The re-entry space vehicles encounter high temperatures when they enter the earth atmosphere and the high temperature air in the shock layer around the body undergoes partial dissociation. Also, the gas molecules injected into the shock layer from the ablative thermal protection system (TPS) undergo pyrolysis which helps in reducing the net heat flux to the vehicle surface. The chemical species due to the pyrolysis add complexity to the stagnation flow chemistry (52 chemical reactions) models which include species like NOx, CO and hydrocarbons (HCs). Although the ablative TPS is responsible for the safety of re-entry space vehicle, the induced chemical species result in variety of adverse effects on environment such as global warming, acid rain, green house effect etc. The well known three-way-catalyst (TWC) involves simultaneous removal of all the three gases (i.e, NOx, CO, Hydrocarbons) present in the shock layer. Interaction of such three-way-catalyst on the heat shield materials or on the wall of the re-entry space vehicle is to reduce the heat flux and to remove the gases in the shock layer, which is an important issue. For the re-entry vehicle the maximum aerodynamic heating occurs at an altitude ranging about 68 to 45 km during which the vehicle is surrounded by high temperature dissociated air. Then the simplest real gas model of air is the five species model which is based on N2, O2, O, NO and N. This five species model assumes no ionization and no pyrolysis gases are emitted from the heat shield materials. The experimental research work presented in this thesis is directed towards the understanding of catalytic and non-catalytic surface reactions on high temperature materials in presence of strong shock heated test gas. We have also explored the possibility of using shock tube as a high enthalpy device for synthesis of new materials. In the first Chapter, we have presented an overview of re-entry space vehicles, thermal protection system (TPS) and importance of real gas effects in the shock layer. Literature survey on TPS, ablative materials and aerothermochemistry at the stagnation point of reentry capsule, in addition to catalytic and non-catalytic surface reactions between the wall and dissociated air in the shock layer are presented. In Chapters 2 and 3, we present the experimental techniques used to study surface reactions on high temperature materials. A brief description of HST2 shock tunnel is presented and this shock tunnel is capable of generating flow stagnation enthalpies ranging from 0.7 to 5 MJ/kg and has an effective test time of ~ 800 µs. High speed data acquisition system (National Instruments and Yokogawa) used to acquire data from shock tube experiments. The experimental methods like X-ray Photoelectron Spectroscopy (XPS), Scanning Electron Microscopy (SEM), X-ray diffraction (XRD), Raman and FTIR spectroscopy have been used to characterize the shock-exposed materials. Preliminary research work on surface nitridation of pure metals with shock heated nitrogen gas is discussed in Chapter 2. Surface nitridation of pure Al thin film with shock heated N2 is presented in Chapter 3. An XPS study shows that Al 2p peak at 74.2 eV is due to the formation AlN on the surface of Al thin film due to heterogeneous non-catalytic surface reaction. SEM results show changes in surface morphology of AlN film due to shock wave interaction. Thickness of AlN film on the surface increased with the increase in temperature of the shock heated nitrogen gas. However, HST2 did not produce sufficient temperature and pressure to carry out real conditions of re-entry. Therefore design and development of a new high enthalpy shock tunnel was taken up. In Chapter 4, we present the details of design and fabrication of free piston driven shock tunnel (FPST) to generate high enthalpy test gas along with the development of platinum (Pt) and thermocouple sensors for heat transfer measurement. A free piston driven shock tunnel consists of a high pressure gas reservoir, compression tube, shock tube, nozzle, test section and dump tank connected to a vacuum pumping system. Compression tube has a provision to fill helium gas and four ports, used to mount optical sensors to monitor the piston speed and pressure transducer to record pressure at the end of the compression tube when the piston is launched. Piston can attain a maximum speed of 150 m/s and compress the gas inside the compression tube. The compressed gas bursts the metal diaphragm and generates strong shock wave in the shock tube. This tunnel produces total pressure of about 300 bar and temperature of about 6000 K and is capable of producing a stagnation enthalpy up to 45 MJ/kg. The calibration of nozzle was carried out by measuring the pitot tube pressure in the dump tank. Experimentally recorded P5 pressure at end of the shock tube is compared with Numerical codes. Calibrated pressure P5 values are used to calculate the temperature T5 of the reflected shock waves. This high pressure and high temperature shock heated test gas interacts with the surface of the high temperature test materials. For the measurement of heat transfer rate, platinum thin film sensors are developed using DC magnetron sputtering unit. Hard protective layer of aluminum nitride (AlN) on Pt thin film was deposited by reactive DC magnetron sputtering to measure heat transfer rate in high enthalpy tunnel. After the calibration studies, FPST is used to study the heat transfer rate and to investigate catalytic/non-catalytic surface reaction on high temperature