Orientadora: Profa. Dra. Juliana Tófano de Campos Leite Toneli / Dissertação (mestrado) - Universidade Federal do ABC. Programa de Pós-Graduação em Energia, 2014. / Os tanques com impulsores mecânicos são empregados nas indústrias químicas, petroquímicas, alimentícia, farmacêutica e mineral, como reatores químicos, diluidores, decantadores, misturadores e trocadores de calor. A transmissão de calor em tanques com agitação é realizada através das jaquetas, serpentinas helicoidais, serpentinas em espiral e chicanas tubulares verticais, sendo que existe uma carência de dados na literatura sobre a utilização das chicanas tubulares, em projetos em escala industrial. O presente estudo teve por objetivo principal comparar a transferência de calor e o consumo energético em tanques com impulsores mecânicos, axial e radial, equipados com chicanas tubulares verticais. Como objetivos específicos, o presente estudo visou determinar correlações semi-empíricas para o coeficiente convectivo no escoamento externo, em relação aos impulsores mecânicos utilizados em função dos parâmetros de similaridade Reynolds e Prandtl, e avaliar o efeito do impulsor mecânico sobre a potência consumida e a transmissão de calor. A unidade experimental consistiu, basicamente, de um tanque de acrílico com um volume útil de 50 litros, um impulsor mecânico axial, um impulsor radial tipo turbina, um motor elétrico de 2,5 hp e uma chicana tubular com 4 bancos de tubos de cobre. Os fluidos frios utilizados foram água e solução de sacarose com concentrações de 20% e 50% em massa. O fluido quente utilizado foi água à temperatura constante de 60°C e vazão de 1,2 LPM. Os ensaios foram realizados alternando as rotações na faixa de 90 a 330 RPM e a temperatura de entrada do fluido frio no intervalo de 28°C a 45°C. A potência consumida por ambos os impulsores mecânicos foi determinada a partir da técnica da medição do torque gerado no motor elétrico. O modelo obtido para a previsão do coeficiente externo de convecção, com o impulsor axial apresentou, um desvio médio de 21% e o modelo para o impulsor radial, um desvio médio de 25%. A partir dos modelos obtidos, verificou-se que o impulsor radial incrementa a transmissão de calor em 43% quando comparado com o impulsor axial. A rotação ideal para a maior transmissão de calor, durante o aquecimento das soluções, com o menor consumo de energia foi de 300 rpm. A partir das curvas simultâneas do número de potência e do número de Nusselt, conclui-se que o impulsor axial é o mais indicado para o aquecimento tendo em vista o seu baixo consumo de potência em relação ao impulsor radial. / EThe tanks with mechanical impellers are employed in chemical, petrochemical, food, pharmaceutical and mineral industries, as chemical reactors, thinners, decanters, mixers and heat exchangers. The heat transmission in tanks with agitation is performed through the jackets, helical coils, coils in spiral and vertical tubular baffles, considering that there is a lack of data in the literature on the use of tubular baffles, in industrial scale projects. The present study aimed to compare the main heat transfer and energy consumption in tanks with mechanical axial and radial impellers equipped with tubular vertical baffles. As specific objectives, this study aimed to determine correlations for convective coefficient in the external flow in relation to mechanical impellers used in function of Reynolds and Prandtl similarity parameters, and evaluate the mechanical effect on power consumption and heat transmission. The experimental unit consisted primarily of an acrylic tank with a useful volume of 50 liters, an axial mechanical and turbine type radial impeller, a 2.5 hp electric motor and a tubular chicanery with 4 banks of copper tubes. The cold fluids applied were water, and sucrose solution with concentrations of 20% and 50% by mass. The hot fluid applied was water at constant temperature of 60° C and a 1.2 LPM flow. The tests were carried out in the range of rotations by 90 to 330 RPM and the cold fluid inlet temperature in the range from 28° C to 45° C. The power consumed by both mechanical impellers was determined through the thechnique of measurement of the torque generated at electric motor. The model obtained for external coefficient prediction of convection with the axial impeller presented an average deviation of 21% and the template for the radial impeller, a standard deviation of 25%. From the models obtained, it was found that the radial impeller increases the transmission of heat in 43% when compared with the axial impeller. The ideal rotation for greater heat transfer during heating of the solutions with the lowest energy consumption amounted to 300 rpm. From the number of concurrent power curves and Nusselt number, it is concluded that the axial impeller is the most indicated for heating in view of its low power consumption compared to radial impeller.

