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Strain Path Effect on Austenite Transformation and Ductility in Q&P 1180 SteelCramer, Jeffrey Grant 01 December 2017 (has links)
The ductility of Q&P 1180 steel was studied with regard to retained austenite transformation under different strain paths. Specimens were tested in uniaxial tension in a standard test frame as well as in situ in the scanning electron microscope (SEM). Then digital image correlation (DIC) was used to compute the effective strain at the level of the individual phases in the microstructure. Stretching experiments were also performed using limiting dome height (LDH) tooling, where specimens were strained in both biaxial and plane strain tension. The experiments were done incrementally, for each strain path, and the retained austenite at each level of strain was measured using electron backscatter diffraction (EBSD). Retained austenite levels in the uniaxial tension case dropped from an initial measured level of about 8% to about 2% during an initial strain increment of 0.02, but then stabilized as the specimen was strained to 0.1. In the plane strain and biaxial tension cases retained austenite also dropped significantly during an initial strain increment of about 0.04, but then continued to decrease as the specimens were strained to failure. Biaxial tension, in particular, was the most effective strain path for transforming retained austenite to martensite, resulting in a final volume fraction of 0.3% at an effective strain of 0.3. Retained austenite in the plane-strain tension case dropped at a faster rate than in the biaxial tension case, but finished at about 1% at a strain of 0.1. The greatest limit strains were seen in the biaxial tension case, which may be partly explained by the more effective conversion of retained austenite than was seen in the uniaxial tension case.
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Microstructural Investigations of Low Temperature Joining of Q&P Steels Using Ag Nanoparticles in Combination with Sn and SnAg as Activating MaterialHausner, Susann, Wagner, Martin Franz-Xaver, Wagner, Guntram 14 February 2019 (has links)
Quenching and partitioning (Q&P) steels show a good balance between strength and ductility due to a special heat treatment that allows to adjust a microstructure of martensite with a fraction of stabilized retained austenite. The final heat treatment step is performed at low temperatures. Therefore, joining of Q&P steels is a big challenge. On the one hand, a low joining temperature is necessary in order not to influence the adjusted microstructure; on the other hand, high joint strengths are required. In this study, joining of Q&P steels with Ag nanoparticles is investigated. Due to the nano-effect, high-strength and temperature-resistant joints can be produced at low temperatures with nanoparticles, which meets the contradictory requirements for joining of Q&P steels. In addition to the Ag nanoparticles, activating materials (SnAg and Sn) are used at the interface to achieve an improved bonding to the steel substrate. The results show that the activating materials play an important role in the successful formation of joints. Only with the activating materials, can joints be produced. Due to the low joining temperature (max. 237 °C), the microstructure of the Q&P steel is hardly influenced.
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