materials. In Chapter 5, an experimental investigation of non-catalytic surface reactions on pure carbon material is presented. The pure carbon C60 films and conducting carbon films are deposited on Macor substrate in the laboratory to perform shock tube experiments. These carbon films were exposed to strong shock heated N2 gas in the shock tube portion of the FPST tunnel. The typical shock Mach number obtained is about 7 with the corresponding pressure and temperature jumps of about 110 bar and 5400 K after reflection at end of the shock tube. Shock exposed carbon films were examined by different experimental techniques. XPS spectra of C(1s) peak at 285.8 eV is attributed to sp2 (C=N) and 287.3 eV peak is attributed to sp3 (C-N) bond in CNx due to carbon nitride. Similarly, N(1s) core level peak at 398.6 eV and 400.1 eV observed are attributed to sp3-C-N and sp2-C=N of carbon nitride, respectively. SEM study shows the formation of carbon nitride crystals. Carbon C60 had melted and undergone non-catalytic surface reaction with N2 while forming carbon nitride. Similar observations were made with conducting carbon films but the crystals were spherical in shape. Micro Raman and FTIR study gave further evidence on the formation of carbon nitride film. This experimental investigation confirms the formation of carbon nitride in presence of shock-heated nitrogen gas by non-catalytic surface reaction. In Chapters 6 and 7, we present a novel method to understand fully catalytic surface reactions after exposure to shock heated N2, O2 and Ar test gas with high temperature materials. We have employed nano ZrO2 and nano Ce0.5Zr0.5O2 ceramic high temperature materials to investigate surface catalytic reactions in presence of shock heated test gases. These nano crystalline oxides are synthesized by a single step solution combustion method. Catalytic reaction was confirmed for both powder and film samples of ZrO2. As per the theoretical model, it is known that the catalytic recombination reaction produces maximum heating on the surface of re-entry space vehicles. This was demonstrated in this experiment when a metastable cubic ZrO2 changed to stable monoclinic ZrO2 phase after exposure to shock waves. The change of crystal structure was seen using XRD studies and needle type monoclinic crystal growth with aspect ratio (L/D) more than 15 was confirmed by SEM studies. XPS of Zr(3d) core level spectra show no change in binding energy before and after exposure to shock waves, confirming that ZrO2 does not change its chemical nature, which is the signature of catalytic surface reaction. When a shock heated argon gas interacted with Ce0.5Zr0.5O2 compound, there was a change in colour from pale yellow to black due to reduction of the compound, which is the effect of heat transfer from the shock wave to the compound in presence of argon gas. The reduction reaction shows the release of oxygen from the compound due to high temperature interaction. The XPS of Ce(3d) and Zr(3d) spectra confirm the reduction of both Ce and Zr to lower valent states. The oxygen storage and release capacity of the Ce0.5Zr0.5O2 compound was confirmed by analyzing the reduction of Ce4+ and Zr4+ with high temperature gas interaction. When Ce0.5Zr0.5O2 (which is same as Ce2Zr2O8) in cubic fluorite structure was subjected to strong shock, it changed to pyrochlore (Ce2Zr2O7) structure by releasing oxygen and on further heating it changed to Ce2Zr2O6.3 which is also crystallized in pyrochlore structure by further releasing oxygen. If this heating is carried out in presence of argon test gas, fluorite structure can easily change to pyrochlore Ce2Zr2O6.3 structure, which is a good electrical conductor. Due to its oxygen storage capability (OSC) and redox (Ce4+/Ce3+) properties, Ce0.5Zr0.5O2 had been used as oxygen storage material in three-way-catalyst. Importance of these reactions is that the O2 gas released from the compound will react with gas released from the heat shield materials, like NOx, CO and hydrocarbon (HCs) species which results in reduction of temperature in the shock layer of the re-entry space vehicle. The compound Ce0.5Zr0.5O2 changes its crystal structure from fluorite to pyrochlore phase in presence of shock heated test gas. The results presented in these two Chapters are first of their kind, which demonstrates the surface catalytic reactions. In Chapter 8, we present preliminary results of the oxygen recombination on the surface of heat shield material procured from Indian Space Research Organization (ISRO) used as TPS in re-entry space capsule (Space capsule Recovery Experiment SRE-1) and on thin film SiO2 deposited on silicon substrate. The formation of SiO between the junctions of SiO2/Si was confirmed using XPS study when shock exposed oxygen reacted on these materials. The surface morphology of the ablated SiO2 film was studied using SEM. The damage induced due to impact of shock wave in presence of oxygen gas was analyzed using Focused Ion Beam (FIB) microscope. The results reveal the damage on the surface of SiO2 film and also in the cross-section of the film. We are further investigating use of FIB, particularly related to residual stress developed on thin films due to high pressure and high temperature shock wave interaction. In Chapter 9, conclusions on the performance of FPST, synthesis of high temperature materials, catalytic and non-catalytic surface reactions on the high temperature material due to shock-heated test gases are presented. Possible scope for future studies is also addressed in this Chapter.

