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  • About
  • The Global ETD Search service is a free service for researchers to find electronic theses and dissertations. This service is provided by the Networked Digital Library of Theses and Dissertations.
    Our metadata is collected from universities around the world. If you manage a university/consortium/country archive and want to be added, details can be found on the NDLTD website.
1

Obtenção de extrato seco de cumaru pelo processo de secagem em leito de jorro. / Preparation of dry extract of coumaru by the drying process in a spout bed.

MARTINS, Joabis Nobre. 25 September 2018 (has links)
Submitted by Johnny Rodrigues (johnnyrodrigues@ufcg.edu.br) on 2018-09-25T19:26:16Z No. of bitstreams: 1 JOABIS NOBRE MARTINS - DISSERTAÇÃO PPGEA 2013..pdf: 17634552 bytes, checksum: 5a460fe8587a52f6e9b0f9e508d71f27 (MD5) / Made available in DSpace on 2018-09-25T19:26:16Z (GMT). No. of bitstreams: 1 JOABIS NOBRE MARTINS - DISSERTAÇÃO PPGEA 2013..pdf: 17634552 bytes, checksum: 5a460fe8587a52f6e9b0f9e508d71f27 (MD5) Previous issue date: 2013-02 / Capes / As práticas relacionadas ao uso popular de plantas medicinais são o que muitas comunidades têm como alternativa viável para o tratamento de doenças ou manutenção da saúde. Objetivou-se no estudo secar extrato fitoterápico de cumaru pelo processo de leito de jorro, analisando as variáveis dependentes como: rendimento, taxa de acúmulo no material inerte e teor de água do extrato seco. As cascas in natura foram coletadas, secas em estufa com circulação de ar forçado a temperatura de 50 °C até o teor de água de 4,26%, sendo trituradas posteriormente. Em seguida, foi obtido o extrato hidroalcoólico, por meio de maceração dinâmica em álcool a 70% e temperatura de 30 °C, sendo em seguida concentrado em evaporador rotativo à 50 °C até uma concentração de sólidos de 9,8%. Para os ensaios de secagem, foi adicionado como adjuvante de secagem dióxido de silício coloidal ao extrato concentrado. As velocidades de secagem foram definidas em ensaios fluidodinâmicos de acordo com a velocidade de jorro mínimo. Para os ensaios de secagem foram utilizadas partículas de poliestireno do tipo 849, produzido pela EDN, Camaçari - Bahia. Adotou-se um planejamento fatorial de 23 + 3 experimentos no ponto central totalizando 11 experimentos. Como variáveis independentes adotaram-se: temperaturas de secagem de 70, 80 e 90 °C; velocidade do ar de 35,28; 36,60 e 37,93 m/s e vazão de suspensão de alimentação de 4, 5 e 6 mL/min. De acordo com os resultados, os rendimentos variaram de 53,9 a 75,851%; a taxa de acúmulo de 7,91 a 44,761% e o teor de água em base úmida de 2,359 a 5,197%. Os resultados demonstraram que o melhor rendimento foi no experimento 4 (temperatura: 90 °C; V^: 2,86 m3/min e Ws: 4 mL/min) 75,851% com uma taxa de acúmulo de 7,913% e teor de água de 3,901%. O menor rendimento segundo os resultados foi no experimento 6 (Tar: 70 °C; Var: 37,932 m/s e Ws: 6 mL/min) de 60,576%, com taxa de acúmulo de 24,90% e teor de água de 2,359%. Diante o exposto, verifica-se um aumento na taxa de recuperação do extrato seco com o aumento da temperatura de secagem, e consequentemente a diminuição na taxa de acúmulo no material inerte. / The practices related to the popular use of medicinal plants are what many communities have as viable alternative for the treatment of diseases or health maintenance. It was aimed at the study of dry herbal extract of cumaru by spouted bed process, analyzing the dependent variables: income, rate of accumulation in inert material and water content of the dried extract. The fresh shells were collected, dried in an oven with forced air circulation at the temperature of 50C to the water content of 4.26%, being crushed later. Then the hydroalcoholic extract was obtained through dynamic maceration in alcohol at 70% and 30C, and then concentrated on a rotary evaporator to 50 °C up to a concentration of solids of 9.757%. For the drying tests, was added as an adjuvant of colloidal silicon dioxide drying to the concentrated extract. Drying speeds were defined in hydrodynamic tests according to the minimum Jet speed. For the drying tests were used polystyrene particles of type 849, produced by EDN, Camaçari-Bahia. Factorial planning was adopted of 2 + 3 experiments at the center point for a total of 11 experiments. As independent variables were adopted: drying temperatures of 70.80 and 90 °C; air flow rate of 35.278; 36.60 and 37.93 m/s and flow of power suspension of 4, 5 and 6 ml/min. According to the results, yields ranged from 53.9 to 75.851%; the rate of accumulation of 7.913 to 44.761% and water content in wet base of 2.359 to 5.197%. The results showed that the best performance was in experiment 4 (Tar: 90 °C; Var: 2.86 m3/min and Ws: 4 mL/min) 75.851% with a rate of accumulation of 7,91% and water content of 3.901%. The lowest income under the results was the experiment 6 (Tar: 70C; Var: 2.86 m3/min and Ws: 6 mL/min) of 60.576%, with accumulation rate of 24.90% and water content of 2.359%. On the above, there is an increase in the yield of dry extract with increasing drying temperature, and consequently a reduction in the rate of accumulation in inert material.

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