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  • About
  • The Global ETD Search service is a free service for researchers to find electronic theses and dissertations. This service is provided by the Networked Digital Library of Theses and Dissertations.
    Our metadata is collected from universities around the world. If you manage a university/consortium/country archive and want to be added, details can be found on the NDLTD website.
1

Laboratory Analysis of a New Sand Consolidation Material for Oilfield Applications

Filbrandt, Joseph Daniel 2010 December 1900 (has links)
The production of sand can be a major issue in many young, unconsolidated sandstone formations where there is little to no cement holding the individual sand grains together. When such reservoirs are produced, quite often operators face problems with reduced well productivity and equipment failure. Because of these issues, the industry has developed numerous techniques in its effort to control formation sand production. Sand consolidation is one technology that has been studied and used since the 1940s. The theory behind sand consolidation technology is to place a liquid material which will create a grain to grain contact that will bind individual sand grains together. Most consolidation treatments contain a preflush to clean and wet the surface, the consolidating system to bind the sand grains and give residual strength, and, finally, an overflush to ensure the formation is still able to produce fluids. With the successful placement of this fluid, the sand grains will be locked in placed so that they will not be produced. The technology has gone through many phases of conception since the 1940s; however, most consolidation material that is pumped in the past has been based upon an epoxy or furan backbone. While there are many technologies available, for the purpose of my research, the epoxy technology was experimentally investigated. The testing of the fluid involved investigating numerous additives to obtain the correct residual strength of the sample, as well as the necessary retained permeability. For the epoxy fluid, the optimal preflush, epoxy system and overflush formulations were determined after 250 checkout tests. Based upon these tests, the fluid was optimized to its working time and UCS results. The optimal system included the addition of PA2 to the preflush, along with PA1 and an aromatic amine curing agent to the epoxy system. PA1 and PA2 are adhesion promoter additives which were deemed necessary as a result of the testing. This system was then tested further in a HP/HT cell. While there is still room for improvement with respect to retained permeability, the system still performs very well in terms of UCS.
2

Hot alkaline treatment to stimulate and consolidate the heavy oil Bachaquero-01 sand

Valera Villarroel, Cesar Amabilis 17 February 2005 (has links)
An experimental study was conducted to verify experimentally whether sand consolidation by high-temperature alkaline treatment was possible in the heavy oil Bachaquero-01 reservoir. The experiments were conducted using sand samples from a core taken from well LL-231 from Bachaquero-01 reservoir. The sample was placed in a vertical 18 in. long aluminum cylindrical cell with an ID of 1.5 in. The top half of the cell was thermally insulated and the bottom half was cooled. The alkaline treatment (pH 11 -12) at 230ºC - 250ºC and 900 – 1000 psig was injected at 20 ml/min for 3 to 6 hours at the top of the cell and liquid produced at the bottom of the cell. After each experiment, the cell contents were removed and analyzed to determine if consolidation occurred. An electron microprobe was used to analyze both loose and polished epoxy-mounted sand grains to determine any change in texture and composition of the sand pack and precipitation and growth of secondary phases. Results showed that under the experimental conditions reached in the laboratory; the consolidation of Bachaquero-01 sand did not occur. However some secondary materials were produced in the runs where sand samples were cleaned of oil. It was noticed that the amount of these secondary phases was not sufficient to bridge the sand grains. These results indicate that further research is needed to better understand and optimize the parameters affecting the consolidation of Bachaquero-01 sands.

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