O presente trabalho teve como objetivo avaliar a influência da intensidade de agitação e tipo de impelidor, bem como a estratégia de alimentação, em reator anaeróbio operado em batelada seqüencial, escala piloto (\'da ordem de\' 1 \'M POT.3\'), com agitação mecânica e em duas configurações: uma com biomassa granulada (ASBR) e outra com biomassa imobilizada em suporte inerte de espuma de poliuretano (ASBBR), aplicadas ao tratamento de esgoto doméstico. No estudo da intensidade de agitação e tipo de impelidor, para cada reator foram avaliadas três tipos de impelidores (turbina de pás planas, turbina de pás inclinadas 45º e hélice) associados a duas intensidades de agitação (40 e 80 rpm), obtendo uma combinação de 6 (seis) condições experimentais. A combinação da intensidade de agitação e tipo de impelidor que apresentou melhor desempenho no processo foi utilizado no estudo da estratégia de alimentação, na qual foi avaliada as seguintes condições: batelada alimentada durante 25%, 50%, 75% e 100% do ciclo. Os resultados obtidos permitiram concluir que: no ASBBR o aumento da intensidade de agitação de 40 rpm para 80 rpm permitiu uma melhoria nos fluxos de transferência de massa e, portanto, aumentou a velocidade de consumo de substrato; no ASBR o aumento da intensidade de agitação de 40 rpm para 80 rpm proporcinou uma desestabilização do sistema, provavelmente por causa da ruptura dos grânulos provocada pela maior agitação; os sistemas operados com impelidor do tipo hélice apresentaram vantagens, tais como: melhor eficiência de remoção de sólidos, maior valor da constante cinética de primeira ordem (melhor fluxo de transferência de massa e conseqüentemente maior consumo de substrato) e maior produção de alcalinidade, ou seja, maior estabilidade para o sistema; tanto o sistema ASBR como o ASBBR quando operados nas condições de batelada típica, batelada alimentada durante 50% e 75% do ciclo apresentaram melhores desempenhos no processo de tratamento, mostrando a flexibilidade operacional dos reatores anaeróbios operados em bateladas seqüenciais; e comparando os sistemas ASBBR e ASBR verificou-se que estes apresentaram comportamentos similares em todas as condições de operação de batelada alimentada avaliadas, não sendo possível, estatisticamente apontar um sistema com melhor desempenho. / The objective of this work was to assess the effect of the stirring speed, the type of impeller and the feed strategy in a mechanically stirred pilot-scale (\'da ordem de\' 1 \'M POT.3\') anaerobic sequencing batch reactor to two configurations: a containing granulated biomass (ASBR) and the other containing immobilized biomass (AnSBBR). Domestic wastewater was treated in 8-h cycles. Three impeller types (turbine with six-flat blades, turbine with six 45º-inclined blades and helix with three blades) were assessed at two different stirring speeds (40 and 80 rpm), totaling six experimental conditions. The stirring speed and the impeller that resulted in the best combination was used in work of the feed strategy . The reactors were operated at room temperature at four different feed strategies (fed batch during 25%, 50% and 75% of the cycle, and conventional fed-batch). The results allowed conclude that: in the AnSBBR increasing the stirring speed from 40 rpm to 80 rpm showed to improve mass transfer, with consequent increase in substrate consumption; in the ASBR increasing the stirring speed from 40 rpm to 80 rpm showed desestabilization in system, because of the disruption caused in the granules witth greater agitation; operation with the helix impeller showed some advantages over the turbine impellers, such as: improved efficiency in solids removal, higher value of the first order kinetic constant and higher alkalinity production; both for the ASBR as for the ASBBR the best performance in wastewater treatment was obtained when the reactors were operated at conventional batch, fed-batch during 50% and 75% of the cycle; no significant difference in performance was observed among these three conditions. Despite poor performance of the conventional fed-batch and fed-batch during 25% of the cycle compared to the other conditions, both these conditions presented operational stability. Hence, the anaerobic sequencing batch reactors presented operational flexibility as far as feed strategy is concerned.

The aim of the diploma thesis is to design the pump impeller. The classical design of the impeller is made for one operating point, in which pump is assumed to operate most of the time. The aim of this diploma thesis is to design a pump, whose pump cover and pump drive discs are designed for each other operating point and then compare the results of both design methods.

