Castings of aluminum alloys are widely used in the automotive and aerospace industries since they play a significant role in improving the performance and fuel efficiency. In aluminum industries, sampling is the most common method to evaluate the inclusion levels which is a key indicator for the quality of the aluminum alloys. Since how the filling process and solidification process will influence the inclusion characteristics during the sampling procedure is of great importance, the objectives of this work is to create a the two-phase flow model to simulate the filling process and solidification process, as well as calculate the particles movement in the whole sampling procedure. Computational Fluid Dynamics (CFD) modeling was used and this work was performed in the software ANSYS FLUENT. A numerical two dimensional (2D) axisymmetric model was built to simulate the sampling procedure with the assumption that the filling could be done along the main axis automatically. First, the initial solidification during the filling was taken into account without particle injection. The realizable k − ε turbulence model was used to model the effects of the turbulence. Several simulations with different inlet filling rate, different initial filling temperature and different inlet diameter was calculated to see the influence on the solidification behavior. Then, the whole sampling system was modeled with particle injection. The Discrete Phase Model (DPM) was used to simulate the particle motion in the melt and the focus was on the influence of the initial solidification on the inclusion distributions. Finally, the optimal sampling position inside the aluminum sampler mold was calculated. / Gjutningar av aluminiumlegeringar används ofta inom bil-, och flygindustrin eftersom de spelar en viktig roll för att förbättra prestanda och bränsleeffektivitet. Inom aluminiumindustrin är provtagning den vanligaste metoden att utvärdera mängden inneslutningar i smältan, vilket är en nyckelindikator för kvaliteten på aluminiumlegeringarna. Eftersom både fyllnads- och stelningsprocessen kommer att påverka inneslutningskarakteristiken är provtagningsproceduren av stor betydelse. Syftet med detta arbete är att skapa en två-fasflödesmodell för att simulera fyllnings-, och stelningsprocessen, samt att beräkna partikelrörelserna under provtagningsförfarandet. Computational Fluid Dynamics (CFD) modellering användes och arbetet har utfördes med mjukvaran ANSYS FLUENT. En numerisk tvådimensionell (2D) axisymmetrisk modell byggdes för att simulera provtagningsproceduren med antagandet att påfyllningen kan göras automatiskt längs huvudaxeln. Till att börja med betraktades det första stelnandet under fyllningen utan partikelinjektion. En antagen k - ε turbulensmodell användes för att modellera effekten av turbulens. Flera simuleringar med olika inloppshastighet, påfyllningstemperatur och inloppsdiametrar beräknades för att se påverkan på stelningsbeteendet. Därefter modellerades hela provtagningsmodellen med partikelinjektion. En Diskret Fasmodell (DPM) användes för att simulera partikelrörelsen i smältan och fokus var inverkan av det initiala stelnandet på inneslutningsfördelningen. Slutligen beräknades den optimala provtagningspositionen inuti aluminiumprovformen.

Melt convection and solid phase movement play an important role in solidification processes, which significantly influence the formation of grain structures and solute segregations. In general, the melt convection and grain movement are a result of buoyancy forces. The densities within melt are different due to the variation of temperature and concentration, leading to thermally and solutally driven melt convection. Similarly, the density differences between the grains and the bulk melt cause the grain movement, leading to solid sedimentation or grain floating, as the case may be. Free, unattached solid grains are produced by partial remelting and fragmentation of dendrites, by mechanical disturbances such as stirring or vibration and by heterogeneous nucleation of grains in solidification of grain-refined alloys. In this way, movement of solid crystals during solidification can be ascertained in the following two cases. In the first case, during columnar solidification of non-grain-refined alloys, solid movement is possible in the form of dendrite fragments detached from the columnar stalks by the process of remelting and fragmentation. Movement of grains during columnar solidification gives rise to altogether different microstructure from columnar to equiaxed. In the second case, during equiaxed solidification of grain-refined alloys, the movement of solid crystals is possible in the form of equiaxed dendrite crystals nucleated due to presence of grain refiners. The rate and manner by which the free solids settle (or float) will influence macrosegregation in metal castings. Control of the solidification process is possible through an understanding of the solid movement and its effect on macrosegregation and microstructure. With this viewpoint, the overall objective of the present thesis is to study, experimentally and numerically, the phenomenon of solid phase movement during solidification. Through this study, deeper insights of the role of solid phase movement in solidification are developed which can be used for possible control of quality in castings. Both columnar and equiaxed solidification are considered. Models for transport phenomena associated with columnar solidification with solid phase movement are rarely found in the literature, because of inherent difficulty