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The impact of a pipeline by a dropped object has been considered to consist of four distinct impact components: the dropped object, pipeline protection, the soil bed and the pipeline itself. The effect of these components as energy absorbers and the effect on system response has been investigated. Quasi-static and dynamic testing has been earned out to investigate the interaction between the various impact components. Quasi-static testing has been widely used to develop initial predictions, since closer observation of interaction is easier. The validity of applying these predictions to dynamic situations has been addressed using results from dynamic impact testing. The Dropped Object: Two areas have been investigated which address the dropped object within the impact system: the dropped object's impact profile and its deformability. Testing has been carried out to study the effect of typical loading profiles. Research has shown that the dropped object profile significantly effects the pipe response; a cone shaped indentor generates deformation with far less energy than either a wedge or a patch shape. The applicability of a method to predict the interaction between two deforming structures, using a method of shared energy, has been investigated for quasi-static and dynamic loading. During quasi-static testing it was found possible to predict a combined response using individual responses. During dynamic testing prediction was not possible, since inertia effects where found to dominate the response. The Concrete Protective Coating: A programme of work carried out has qualified the role of a pipeline protective coating and assessed the effect of four different types of concrete reinforcement. Summary Although the study has not been exhaustive, it is clear that reinforcements, which hold the concrete coating to the pipe, allow the coating to continue its protection. Fibres added to a concrete mix were found to reduce the damage to the pipe. However mesh reinforcements were found to hold the concrete together most effectively and provided the greatest added protection. The Soil Support: All foundations absorb some energy. Tests have been carried out to investigate the effect of a soil bed on the response of a laterally loaded pipeline. During dynamic tests on sand supported pipes it was noted that no energy was absorbed during the initial deformation, possibly corresponding to local indentation of the pipe wall. After this the sand was seen to react and absorbed a proportion of the energy, depending on the hammer's drop height. The energy absorbed by the soil continued to increase until an energy plateau was reached, after which the soil absorbed no further energy. It was noted that the displacement at which this energy plateau was reached increased as the drop height increased. Two possible causes of the energy plateau have been discussed. The first cause questioned an assumption that the pipe would deform as if on simple supports. The second possible cause suggested a change from dynamic to quasi-static response and investigated the relationship between acceleration, velocity and reaction force. Of the possible causes of the energy plateau, the most likely is thought to be soil related. Investigation into the Deformation of Locally Loaded Pipes: The investigation into pipeline deformation has been carried out using experimental, numerical and theoretical analysis methods. Quasi-static test results have been used to investigate four pipeline parameters and their influence on energy absorbed by the pipeline, (length, L, wall thickness, t, diameter, D and material yield stress, ay). This investigation led to an empirical equation, which brought all energy-displacement (E-8) curves on to a common curve, for a wide range of these variables. This empirical relationship has been developed to predict deformation, for the range of parameters investigated. Dynamic results obtained were normalised using these empirical equations and data was seen to fall into two broad groups, one group comprising seam welded pipe and one group comprising cold drawn pipe. Strain rate effects were proposed as the most likely cause of this bi-grouping. Limitations in the experimentally derived empirical relationship have been identified, resulting from an insufficient range of pipe samples tested.

The purpose of this study is to investigate the behaviour of functionally graded materials in the coating design through analytical and numerical work. Functionally graded materials are advanced composite materials formed from two or more constituents with a continuously varying composition, which results in a continuous variation of material properties from one surface of the material to the other. The concept of functionally graded material is actively explored in coating design where structural and/or functional failures of the coating can happen due to a mismatch between the material properties of the coating and substrate, particularly at the coating/substrate interface. This work focuses on the performance of coated plates with homogeneous and graded coatings under various types of loading to develop a better understanding of their response. Firstly, the three dimensional elasticity solution for an isotropic coated plate with a stiffness gradient in the coating is extended to cover different types of applied loading and then a three dimensional elasticity solution for transversely isotropic materials with gradients in elastic properties is also developed. Based on the extended/developed solutions, a MATLAB code is created to produce a model that would enable the analysis of coated plates for a range of material, geometric and loading parameters. To test the analytical models, a finite element analysis is performed using the commercial finite element software ABAQUS, in which a user material subroutine is employed to generate a gradient in the material properties within each element and increase the accuracy of the results. All the developed analytical and numerical models are then used to carry out a comparative study of three-dimensional stress and displacement fields in the coated plates with homogeneous and graded coatings and establish the effect of various parameters such as coating thickness, coating position, plate dimensions, stiffness gradient, loading distributions and anisotropy on the coated plate response.

