinding and polishing, as well as by chewing simulation and thermocycling. All specimens were examined via laser microscopy (surface roughness) and X-ray diffraction (DIN EN ISO 13356 and the Rietveld method). As a result, the monoclinic phase fraction was halved by grinding for the 3y-TZP and transformed entirely into one of the tetragonal phases by polishing/chewing for all specimens. The tetragonal phase t is preferred for an yttria content of 3 mol% and phase t″ for 5 mol%. Mechanical stress, such as polishing or grinding, does not trigger low-temperature degradation (LTD), but it fosters a phase transformation from monoclinic to tetragonal under certain conditions. This may increase the translucency and deteriorate the mechanical properties to some extent.