associated with consideration of microscopic features such as remelting and fragmentation. To tackle this problem, solidification modules for remelting and fragmentation are developed first, followed by integration of these molecules in a macroscopic solidification model. A Rayleigh number based fragmentation criterion is developed for detachment of dendrite fragments from the developing mushy zone, which determines the conditions favorable for fragmentation of dendrites. The criterion developed is a function of net concentration difference, liquid fraction, permeability, growth rate of mushy layer, and thermophysical properties of the material. The effect of various solidification parameters on fragmentation is highlighted. The integrated continuum model developed is applied to stimulate the solidification of aqua-ammonia system in a side-cooled rectangular cavity. The numerical results are in good qualitative agreement with those of experiments reported in literature. A gentle ramp of the mushy zone due to settling of solid crystals, as also noticed in experimental literature, is observed towards the bottom of the cavity. The influence of various modeling parameters on solid phase movement and resulting macrosegregation is investigated through a parametric study. Movement of grains during columnar solidification gives rise to altogether different microstructure and sometimes may initiate a morphological transition of the microstructure from columnar to equiaxed if the number and size of equiaxed grains ahead of the columnar front become sufficient to arrest the columnar growth. The generalised model developed, considering solid phase movement during columnar solidification is used to predict columnar-to-equiaxed transition (CET) based on a prescribed cooling rate criterion. It is found that presence of convection significantly affects the solidification behaviour. Moreover, the movement of dendrite fragments and their accumulation at the columnar front further trigger the occurrence of CET. Cooling configuration, too significantly affects the nature of CET. In unidirectional solidification cases, the locations of CET are found to be in a plane parallel to the chill face. However, for the case of the non-unidirectional solidification (as in side-cooled cavity), the locations of CET need not be in a plane parallel to the chill face. In contrast to fixed columnar solidification, equiaxed solidification is poorly understood; in particular, the phenomena associated with solid crystal movement. Movement of unattached solid crystals, formed due to heterogeneous nucleation on grain-refiners, is induced by the convective currents as well as by buoyancy effects, causing the solid to sediment or to float, depending on density of solid compared to that of the bulk melt. While moving in the bulk melt these crystals can also remelt or grow. A series of casting experiments with AI-based alloys are performed to investigate the role and influence of movement of solid crystals on macrosegregation and microstructure evolution during equiaxed solidification. Controlled experiments are designed for studying, separately, settling and floatation of equiaxed crystals for different cooling conditions and configurations. Further, these experiments are carried out in convective and non-convective cases to understand the effect of convection on solid phase movement. Temperature measurements are performed at various locations in the mould during the experiments. After the cavity is solidified, microstructural and chemical analyses of the experimental samples are carried out, several notable features are observed in temperature histories, macrosegregation pattern, and microstructures due to settling/flotation phenomenon of solid crystals. It is found that the flow behavior of solid grains has a profound influence on the progress of solidification (in terms of grain size distribution and fraction eutectic) and macrosegregation distribution. In some cases, the induced flow due to solid phase movement can cause a flow reversal. The observations and quantitative data obtained from experiments, with the help of detailed solidification conditions provided, can be used for future validations of models for equiaxed solidification. Subsequently, numerical studies are carried out, using a modified version of the macroscopic model developed for columnar solidification with motion of solid crystals, to predict the transport phenomena during equiaxed solidification. The model is applied to simulate the solidification processes corresponding to each of the experimental cases performed in this study. For a better understanding of the phenomenon of movement of solid crystals, the following two special cases of solidification are also presented: 1) without movement of solid crystals and 2) movement of solid crystals without any relative velocity between solid and liquid phases. The numerical predictions showing nature of flow field and progress of solidification are substantiated by the experimental data for the thermal analysis, qualitative microstructural Images and quantitative microstructural analysis. It is concluded, with the help of various experiments and simulations, that movement of solid crystals influences the casting quality appreciably, in terms of macrosegregation and microstructures. It is expected that the improved understanding of the role and influence of solid phase movement during solidification processes (both columnar and equiaxed) obtained through this thesis will be useful for possible control of quality of as-cast products.