Superhydrophobic (SH) surfaces equipped on the skins of natural living beings give them trumps of self-cleaning, anti-bacterial, water harvest, and directional liquid transport, etc., to survive in harsh environments. Bioinspired Superhydrophobic (SH) surfaces have developed many emerging functions, such as self-cleaning, anti-bacterial, water harvest, anti-icing, anti-corrosion, oil-water separation, and many other fascinating functions. However, the implementations of SH coating in real world are still in its infancy, due to (i) the poor performance in the harsh real-world environment and industrial process application, where a multi-level robustness including the mechanical, chemical, and thermal robustness, as well as the strong adherent strength to substrates, is strictly required; (ii) the lack of a technology for facile and mass production. In the light of that any non-perfluorinated component in the formula of an SH coating inevitably generates vulnerable points to the external invasions and the functional applications of SH coatings require control surface topography, we here propose an SH coating entirely made of perfluorinated materials (referred to as Teflon). To achieve this goal, we developed a complete strategy involving material, fabrication, and applications. Firstly, we developed a feasible dynamic soft molding method for the fabrication of three-dimensional (3D) structures. This method paves a road not only to the fabrication of whole-Teflon SH coatings but also to the practical adoption of many other important technologies based on 3D structures. Secondly, we generated whole-Teflon and multi-resist SH coatings by using this method and tightly attached them to different substrates with superior adhering strength surpassing the conventional work. Thirdly, we performed a proof-of-concept demonstration of a roll-to-roll (R2R) hot molding process, which has the potential of translating the lab-scale and plate-to-plate fabrication to industrial mass production. Finally, some fundamental mechanisms and problems of the multifunctional applications in self-cleaning, anti-bacterial fouling, and anti-icing are studied. The outcomes are expected to provide insight understandings on the multifunctional SH coating and move SH coatings toward real-world application.

The Copper Development Association (CDA) has identified over 450 copper alloys registered with the U.S. Environmental Protection Agency (EPA) as antimicrobial. With growing antibiotic resistance, there is a need for copper coatings with increased antimicrobial capability. Cold spray is a high velocity, high deposition rate process that forms dense coatings with little to no oxides or inclusions. It is possible that this process contributes to the increased antimicrobial capability of copper cold spray coatings as compared to other additive processes. The focus of this effort is to understand the effects of powder production and cold spray process parameters on copper cold spray coatings in order to optimize antimicrobial properties. Specifically, this work looks at the differences in conventional and nanomaterial copper cold spray coatings. Materials characterization and test methods show differences in adhesion, microstructure, corrosion, mechanical properties, and surface topography. Materials data is compared against Abaqus FEA software model outputs, and antimicrobial efficacy test data, based on the EPA approved procedure, is used to support materials observations and modelling outputs.

Strawberries are a popular fruit with a pleasing color and flavor. However, its delicate tissue and high sugar content makes it highly perishable with visible mold. In this study, we have attempted to test feasibility of different edible coatings for extending shelf life of ‘Chandler’ strawberries subjected to simulated vibrations of local transportation. Six types of coatings were compared based on the quality of treated berries. Curcumin and limonene were used as natural antimicrobials and coatings were prepared from their liposomes and were over-coated with methyl cellulose. One set of each coating type were subjected to the simulated vibration of local transportation. The vibrated samples had lower shelf life than non-vibrated samples, indicating a robust coating which remains intact during road vibrations is required. Based on the number of berries with visible mold, limonene liposomes showed significantly lower fungal growth compared to the control on the 14th day of storage. Titratable acidity and total phenolic contents were also found to be higher in limonene-coated strawberries compared to other coatings. From the findings, further study of liposome coatings of limonene with different particle size and concentration of the lipid bilayer was necessary to characterize the liposome for an effective application in strawberries. To this regard, another study was done with the aim to develop and characterize alginate and limonene liposomes as edible coating materials and to determine their efficacy in shelf life extension and maintaining quality parameters of ‘Chandler’ strawberries. Alginate solution (1.5% w/v) and limonene liposomes prepared from 80% lecithin and 20% PDA were used as edible coating materials. Fungal decay percentage, total yeast and mold counts, headspace atmosphere analysis, total soluble solids, pH, titratable acidity, total anthocyanin content and total phenolics were analyzed to assess fruit quality during 14 days at 4ºC of storage. Days of storage were found to be significant in maintaining the quality of the strawberries. Among the coating types, strawberries coated limonene liposomes were found to be significantly effective in maintaining the lesser respiration rate, lower the change in pH (3.9), and had higher total anthyocyanin (43.849) content during storage. Thus, limonene liposomes were found to be useful for extending the shelf life and maintaining quality of strawberry fruits.

Typescript (photocopy). / Digitized by Kansas Correctional Industries

Thesis (M.S.)--University of Akron, 2004. / Title from Web page (viewed on Dec. 17, 2007). "August, 2004." Includes bibliographical references (p. 121-127).