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  • About
  • The Global ETD Search service is a free service for researchers to find electronic theses and dissertations. This service is provided by the Networked Digital Library of Theses and Dissertations.
    Our metadata is collected from universities around the world. If you manage a university/consortium/country archive and want to be added, details can be found on the NDLTD website.
1

Estudo de Mat?rias-Primas do Rio Grande do Norte para Uso em Revestimento Poroso: Influ?ncia do teor de dolomita e temperatura de calcina??o nas propriedades f?sico-mec?nicas / Study of Raw materials of the Rio Grande do Norte for the use in Porous Wall Tile: Influence of the dolomite content and calcinations temperature in the physical- mechanical properties

Silva Neto, Gilson da 04 July 2007 (has links)
Made available in DSpace on 2014-12-17T14:07:23Z (GMT). No. of bitstreams: 1 GilsonSN.pdf: 6365807 bytes, checksum: a479a13345717293c658748ef49aab97 (MD5) Previous issue date: 2007-07-04 / The state of Rio Grande do Norte presents a great potentiality for the production of ceramic tiles because of having natural raw material in quantity and quality making its economical exploration possible, beyond the great energetic differential of the state, the natural g?s. This works aims to study the influence of the dolomite and granulometry concentration and calcinations temperature in the obtaining of formulations for porous coverings which have to be coherent to the project,s specifications. The experiments have involved the physical-chemical and mineralogical characterizations of raw materials and mechanical tests in the dry and burnt proof bodies preceding a mixture experiment planning with the use of the response surface methodology, in order to get the best raw materials combinations to produce a ceramic mass with specific properties. The twelve ceramic masses studied in this work were prepared by the via dry process, characterized, shaped by uniaxial pressing and sinterized in the temperatures of 940?C, 1000?C, 1060?C, 1120?C and 1180?C, using a fast burning cycle. The crystalline phases formed during the sintering in the temperatures in study have revealed the presence of anorthite and diopside beyond quartz with a remaining phase. These phases were the main responsible ones by the physical- mechanical properties of the sinterized proof bodies. The proof bodies after the sintering stage have presented water absorption higher than 10% and a good dimensional stability in all studied temperatures. However, the flexural breaking strength results in the temperatures of 940?C, 1000?C and 1060?C, under the temperature zone of the vitrification of ceramic whiteware do not reach the flexural breaking strength specific for the porous wall tile (15 MPa), but in the temperature of 1120?C next to the vitrification temperature zone, some whiteware ceramic (formulations) has reached the specified value for the porous wall tile. The results of this work have showed that the studied raw materials have great importance for used in the production of porous wall tiles (BIII) / Rio Grande do Norte apresenta uma grande potencialidade para produ??o de revestimento cer?mico, haja vista, possuir mat?rias-primas naturais em quantidade e qualidade possibilitando sua explora??o econ?mica, al?m do grande diferencial energ?tico do Estado, que ? o g?s natural. Este trabalho objetiva estudar a influ?ncia da concentra??o de dolomita, sua granulometria e temperatura de sinteriza??o na obten??o de formula??es para revestimento poroso que atendam as especif?ca??es do projeto. Os experimentos envolveram a caracteriza??o f?sico qu?mico e mineral?gica das mat?rias-primas, e ensaios mec?nicos nos corpos de prova secos e queimados, precedendo-se de um planejamento de experimento de mistura, com o uso da metodologia de superf?cie de resposta, a fim de se obter as melhores combina?oes das mat?rias-primas para produzir massa cer?mica com propriedades especif?cas. As doze massas cer?micas estudadas foram preparadas pelo processo via seca, caracterizadas, conformadas por presagem uniaxial e sinterizadas nas temperaturas de 940?C, 1000?C, 1060?C, 1120?C, e 1180?C, utilizando um ciclo de queima r?pido. As fases cristalina formadas durante a sinteriza??o nas temperaturas em estudo, revelaram a presen?a de anortita e diopsita, al?m de quartzo com fase remanescente. Estas fases foram as principais respons?veis pelas propriedades f?sico-mec?nicas dos corpos de provas sinterizados. As fases cristalina formadas durante a sinteriza??o nas temperaturas em estudo, revelaram a presen?a de anortita e diopsita, al?m de quartzo com fase remanescente. Estas fases foram as principais respons?veis pelas propriedades f?sico-mec?nicas dos corpos de provas sinterizados. Os corpos de prova ap?s sinteriza??o apresentaram absor??o de ?gua superior a 10%, e uma boa estabilidade dimensional em todas as temperaturas estudadas, entretanto, os resultados da tens?o de ruptura ? flex?o nas temperaturas ( 940?C, 1000?C,e1060?C) abaixo da faixa de temperatura de gresifica?ao das massas cer?micas, n?o atigiram o valor de TRF especificado para revestimento poroso(15 MPa), por?m, na temperatura de 1120?C pr?xima da faixa da temperatura de gresifica??o, algumas massas cer?micas (formula??es) j? atingiram o valor especificado para revestimento poroso. Os resultados desse trabalho mostraram que, as mat?rias primas estudadas possuem grande potencial para serem utilizadas na fabrica??o de revestimento poroso (BIII)

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