Thesis (M.S.)--University of Missouri--Rolla, 2007. / Vita. The entire thesis text is included in file. Title from title screen of thesis/dissertation PDF file (viewed April 16, 2008) Includes bibliographical references.

Thesis (Ph. D.)--University of Washington, 2002. / Vita. Includes bibliographical references (leaves 100-118).

Thesis (Ph. D.)--University of Texas at Austin, 2000. / Vita. Includes bibliographical references (leaves 147-159). Available also in a digital version from Dissertation Abstracts.

Thesis (Ph. D.)--Missouri University of Science and Technology, 2008. / Vita. The entire thesis text is included in file. Title from title screen of thesis/dissertation PDF file (viewed May 28, 2009) Includes bibliographical references (p. 91-93).

Thesis (M.S. in mechanical engineering)--Washington State University, August 2009. / Title from PDF title page (viewed on Sept. 16, 2009). "School of Engineering and Computer Science." Includes bibliographical references (p. 77-83).

Electron beam freeform fabrication (EBF3) is a rapid metal deposition process that works efficiently with the wieldable alloy Inconel 718 (IN 718). EBF3 is a developing additive manufacturing (AM) process that can manufacture IN 718 parts directly from computer aided design (CAD) data. EBF3 can produce parts significantly faster and more energy efficient than competing IN 718 AM technologies. The EBF3 process utilizes metal wire feedstock which is induced into a molten pool using a focused electron beam in a vacuum environment. This allows parts to be built layer by layer, creating intricate shapes that can be produced cheaper and faster than traditionally manufactured IN 718 parts. Furthermore, it allows traditionally manufactured parts to be modified as additional form is added to them using EBF3. Multiple industries rely on IN 718 parts and can utilize this technology including aerospace engineering, oil refinery, nuclear power generation, and food processing.A main drawback of EBF3 is the lack of knowledge of the effect different EBF3 build techniques will have on the properties of the deposited materials. Most of the reliable data on the mechanical properties relate to a linear build-up strategy and focus on the mechanical properties in the deposition direction (DD). There is no data related to other build-up techniques such as rotation build-up or transitional builds from forged material to EBF3 material. Reliable data on the behavior and microstructure of EBF3 material in a direction other than the DD is also difficult to find. Previous studies showed build-up height influenced mechanical properties but its role is not fully understood yet. This paper presents the mechanical properties and microstructure of an IN 718 plate built using a EBF3 rotational build-up strategy through utilizing a forged plug in the center. The tensile properties of samples at the transition from forged to EBF3 material showed higher ductility and reduced strength than pure EBF3 material. This is likely due the influence of the forge material in one half of the specimen. Samples taken at approximately 15 degree increments from 0 to 90 degrees rotation to the DD in the additive portion of the plate were subjected to tensile testing. Along the build height, or the transverse direction (TD), the lowest strength was demonstrated and the TD aligned strongly to a <001> texture. Samples 45 degrees to the DD showed the greatest strength due to their preference for aligning to a <111> texture. Samples low on the build height demonstrated a higher strength than those on the top and displayed grain structures along the TD which were long, linear, and narrow across multiple deposition layers.

The quality of parts fabricated using Laser Solid Freeform Fabrication (LSFF) is highly dependent on the physical phenomena and operating parameters which govern the process. For instance, the thermal stress patterns and intensity, induced throughout the process domain due to the layer-by-layer material deposition and the temperature distribution characteristics, contribute significantly to potential delamination and crack formation across the fabricated part. In this research, some of the main features as well as drawbacks of this technique are studied through a multi-physics analysis of the process. For this purpose, a coupled time-dependent 3D model is developed with which the geometry of the deposited material as well as temperature and thermal stress fields across the process domain can be predicted. In the proposed approach, coupled thermal and stress domains are numerically obtained assuming a decoupled interaction between the laser beam and powder stream. To predict the geometry of the deposited material, once the melt pool boundary is obtained, the process domain is discretized in a cross-sectional fashion based on the powder feed rate, elapsed time, and intersection of the melt pool and powder stream projected on the substrate. Layers of additive material are then added onto the non-planar domain. The main process parameters affected by a multilayer deposition due to the formation of non-planar surfaces, such as powder catchment, are incorporated into the modelling approach to enhance the accuracy of the results. To demonstrate the proposed algorithm and to study the main features of the process, a four-layer thin wall of AISI 304L steel on a substrate of the same material is numerically and experimentally fabricated. The numerical analyses along with the experimental results are then used to investigate the correlation between the temperature-thermal stress fields and crack formation across the fabricated parts. The trend of the results reveals that by preheating the substrate prior to the fabrication process, it is possible to substantially reduce the formed micro-cracks. To demonstrate the feasibility of preheating on the reduction of micro-cracks, several simulations and experiments are performed in which a crack-free result is obtained, with a 22 per cent reduction in thermal stresses when the substrate is preheated to 800 K. The numerical and experimental results are also used to study the circumstances of the microstructural formation during the fabrication process. To conclude this research, the developed modelling approach is further extended to briefly discuss the effects of the path patterns and the main operating parameters on the outcomes of the process. The effects of the material properties and their variations on the temperature distributions and thermal stress fields are studied by fabrication of a thin wall of two Stellite 6 layers and two Ti layers on a stainless steel substrate.

