Thesis (M.S.)--West Virginia University, 2006. / Title from document title page. Document formatted into pages; contains x, 133 p. : ill. (some col.). Includes abstract. Includes bibliographical references (p. 132-133).

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This work presents mechanical nano-grinding as an alternative technique for the fabrication of optical fibers endface microlenses. It also presents a novel surface-roughness improvement technique called Loose Abrasive Blasting (LAB). Traditionally, the majority of such microlenses are made using either chemical etching or heating and pulling methods. Despite the success of these methods, they suffer some common drawbacks such as the lack of controllability on the produced lens profile. Consequently the possible variations of the lens profiles that can be made by these methods are also limited. The difficulty to center the lens on the fiber core is another problem associated with heating and pulling method. The exposure to hazardous chemical such as hydrofluoric acid is yet another problem associated with chemical etching. Nano-grinding technique described in this thesis should provide a much better alternative to the traditional optical fabrication techniques. Nano-grinding experiments were conducted on a nano-grinding machine (NGM) specially built for this purpose. The machine incorporates state-of-the-art air-bearing spindles, piezo electric actuators, and capacitive displacement sensors with accuracy down to 2 nm. Such precise motion provided by this system is the key for the success of this technique. With such system, it was possible to produce a multitude variety of lens profiles with high profile accuracy and with surfaces of optical quality without the need for exposure to any kind of hazardous chemicals. In achieving this objective, the research was conducted on many frontiers. First, the possibility of grinding optical fibers without inducing surface and subsurface damages was investigated. Micro-indentation, nano-indentation, and nano-scratch tests were conducted to determine the critical depth of cut that can be achieved before the occurrence of surface and subsurface cracks. Nano-scratch test in particular provided a clear insight to the cracking and the chipping mechanisms that might unfold if the critical depth of cut was exceeded in an actual grinding situation. The knowledge gained from this exercise laid the ground base for the design of the NGM. Using the NGM, further experiments were carried out to determine the optimal grinding parameters for an efficient and successful grinding process. Parameters investigated include the grit size, the cutting speed, and the in-feed rates. The optimum parameters have to ensure the best endface surface quality and the same time maintain a high throughput. This study shows that based on these optimal parameters, it should be possible to produce endface microlenses of optical surface quality free surface and/or subsurface damages in less than 30 seconds with surface roughness (Ra) less than 3 nm. A novel post-grinding surface improvement techniques was also developed. The technique called loose abrasive blasting (LAB) can be used for polishing at and non-flat surfaces. Experiments were conducted on a loose abrasive blasting machine built specially for this purpose. The performance of this technique was compared with other techniques such as slurry polishing and chemical etching used for polishing of brittle materials. The results showed that while chemical etching was found unsuitable for polishing of at optical fiber endfaces, LAB outperformed slurry polishing by significant margin. After the optimal grinding conditions were established, the NGM was used for grinding of different kinds of optical fiber microlens profiles. Among the endface profiles produced were conical lenses, tapered lenses, D-shaped lenses and others. It has also been shown, in case of conical lenses for instance, that there is almost unlimited number of profiles that can be produced by simply changing the contact angle between the fiber endface and the grinding film. The effect of surface roughness on light coupling efficiency between a fiber endface and a laser diode was also investigated. Cleaved fiber endfaces as well as ground endfaces with variant degrees of surface roughness were used in this experiment. The results showed that surface roughness has significant effect on light coupling efficiency. The effect of lens eccentricity on light coupling was also investigated.

Thesis (Ph. D.)--University of Texas at Austin, 2001. / Vita. Includes bibliographical references. Available also from UMI/Dissertation Abstracts International.

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Because of their compatibility with the planar concept of integrated optics, grating couplers offer the most satisfactory means of coupling light into thin film optical waveguides. The purpose of this dissertation has been to study the behaviour, both theoretically and experimentally, and fabrication of grating couplers in nonlinear waveguides. A theory of nonlinear grating couplers is presented based on a coupled-mode approach. The dependence of coupling efficiency on incident beam intensity, beam size, beam position, incident angle, chirp rate, and waveguide losses have been examined all in the presence of nonlinearities in the waveguide. It is reported that, in the presence of nonlinearities, the coupling efficiency decreases with increasing incident power. Different ways of optimizing the coupling efficiency at high incident power levels are presented. These include adjusting the beam size, the coupling angle, and chirping the grating. A new technique is reported for fabrication of regular period, chirped, and curved photoresist gratings. The experimental arrangement is essentially based on Lloyd's mirror fringes and is characterized by its stability, simplicity, and versatility. We also report on successful use of Reactive Ion-Beam Etching (RIBE) with C₂F₆ gas in producing very smooth and deep gratings with high aspect ratios in different waveguide structures. Experimental coupling efficiencies of up to 40% are reported in polystyrene waveguides using etched grating couplers. Experiments are reported in support of the theoretical findings of this dissertation using a polystyrene waveguide with thermal nonlinearity.

Light can be coupled out of a waveguide to a focused point by a focusing grating coupler and has possible applications in optical data storage. The grating can be fabricated with either e-beam techniques or holographic techniques. Two design methods are demonstrated that model the focusing grating coupler with holographic optical elements. Both methods take a geometrical optics approach to designing the holographic optical elements and both methods make use of commercially available ray trace programs. The first method uses complicated non-rotationally symmetric construction optics and requires either a modified ray trace program or special user defined surfaces. The second method involves a much simpler approach which did not require any changes to an existing ray trace program and requires only rotationally symmetric elements to correct the aberrations.