One of the characteristics of the high speed ows over blunt bodies is the detached shock formed in front of the body. The distance of the shock from the stagnation point measured along the stagnation streamline is termed as the shock stand o distance or the shock detachment distance. It is one of the most basic parameters in such ows. The need to know the shock stand o distance arises due to the high temperatures faced in these cases. The biggest challenge faced in high enthalpy ows is the high amounts of heat transfer to the body. The position of the shock is relevant in knowing the temperatures that the body being subjected to such ows will have to face and thus building an efficient system to reduce the heat transfer. Despite being a basic parameter, there is no theoretical means to determine the shock stand o distance which is accepted universally. Deduction of this quantity depends more or less on experimental or computational means until a successful theoretical model for its predictions is developed. The experimental data available in open literature for spherical bodies in high speed ows mostly lies beyond the 2 km/s regime. Experiments were conducted to determine the shock stand o distance in the velocity range of 1-2 km/s. Three different hemispherical bodies of radii 25, 40 and 50 mm were taken as test models. Since the shock stand o distance is known to depend on the density ratio across the shock and hence gamma (ratio of specific heats), two different test gases, air and carbon dioxide were used for the experiments here. Five different test cases were studied with air as the test gas; Mach 5.56 with Reynolds number of 5.71 million/m and enthalpy of 1.08 MJ/kg, Mach 5.39 with Reynolds number of 3.04 million/m and enthalpy of 1.42 MJ/kg Mach 8.42 with Reynolds number of 1.72 million/m and enthalpy of 1.21 MJ/kg, Mach 11.8 with Reynolds number of 1.09 million/m and enthalpy of 2.03 MJ/kg and Mach 11.25 with Reynolds number of 0.90 million/m and enthalpy of 2.88 MJ/kg. For the experiments conducted with carbon dioxide as test gas, typical freestream conditions were: Mach 6.66 with Reynolds number of 1.46 million/m and enthalpy of 1.23 MJ/kg. The shock stand o distance was determined from the images that were obtained through schlieren photography, the ow visualization technique employed here. The results obtained were found to follow the same trend as the existing experimental data in the higher velocity range. The experimental data obtained was compared with two different theoretical models given by Lobb and Olivier and was found to match. Simulations were carried out in HiFUN, an in-house CFD package for Euler and laminar own conditions for Mach 8 own over 50 mm body with air as the test gas. The computational data was found to match well with the experimental and theoretical data

Despite years of research in high speed boundary layer flow, there is still a need for insightful experiments to realize key features of the flow like boundary layer response to different conditions and related transition mechanisms. Volumes of data on the these problems point to the fact that there is still much to be understood about the nature of boundary layer instability causing transition and growth of boundary layer in different conditions. Boundary layer stability experiments have been found to be more useful, in which the boundary layer is perturbed and its behavior observed to infer useful conclusions. Also, apart from the stability part, the effect of various changes in boundary layer due to the perturbation makes interesting observation to gain more insight into the understood and the not so understood facets of the same. In view of the above, the effect of a steady axisymmetric thermal bump is investigated on a hypersonic boundary layer over a 60º sharp cone cylinder model. The thermal bump, placed near tip of the cone, perturbs the boundary layer, the behavior of which is observed by recording the wall heat flux on the cone and cylinder surface using platinum thin film sensors. The state of the boundary layer is qualitatively assessed by the wall heat flux comparisons between laminar and turbulent values. The same thermal bump also acts as a heat addition source to boundary layer in which case this recorded data provides a look into the effect of the heat addition to the wall heat flux. To gain a larger view of heat addition causing changes to the flow, effects of change in enthalpy are also considered. Experiments are performed in the IISc HST2 shock tunnel facility at 2MJkg−1 stag-nation enthalpy and Mach number of 8,with and without the thermal bump to form comparisons. Some experiments are also performed in the IISc HST3 free piston driven shock tunnel facility at 6MJkg−1, to investigate the effect of change in stagnation enthalpy on the wall heat flux. To support the experimental results theoretical comparisons and computational studies have also been carried out. The results of experiments show that the laminar boundary layer over the whole model remains laminar even when perturbed by the thermal bump. The wall heat flux measurements show change on the cone part where there seems to be fluctuation in the temperature gradients caused by the thermal bump, which decrease at first and then show an increase towards the base of the cone. The cylinder part remains the same with and without the thermal bump, indicating heavy damping effects by the expansion fan at cone cylinder junction. A local peak in wall heat flux is observed at the junction which is reduced by 64% by the action of the thermal bump. The possible reason for this is attributed to the increased temperature gradients at the wall due to delayed dissipation of heat that is accumulated in the boundary layer as a result of the thermal bump action. The comparison of data for enthalpies of 2MJkg−1 and 6MJkg−1 show that there are negligible real gas effects in the higher enthalpy case and they do not affect the wall heat flux much. Also it is found that the thermal bump fails to dump heat into the flow directly though it creates heat addition virtually by mere discontinuity in the surface temperature and causes temperature gradients fluctuation in the boundary layer. Considering the thermal bump action and the change in stagnation enthalpy of the flow, there seems to be no change in both cases that can be attributed to a common observation resulting from the factor of change in heat inside the boundary layer.