The aim of the thesis was to propose a pump impeller with higher effectiveness and verify the proposal with the calculation using programs Gambit and Fluent. Three designed impellers were afterwards made using 3D printer and its characteristics were measured in a hydraulic laboratory in Kaplan Department of hydraulic machines. The proposal of a so called wideband impeller of the centrifugal pump was made with chaotic ordering of blade cascades, in one impeller occur blades with various input and output angles and different shapes of blades but all blades have got similar shape in a meridian sectional view of impeller. The thesis was divided into three parts. In the first part, a conforming transformation was theoretically described which was in the thesis used for the shape proposal of impeller blades. In the second part of the thesis final proposals and calculations of pump impellers were made. The third part of the thesis focused on the processing and evaluation of experimental measurement in the hydraulic laboratory and finally the results of the thesis were summarized in the conclusion.

The presented master's thesis deals with the safety assessment of several variants of the impeller with different blades length. The motivation for creating this thesis is to find the solution of the problem situation which is characterized by the breakdown of the steam turbine impeller with blades length of 30mm. As confirmed in this thesis, the impeller with blades length of 30mm is operated in the resonance. Likewise, according to the technical standard ČSN EN ISO 10437 its operation is not safe. As the correction action for the problem situation solving is proposed the prolongation of the impeller's blades. The safety is detected for six variants of impeller with dierent blades length. For each variant, there is executed a modal analysis and its results are drawn up into the Campbell diagram. On the basis of this diagram, the safety of individual components is evaluated. The last part of the masters thesis concerns with the examination of the influence of blades length on the modal properties of the impeller.

The effects of impeller-diffuser interaction are investigated through numerically simulating the modified wedge vane profiles. Steady and time-accurate, 3D- viscous RANSsolver is used to perform flow field computations. The original design is modified to obtain better aerodynamic performance. Five morechanges are made to the leading edge profile of the new design, in order to assess different degrees of unsteadiness. These changes show that their contribution on stageefficiency is rather minor, while they have a huge reduction on blade loadings. Moreover, it is shown that the shorter radial distance of vaneless space does not necessarilymean an increased loading thanks to the eliminating in-phase fluctuations on pressureand suction sides. It is found that the impeller reacts to the upstream static pressure disturbance, whichis caused by the applied geometry change and its resultant flow field in the wedge diffuser, but not to the radial location of a certain profile. In addition, the results indicatethat the wedge diffuser aerodynamic performance is driven by time-averaged flow fieldbehaviour.

Čerpadla s nízkými specifickými otáčkami nacházejí uplatnění v široké škále aplikací, ale trpí nízkou účinností a rizikem nestability křivky dopravní výšky. Tato disertační práce pojednává o vylepšení hydraulických parametrů čerpadla se specifickými otáčkami ns = 32. Práce se zaměřuje na průtok v oběžném kole a ve spirále, které jsou řešeny pomocí CFD. Průzkum literatury ukázal, že přidání mezilopatek do průtokového kanálu je účinný způsob, jak zlepšit neuspokojivé proudění obecně přítomné v oběžných kolech s nízkými specifickými otáčkami. Byla zkoumána poloha mezilopatky v kanálu a vliv počtu přítomných mezilopatek. Část výsledků je ověřena experimentálně v laboratoři fakulty. Rovněž je zkoumán tvar spirály a pozornost je věnována numerickému řešení proudění u stěn a jeho vlivu na simulaci. Po numerických výpočtech na třech různých spirálách je navržen nový tvar, který zlepšuje vypočtové parametry čerpadla při nízkém i vysokém průtoku.

Due to the increasing demand for processing low-grade ores, larger volumes of material are being processed. Therefore, the size of flotation equipment has significantly increased for the past decades. The studies related to scale-up are and will remain to be crucial in terms of designing larger flotation equipment. One of the most important factors for flotation scaling-up is the “flotation rate constant”. Hence, the main aim of this investigation was to understand the scale-up criteria when the size of different laboratory-scale cells increases, using the Outotec GTK LabCell®. This was done by assessing the influence of impeller speed, as a hydrodynamic variable, on the flotation performance. Recovery was found to increase with an increase in the cell area to rotor diameter ratio. Flotation rate and recovery increased with an increase in the impeller speed until a certain point that it eventually decreased for the 2 l and 7.5 l cells. For the 4 l cell, the flotation rate and recovery decreased with increasing the impeller speed. The impeller speed of 1200 rpm allowed a successful scale-up based on the flotation rate constants and recovery when increasing the size of the cells. Maintaining the impeller speeds constant at 1300 rpm increased the flotation rate constants and recovery when increasing the cell size from both the 2 and 4 l cells to the 7.5 l cell. A further increase in the impeller speed to 1400 rpm also produced the flotation rate constants and recovery to increase as the cell size increased from both the 2 and 4 l cells to the 7.5 l cell. However, when increasing the cell size from 2 l to 4 l, good results were also observed for all impeller speeds. The products concentrate seem to become finer when decreasing the cell size, with only a few exceptions. The recovery of particles larger than 38 μm was found to differ considerably less among the different scales.