The quality of parts fabricated using Laser Solid Freeform Fabrication (LSFF) is highly dependent on the physical phenomena and operating parameters which govern the process. For instance, the thermal stress patterns and intensity, induced throughout the process domain due to the layer-by-layer material deposition and the temperature distribution characteristics, contribute significantly to potential delamination and crack formation across the fabricated part. In this research, some of the main features as well as drawbacks of this technique are studied through a multi-physics analysis of the process. For this purpose, a coupled time-dependent 3D model is developed with which the geometry of the deposited material as well as temperature and thermal stress fields across the process domain can be predicted. In the proposed approach, coupled thermal and stress domains are numerically obtained assuming a decoupled interaction between the laser beam and powder stream. To predict the geometry of the deposited material, once the melt pool boundary is obtained, the process domain is discretized in a cross-sectional fashion based on the powder feed rate, elapsed time, and intersection of the melt pool and powder stream projected on the substrate. Layers of additive material are then added onto the non-planar domain. The main process parameters affected by a multilayer deposition due to the formation of non-planar surfaces, such as powder catchment, are incorporated into the modelling approach to enhance the accuracy of the results. To demonstrate the proposed algorithm and to study the main features of the process, a four-layer thin wall of AISI 304L steel on a substrate of the same material is numerically and experimentally fabricated. The numerical analyses along with the experimental results are then used to investigate the correlation between the temperature-thermal stress fields and crack formation across the fabricated parts. The trend of the results reveals that by preheating the substrate prior to the fabrication process, it is possible to substantially reduce the formed micro-cracks. To demonstrate the feasibility of preheating on the reduction of micro-cracks, several simulations and experiments are performed in which a crack-free result is obtained, with a 22 per cent reduction in thermal stresses when the substrate is preheated to 800 K. The numerical and experimental results are also used to study the circumstances of the microstructural formation during the fabrication process. To conclude this research, the developed modelling approach is further extended to briefly discuss the effects of the path patterns and the main operating parameters on the outcomes of the process. The effects of the material properties and their variations on the temperature distributions and thermal stress fields are studied by fabrication of a thin wall of two Stellite 6 layers and two Ti layers on a stainless steel substrate.

Applications involving high electrical conduction require complex components that are difficult to be manufactured by conventional processes. Laser sintering (LS) is an additive manufacturing technique that overcomes these drawbacks by offering design flexibility. This study focuses upon optimizing the process of laser sintering to manufacture functional prototypes of components used in high electrical conduction applications. Specifically, components for two systems – high current sliding electrical contacts and fuel cells – were designed, manufactured and tested. C-asperity rails were made by LS and tested in a high current sliding electrical setup. Corrugated flow field plates were created by LS and their performance in a direct methanol fuel cell (DMFC) was tested. This is the first experimental attempt at using laser sintering for manufacturing such complex components for use in high electrical conduction applications. The second part of this study involves optimization the laser sintering process. Towards this, efforts were made to improve the green strength of parts made by LS. Particle size of graphite/ phenolic resin and addition of nylon/11 and wax were tested for their effect upon green strength. Of these, significant improvement of green strength was observed by altering the particle size of the graphite/ phenolic resin system. New methods of improving green strength by employing fast cure phenolic resins with carbon fiber additions were successfully demonstrated. This study also identified a binder system and process parameters for indirect LS of stainless steel –for bipolar plate compression/ injection mold tooling. All the experimental results of this study lead us to believe that laser sintering can be developed as a robust and efficient process for the manufacture of specialized components used in advanced electrical conduction systems. / text

Thesis (M.S.)--University of Texas at El Paso, 2009. / Title from title screen. Vita. CD-ROM. Includes bibliographical references. Also available online.