Hypersonic vehicles are exposed to severe heating loads during their flight in the atmosphere. In order to minimize the heating problem, a variety of cooling techniques are presently available for hypersonic blunt bodies. Introduction of a forward-facing cavity in the nose tip of a blunt body configuration of hypersonic vehicle is one of the most simple and attractive methods of reducing the convective heating rates on such a vehicle. In addition to aerodynamic heating, the overall drag force experienced by vehicles flying at hypersonic speeds is predominate due to formation of strong shock waves in the flow. Hence, the effective management of heat transfer rate and aerodynamic drag is a primary element to the success of any hypersonic vehicle design. So, precise information on both aerodynamic forces and heat transfer rates are essential in deciding the performance of the vehicle. In order to address the issue of both forces and heat transfer rates, right kind of measurement techniques must be incorporated in the ground-based testing facilities for such type of body configurations. Impulse facilities are the only devices that can simulate high altitude flight conditions. Uncertainties in test flow conditions of impulse facilities are some of the critical issues that essentially affect the final experimental results. Hence, more reliable and carefully designed experimental techniques/methodologies are needed in impulse facilities for generating experimental data, especially at hypersonic Mach numbers. In view of the above, an experimental program has been initiated to develop novel techniques of measuring both the aerodynamic forces and surface heat transfer rates. In the present investigation, both aerodynamic forces and surface heat transfer rates are measured over the test models at hypersonic Mach numbers in IISc hypersonic shock tunnel HST-2, having an effective test time of 800 s. The aerodynamic coefficients are measured with a miniature type accelerometer based balance system where as platinum thin film sensors are used to measure the convective heat transfer rates over the surface of the test model. An internally mountable accelerometer based balance system (three and six-component) is used for the measurement of aerodynamic forces and moment coefficients acting on the different test models (i.e., blunt cone with after body, blunt cone with after body and frustum, blunt cone with after body-frustum-triangular fins and sharp cone with after body-frustum-triangular fins), flying at free stream Mach numbers of 5.75 and 8 in hypersonic shock tunnel. The main principle of this design is that the model along with the internally mounted accelerometer balance system are supported by rubber bushes and there-by ensuring unrestrained free floating conditions of the model in the test section during the flow duration. In order to get a better performance from the accelerometer balance system, the location of accelerometers plays a vital role during the initial design of the balance. Hence, axi-symmetric finite element modeling (FEM) of the integrated model-balance system for the missile shaped model has been carried out at 0° angle of attack in a flow Mach number of 8. The drag force of a model was determined using commercial package of MSC/NASTRAN and MSC/PATRAN. For test flow duration of 800 s, the neoprene type rubber with Young’s modulus of 3 MPa and material combinations (aluminum and stainless steel material used as the model and balance) were chosen. The simulated drag acceleration (finite element) from the drag accelerometer is compared with recorded acceleration-time history from the accelerometer during the shock tunnel testing. The agreement between the acceleration-time history from finite-element simulation and measured response from the accelerometer is very good within the test flow domain. In order to verify the performance of the balance, tests were carried out on similar standard AGARD model configurations (blunt cone with cylinder and blunt cone with cylinder-frustum) and the results indicated that the measured values match very well with the AGARD model data and theoretically estimated values. Modified Newtonian theory is used to calculate the aerodynamic force coefficient analytically for various angles of attack. Convective surface heat transfer rate measurements are carried out by using vacuum sputtered platinum thin film sensors deposited on ceramic substrate (Macor) inserts which in turn are embedded on the metallic missile shaped body. Investigations are carried out on a model with and without fin configurations in HST-2 at flow Mach number of 5.75 and 8 with a stagnation enthalpy of 2 MJ/kg for zero degree angle of attack. The measured heating rates for the missile shaped body (i.e., with fin configuration) are lower than the predicted stagnation heating rates (Fay-Riddell expression) and the maximum difference is about 8%. These differences may be due to the theoretical values of velocity gradient used in the empirical relation. The experimentally measured values are expressed in terms of normalized heat transfer rates, Stanton numbers and correlated Stanton numbers, compared with the numerically estimated results. From the results, it is inferred that the location of maximum heating occurs at stagnation point which corresponds to zero velocity gradient. The heat-transfer ratio (q1/Qo)remains same in the stagnation zone of the model when the Mach number is increased from 5.75 to 8. At the corners of the blunt cone, the heat transfer rate doesn’t increase (or) fluctuate and the effects are negligible at two