This doctoral thesis studies the non-uniform blade cascade for centrifugal pumps. Influence of non-uniform blade cascade is investigated on the impeller and diffuser. A non-uniform blading impeller of pumps in this doctoral thesis was examined in terms of influence on efficiency characteristic. The idea of using non-uniform blading is to obtain a flat efficiency characteristic. Then the centrifugal pump could be used on larger scale of power with achieving a sufficiently high efficiency. The work is based on experimental measurements and numerical simulations of non-uniform hydraulic pump components. Non-uniform impeller and the diffuser were newly designed for this research. A new measuring track of small submersible pumps was needed to design and build for measurements. Different pump combinations with conventional hydraulics on one working point and hydraulics with non-uniform were measured. All measurements were evaluated and characteristics of efficiency, head and power were obtained for each measured combination. Some of pump combinations (which were measured in experiment) were numerically simulated by program Ansys Fluent. Data needed to evaluate the characteristic of efficiency and specific energy were collected from each numerical simulation. A theoretical consideration concerns the influence of non-uniform blade cascade applied on diffuser. The suggestion how to decrease hydraulic losses in canals was done. The theoretical consideration how to make a flat efficiency characteristic was made.

Em um reator de fundo redondo e volume útil de 5 L tratando esgoto sintético com carga orgânica de 800 mgDQO.'L POT.-1' com biomassa granulada a influência do tipo de escoamento e velocidade rotacional foi investigada com o uso de cinco impelidores sendo eles turbina e pá de seis pás planas verticais, turbina e pá de seis pás planas inclinadas 45 graus e hélice, comumente aplicados em processos biológicos. Foi também investigada a viabilidade de implementação de tubo de tiragem ao reator em conjunto com os impelidores tipo hélice e tipo pá de pás planas inclinadas alternadamente, com vistas a melhorar a mistura e conseqüente transferência de massa no meio reacional. Os resultados mostram que a alteração do tipo de impelidor e as variações da velocidade rotacional não exerceram influência significativa sobre a estabilidade e desempenho dos sistemas estudados. Entretanto a análise das constantes do modelo cinético de primeira ordem mostrou que a alteração na velocidade rotacional exerceu influência de aumento dos valores das constantes, demonstrando com isto que o aumento da velocidade rotacional melhora a transferência de massa sólido-líquido no meio reacional. A análise das constantes cinéticas também demonstrou que a promoção de escoamento axial em reatores agitados mecanicamente é preferível ao escoamento radial quando comparados os impelidores tipo pá de pás planas verticais e de pás planas inclinadas. A presença do tubo de tiragem demonstrou incrementar significativamente a transferência de massa, através do aumento dos valores numéricos das constantes utilizadas no ajuste do modelo cinético de primeira ordem aos valores experimentais. A potência consumida foi inferior a 1,6.'10 POT.-3' HP/'M POT.3' com rotações abaixo de 200 rpm e os impelidores axiais consumiram 75% a menos de potência do que os radiais / The effect of flow type and rotor speed were investigated in a round-bottom reactor with 5 L useful volume containing granular biomass and treating synthetic wastewater with organic load of 800 mgCOD.'L POT.-1'. Five impellers have been used to this end, namely: turbine and paddle with six-vertical-flat blade, turbine and paddle with six-45 degrees-inclined-flat-blade and helix, commonly used in biological processes. Utilization of a draft tube together with the helix and six-alternately-inclined-flat-blade impellers was also assessed as a means to improve mixing and consequently mass transfer in the reaction medium. Results showed that altering impeller type and variation in rotor speed did not exert significant effect on the stability and performance of the investigated systems. However, analysis of the first order kinetic model constants showed that alteration in rotor speed resulted in increase in the values of the constants, demonstrating that increase in rotor speed improves solid-liquid mass transfer in the reaction medium. Analysis of the kinetic constants also showed that axial flow in mechanically stirred reactors is preferable over radial flow when the vertical flat blade impeller is compared to the inclined flat blade impeller. The presence of the draft tube showed significant improvement in mass transfer, which could be seen by the increase in the values of the constants used in the fit of the first order kinetic model to the experimental values. The power consumed was less than 1.6.'10 POT.-3' HP/'M POT.3' at rotor frequency below 200 rpm and the axial impellers consumed 75% less power than the radial ones