Surface plasmons are of interest for various applications, including optical interconnects and devices, light sources, nanolithography, biosensors, solar cells, and negative-refraction prisms or superlenses. Some of the most important applications are SP-based optical interconnects and devices, which offer the potential of realizing integrated optical nanocircuitry due to the subwavelength confinement and the slow-wave nature of SPs. The fundamental building element of these applications is the plasmonic waveguide. Among the family of various plasmonic waveguides, the metal-insulator-metal waveguide has superior lateral confinement because of the relatively shallow field penetration into the metal claddings (about a skin depth -- usually tens of nanometers). Such subwavelength confinement cannot be achieved by conventional dielectric optical waveguides. However, the loss in the MIM waveguide is substantial due to the strong absorption of metal in the visible or near-infrared spectrum. Therefore, the design, simulation, and measurement of the loss in the MIM waveguide are critically important in the development of SP-based nanocircuitry. Surface plasmons (SPs) are of interest for various applications, including optical interconnects and devices, light sources, nanolithography, biosensors, solar cells, and negative-refraction prisms or superlenses. Some of the most important applications are SP-based optical interconnects and devices, which offer the potential of realizing integrated optical nanocircuitry due to the subwavelength confinement and the slow-wave nature of SPs. The fundamental building element of these applications is the plasmonic waveguide. Among the family of various plasmonic waveguides, the metal-insulator-metal (MIM) waveguide has superior lateral confinement because of the relatively shallow field penetration into the metal claddings (about a skin depth -- usually tens of nanometers). Such subwavelength confinement cannot be achieved by conventional dielectric optical waveguides. However, the loss in the MIM waveguide is substantial due to the strong absorption of metal in the visible or near-infrared spectrum. Therefore, the design, simulation, and measurement of the loss in the MIM waveguide are critically important in the development of SP-based nanocircuitry. Owing to the subwavelength sizes of MIM waveguides, the excitation of an MIM plasmonic mode typically requires end-fire coupling with tapered fibers or waveguides. Further, the conventional loss measurements require the usage of a near-field scanning optical microscopy (NSOM) or multiple waveguide samples with various length scales; however, the two aforementioned techniques are both complicated and have issues of sensitivity to uncontrollable environmental factors or variations in coupling strength, respectively. These experimental challenges have been a primary reason for the slow experimental development of the MIM waveguide and device. The research in this thesis focuses on the development of the transverse transmission/reflection (TTR) method, which is a more reliable, accurate, and straightforward method of characterizing the plasmonic modes in the MIM waveguide. The theory of the TTR method, which incorporates an attenuated total reflection (ATR) configuration, is developed based on the transmission matrix formulation. A methodology for obtaining the propagation constant and attenuation coefficient of a plasmonic mode in an MIM waveguide is illustrated. Using the Metricon Prism Coupler, the TTR method is experimentally applied to planar, single-mode MIM (Au-SiO$_2$-Au) waveguides with various core thicknesses at $lambda=1550$ nm. The experimental results are in very good agreement with the theoretical results. It is also shown experimentally that the TTR method is robust against difficult-to-quantify parameters such as the metal cladding thickness and the air gap thickness between the prism and the waveguide. As a result, the TTR method can be readily applied by using other similar ATR or prism-coupler configurations, without concern for the sensitivity issues caused by the subtle differences between various configurations. Moreover, the TTR method is also experimentally applied to planar, multimode MIM waveguides. Multimode MIM waveguides, which have larger core sizes, may be of interest for applications in low-loss interconnects or tapered end-couplers. Thanks to the superior angular selectivity of the ATR configuration, the TTR method is capable of detecting the propagation constant and attenuation coefficient of each mode. To the best of the author's knowledge, this is the first time the propagation constant of each mode in a multimode MIM waveguide has been individually measured. Also, to the best of the author's knowledge, this is the first time the attenuation coefficient of each mode in a multimode MIM waveguide has been individually measured. The TTR method is proved to be a reliable, accurate, and straightforward approach to characterize plasmonic modes in MIM waveguides. Future research will target the extension of the TTR method to 2D MIM waveguides, asymmetric MIM waveguides, and inclusion of scattering loss. Taking full advantage of the TTR method, the development of plasmonic devices can be potentially accelerated. The theory of the TTR method, which incorporates an attenuated total reflection (ATR) configuration, is developed based on the transmission matrix formulation. A methodology for obtaining the propagation constant and attenuation coefficient of a plasmonic mode in an MIM waveguide is illustrated. Using the Metricon Prism Coupler, the TTR method is experimentally applied to planar, single-mode MIM (Au-SiO$_2$-Au) waveguides with various core thicknesses at $lambda=1550$ nm. The experimental results are in very good agreement with the theoretical results. It is also shown experimentally that the TTR method is robust against difficult-to-quantify parameters such as the metal cladding thickness and the air gap thickness between the prism and the waveguide. As a result, the TTR method can be readily applied by using other similar ATR or prism-coupler configurations, without concern for the sensitivity issues caused by the subtle differences between various configurations. Moreover, the TTR method is also experimentally applied to planar, multimode MIM waveguides. Multimode MIM waveguides, which have larger core sizes, may be of interest for applications in low-loss interconnects or tapered end-couplers. Thanks to the superior angular selectivity of the ATR configuration, the TTR method is capable of detecting the propagation constant and attenuation coefficient of each mode. To the best of the author's knowledge, this is the first time the propagation constant of each mode in a multimode MIM waveguide has been individually measured. Also, to the best of the author's knowledge, this is the first time the attenuation coefficient of each mode in a multimode MIM waveguide has been individually measured. The TTR method is proved to be a reliable, accurate, and straightforward approach to characterize plasmonic modes in MIM waveguides. Future research will target the extension of the TTR method to 2D MIM waveguides, asymmetric MIM waveguides, and inclusion of scattering loss. Taking full advantage of the TTR method, the development of plasmonic devices can be potentially accelerated.