different Mach numbers (5.75 and 8). On the basis of equivalent total enthalpy, the heat-transfer rate with fin configuration (i.e., at junction of cylinder and fins) is slightly higher than that of the missile model without fin. Attempts have also been made to evaluate the feasibility of using forward facing cavity as probable technique to reduce the heat transfer rate and to study its effect on aerodynamic coefficients on a 41° apex angle missile shaped body, in hypersonic shock tunnel at a free stream Mach number of 8. The forward-facing circular cavities with two different diameters of 6 and 12 mm are chosen for the present investigations. Experiments are carried out at zero degree angle of attack for heat transfer measurements. About 10-25 % reduction in heat transfer rates is observed with cavity at gauge locations close to stagnation region, whereas the reduction in surface heat transfer rate is between 10-15 % for all other gauge locations (which is slightly downstream of the cavity) compared with the model without cavity. In order to understand the influence of forward facing cavities on force coefficients, measurement of aerodynamic forces and moment coefficients are also carried out on a missile shaped body at angles of attack. The same six component balance is also being used for subsequent investigation of force measurement on a missile shaped body with forward facing cavity. Overall drag reductions of up to 5 % is obtained for a cavity of 6 mm diameter, where as, for the 12 mm cavity an increase in aerodynamic drag is observed (up to about 10%). The addition of cavity resulted in a slight increase in the missile L/D ratio and did not significantly affect the missile lateral components. In summary, the designed balances are found to be suitable for force measurements on different test models in flows of duration less than a millisecond. In order to compliment the experimental results, axi-symmetric, Navier-Stokes CFD computations for the above-defined models are carried out for various angles of attack using a commercial package CFX-Ansys 5.7. The experimental free stream conditions obtained from the shock tunnel are used for the boundary conditions in the CFD simulation. The fundamental aerodynamic coefficients and heat transfer rates of experimental results are shown to be in good agreement with the predicted CFD. In order to have a feeling of the shock structure over test models, flow visualization experiments have been carried out by using the Schlieren technique at flow Mach numbers of 5.75 and 8. The visualized shock wave pattern around the test model consists of a strong bow shock which is spherical in shape and symmetrical over the forebody of the cone. Experimentally measured shock stand-off distance compare well with the computed value as well as the theoretically estimated value using Van Dyke’s theory. These flow visualization experiments have given a factual proof to the quality of flow in the tunnel test section.

One of the major technological innovations that are necessary for faster and cheaper access-to-space will be the commercial realization of supersonic combustion jet engines (SCRAMJET). The establishment of the flow through the inlet is one the prime requirement for the success of a SCRAMJET engine. The flow through a SCRAMJET inlet is dominated by inviscid /viscous coupling, transition, shock-shock interaction, shock boundary layer interaction, blunt leading edge effects and flow profile effects. Although the literature is exhaustive on various aspects of flow features associated with SCRAMJET engines, very little is known on the fundamental gasdynamic features dictating the flow establishment in the SCRAMJET inlet. On one hand we need the reduction of flight Mach number to manageable supersonic values inside the SCRAMJET combustor, but on the other hand we have to achieve this with minimum total pressure loss. Hence the dynamics of ramp/cowl shock interaction process ahead of the inlet has a direct bearing on the quality and type of flow inside the SCRAMJET engine. There is virtually no data base in the open literature focusing specifically on the cowl/ramp shock interactions at hypersonic Mach numbers. Hence in this backdrop, the main aim of the present investigation is to systematically understand the ramp/cowl shock interaction processes in front of a generic inlet model. Since we are primarily concerned with the shock interaction process ahead of the cowl all the investigations are carried out without any fuel injection. Variable geometry is necessary if we want to operate the inlet for a wide range of Mach numbers in actual flight. The investigation mainly comprises of three variable geometry configurations; namely, variation of contraction ratios at 00 cowl (CR 8.4, 5.0 and 4.3), variation of cowl length for a given chamber height (four lengths of cowls at 10 mm chamber height) and variation of cowl angle (three angles cowl each for two chamber heights). The change in cowl configuration results in different ramp/cowl shock interaction processes affecting the performance of the inlet. Experiments are performed in IISc hypersonic shock tunnel HST 2 (test time ~ 1 ms) at two nominal Mach numbers 8.0 and 5.74 for design and off-design testing conditions. Exhaustive numerical simulations are also performed to compliment the experiments. Further the effect of concentrated energy deposition on forebody /cowl shock interactions has also been investigated. A 2D, planar, single ramp scramjet inlet model has been designed and fabricated along with various cowl geometries and tested in a hypersonic shock tunnel to characterize the forebody/cowl shock interaction process for different inlet configurations. Further a DC plasma power unit and a plasma torch have been designed, developed and fabricated to serve as energy source for conducting flow-alteration experiments in the inlet model. The V-I characteristics of the plasma torch is studied and an estimation of plasma temperature is also performed as a part of characterizing the plasma flame. Initial standardization experiments of blunt body flow field alteration using the plasma torch and hence its drag reduction, are performed to check the torch’s suitability to be used as a flow-altering device in a shock tunnel. The plasma torch is integrated successfully with the inlet model in a shock tunnel to perform experiments with plasma jet as the energy source. The above experiments are first of its kind to be conducted in a shock tunnel. They are performed at various pressure ratios and supply currents. Time resolved schlieren flow visualization using Phantom 7.1 (Ms Vision Research USA) high speed camera, surface static pressure measurements inside a generic inlet using miniature kulite transducer and surface convective heat transfer rate measurements inside a generic inlet using platinum thin film sensors deposited on Macor substrate are some of the shock tunnel flow diagnostics that have been used in this study. Some of the important conclusions from the study are: • Experiments performed at different contraction ratios show different shock patterns. At CR 8.4, the SOL condition is satisfied, but the flow gets choked due to over contraction and flow through inlet is not established. For CR 5.0, formation of a small Mach stem before the chamber is observed with the reflection point on the cowl and the weak reflected shock entering inside the chamber. The Mach stem grows with time. For CR 4.3, the forebody/cowl shock interference created an Edney’s Type II shock interaction pattern. However, at off-design conditions, for CR 5 the shock reflection is regular and at CR 4.3, the Edney’s Type II pattern lasts for a short time. • For all lengths of cowl tested, 131mm and 141mm showed Edney’s Type II shock interference where as 151mm showed Edney’s Type I pattern at design condition. In all cases the flow is choked for high contraction ratio. At off-design condition these shock patterns do not last for the entire test time but rather it becomes a lambda pattern with the normal shock before the inlet. • For inlet configurations with cowl angle other than 00, the flow is found to be established for all cases at designed condition and except for 100 cowl at off-design condition. • For CR 8.4 the peak value of pressure (~1.7x104 Pa) occurs at a location of 151mm, where as for CR 5.0 and 4.3 they occur at 188mm and 206mm having values ~1.6x104 Pa and ~1.4x104 Pa respectively. These locations indicate the likely locations of shock impingements inside the chamber. • For cowl angle of 00 for a 10 mm chamber the maximum pressure value recorded is ~1.7x104 Pa whereas for 100 and 200 cowl it is ~1.1x104 Pa and 1.2 x104 Pa respectively. This is because in the first case the inlet is choked because of over contraction whereas in the other two cases the CR is less and flow is established inside the inlet. • The average heat transfer rates of last four heat transfer gauges (180 mm, 190 mm, 200 mm and 210 mm from the forebody tip) for all lengths of cowls tested are found to be almost same (~ 20 W/cm2). This is because the flow is choked in all these cases. The numerical simulation also shows uniform distribution here, consistent with the experimental findings. • The locations of heat transfer peaks for 100 cowl at design condition can be observed to be occurring at 170 mm and 200 mm from the forebody tip having values ~44 W/cm2 and ~39 W/cm2 respectively. For a 200 cowl they seem to be occurring at 170 mm and 180 mm from the forebody tip having values ~50 W/cm2 and ~30 W/cm2. These locations indicate the likely locations of shock impingements inside the chamber. With the evolution of concept of upstream fuel injection in recent times these may the most appropriate locations for fuel injection. • At higher jet pressure ratios the plasma jet/ramp shock interaction results in a lambda shock pattern with the triple point forming vertically above the cowl level. This means the normal shock stands in front of the inlet making a part of the flow entering the inlet subsonic. The reflected shock from the triple point also separates the ramp boundary layer. • At lower jet pressure ratios the triple point is formed below the cowl level and the flow entering inside the inlet is supersonic. The reflected shock interacts with the cowl shock and a weak separation shock is seen. • Experiments are performed with concentrated DC electric discharge as energy source. Even though the amount of energy dumped here is less than 0.25% of the total energy it creates a perceptible disturbance in the flow. • Experiments are also performed to see the effect of electric discharge as energy source on height of Mach stem for a given inlet configuration. Deposition of energy in the present location does not seem to alter the Mach stem height. However more experiments need to be performed by varying the energy location to see its effect. Non-intrusive energy sources like microwave and lasers can be thought of as options for depositing energy to study its effect on Mach stem height. Since they provide more flexibility on varying the location of energy the optimum location of energy can be found out for highest reduction of Mach stem height.

Hypersonic flow is both fascinating and intriguing mainly because of presence of strong entropy and viscous interactions in the flow field. Notwithstanding the tremendous advancements in numerical modeling in the last decade separated hypersonic flow still remains an area where considerable differences are observed between experiments and numerical results. Lack of reliable data base of surface static pressures with good spatial resolution in hypersonic separated flow field is one of the main motivations for the present study. The experiments in hypersonic shock tunnels has an advantage compared to wind tunnels for simulating the total energy content of the flow in addition to the Mach and Reynolds numbers. However the useful test time in shock tunnels is of the order of few milliseconds. Hence in shock tunnel experiments it is essential to have pressure measurement devices which has special features such as small in size, faster response time and the sensors in array form with improved spatial resolutions. Micro Electro Mechanical Systems (MEMS) is an emerging technology, which holds lot of promise in these types of applications. In view of the above requirement, MEMS based pressure sensor array was developed to measure the static pressure distribution. The study is comprised of two parts: one is on the development of MEMS based pressure sensor array, which can be used for hypersonic application and other is on experimental static pressure measurement using MEMS based sensors in separated hypersonic flow over a backward facing step model. Initially a static pressure sensor array with 25 sensors was developed. The static calibration of sensor array was carried out to characterize the sensor array for various characteristic parameters. The preliminary experimental study with cluster of 25 MEMS sensor array mounted on the flat plate did not provide reliable and repeatable results, but gave valuable inputs on the typical problems of using MEMS sensors in short duration hypersonic ground test facilities like shock tunnels. Incidentally, to the best of our knowledge this is first report on use of MEMS based pressure sensors in hypersonic shock tunnel. Later cluster of 5 sensor array was developed with improved electronic packaging and surface finish. The experiments were conducted with flat plate by mounting 5 sensor array shows good agreement in static pressure measurement compared with standard sensors. In the second part of the study a backward facing step model, which simulates the typical gasdynamic flow features associated with hypersonic flow separation is designed. Backward facing step model with step height of 3 mm was mounted with sensor array along the length of model. Just after the step, static pressure measurements were carried out with MEMS sensors. It is important to note that, in the space available in backward facing step model we could mount only one conventional Kulite pressure transducer. The experiments were conducted at Mach number of 6.3 and at stagnation enthalpy of 1.5 MJ/kg in hypersonic shock tunnel (HST-5) at IISc. Based on the static pressure measurement on backward facing step, the location of separation and reattachment points were clearly identified. The static pressure values show that reattachment of flow takes place at about 7 step heights. Numerical simulations were carried out using commercial CFD code, FLUENT for flat plate and backward facing step models to compliment the experiments. The experimental tests results match well with the illustrative numerical simulations results.

The interaction of a shock wave and boundary layer often occurs in high speed flows. For sufficiently strong shock strengths the boundary layer separates, generating shock patterns in the contiguous inviscid flow (termed strong interactions); which may also affect the performances of the systems where they occur, demanding control of the interaction to enhance the performances. The case of impinging shock wave boundary layer interaction is of fundamental importance and can throw light on the physics of the interaction in general. Although various aspects of the interaction are studied at supersonic speeds, the complexities involved in the interaction at hypersonic speeds are not well understood. Of importance is the high total enthalpy associated with hypersonic flows the simulation of which requires shock tunnels. The present experimental study focuses on the interaction between strong impinging shock and boundary layer in hypersonic flows of moderate to high total enthalpies. Experiments are performed in hypersonic shock tunnels HST-2 and FPST (free piston driven shock tunnel), at nominal Mach numbers 6 and 8, with total enthalpy ranging from 1.3 MJ/kg to 6 MJ/kg, and freestream Reynolds number ranging from 0.3 million/m to 4 million/m. The strong impinging shock is generated by a wedge of angle 30.960 to the freestream. The shock is made to impinge on a flat plate (made of Hylem which is adiabatic, except for one case with plate made of aluminium which allows heat transfer). The position of (inviscid) shock impingement may be varied (from 55 mm from the leading edge to 100 mm from the leading edge) by moving the plate back and forth on the fixture which holds the wedge and the plate. Expectedly the strong shock generates a large separation bubble of length comparable to the distance of the location of shock impingement from the leading edge of the plate. Such large separation bubbles are typical of supersonic/hypersonic intakes at off-design operation. The evolution of the flow field- including the evolution of impinging shock and subsequent evolution of the large separation bubble- within the short test duration of the shock tunnels is one of the main concerns addressed in the study. Time resolved schlieren flow visualizations using high speed camera, surface pressure measurements using PCB, kulite and MEMS sensors, surface convective heat transfer measurements using platinum thin film sensors are the flow diagnostics used. From the time resolved visualizations and surface pressure measurements with the fast response sensors, the flow field, even with a separation bubble as large as 75 mm (at Mach 5.96, with shock impingement at 95 mm from the leading edge) was found to be established within the short shock tunnel test time. The effects of various parameters- freestream Mach number, distance of the location of shock impingement, freestream total enthalpy and wall heat transfer- on the interaction are investigated. With increase in Mach number from 5.96 to 8.67, for nearly the same shock impingement locations (95 mm and 100 mm from the leading edge respectively), the separation length decreased from 75 mm to 60 mm despite the fact that the shocks are doubly stronger at the higher Mach number. Inflectional trend in separation length was observed with enthalpy at nominal Mach number 8- separation length increased from 60 mm at 1.6 MJ/kg to 70 mm at 2.4 MJ/kg, and decreased drastically to ~40 mm at 6 MJ/kg (when dissociations are expected). The separation length Lsep for all the experiments, except the experiments at 6 MJ/kg, were found to be large, i.e. comparable with the distance xi of location of shock impingement from the leading edge of the flat plate. The scaled separation length (with Hylem wall) was found to obey the inviscid similarity law proposed from the present study for large separation bubbles with strong impinging shocks, where M∞ is the freestream Mach number, p∞ is the freestream pressure and pr is the measured reattachment pressure; this holds for freestream total enthalpy ranging from 1.3 MJ/kg to 2.4 MJ/kg and Reynolds number (based on location of shock impingement) ranging from 1x105 to 4x105. While the increase in separation length from 1.6 MJ/kg to 2.4 MJ/kg could thus be attributed to the small difference in Mach number between the cases (due to inverse variation with cube of Mach number), the decrease in separation length and the non-confirmation to the proposed similarity law for the 6 MJ/kg case is attributed to the real gas effects. At Mach 6 the flow was observed to separate close to the leading edge, even when the (inviscid) shock impingement was at 95 mm from the leading edge. This prompted the proposal of an approximate inviscid model of the interaction for the Mach 6 case with separation at leading edge, and reattachment at the location of (inviscid) shock impingement; Accordingly, the closer the location of impingement, the more the angle that the separated shear layer makes with the plate and hence more the pressure inside the separation bubble. A small reduction in separation length was also observed with aluminium wall when compared with Hylem wall, emphasizing the importance of wall heat conductivity (especially when concerning separated flows) even within the short test durations of shock tunnels. The free interaction theory over adiabatic wall was found to predict the pressure at the location of separation, but under-predict the plateau pressure (at nominal Mach number 8). Numerical simulations (steady, planar) were also carried out using commercial CFD solver FLUENT to complement the experiments. Simulations using one equation turbulence model (Spalart-Allmaras model) were closer to the experimental results than the laminar simulations, suggesting that the flow field may be transitional or turbulent after separation. Significant reduction of the separation bubble length was demonstrated with the control of the interaction using boundary layer bleed within the short test time of the shock tunnel; with tangential blowing at the separation location20% reduction in separation length was observed, while with suction at separation location the reduction was 13.33 %.

No description available.

Aerodynamic cavities are common features on hypersonic vehicles which are caused in both large and small scale features like surface defects, pitting, gap in joints etc. In the hypersonic regime, the presence of such cavities alters the flow phenomenon considerably and heating rates adjacent to the discontinuities can be greatly enhanced due to the diversion of flow. Since the 1960s, a great deal of theoretical and experimental research has been carried out on cavity flow physics and heating. However, most of the studies have been done to characterize the effect downstream and within the cavity. In the present study, a series of were carried out in the shock tunnel to investigate the heating characteristics, upstream and on the lateral side of the cavity. Heat flux measurement has been done using indigenously developed high resistance platinum thin film gauges. High resistance gauges, as contrary to the conventionally used low resistance gauges were showing good response to the extremely low heat flux values on a flat plate with sharp leading edge. The experimental measurements of heat done on a flat plate with sharp leading edge using these gauges show good match with theoretical relation by Crabtree et al. Flow visualization using high speed camera with the cavity model and shock structures visualized were similar to reported in supersonic cavity flow. This also goes to state that in spite of the fluctuating shear layer-the main feature of hypersonic flow over a cavity ,reasonable studies can be done within the short test time of shock tunnel. Numerical Simulations by solving the Navier-Stokes equation, using the commercially available CFD package FLUENT 13.0.0 has been done to complement the experimental studies.