This thesis discusses the full scope of a project exploring the physics of hierarchical clusters of interacting nanomagnets. These clusters may be relevant for novel applications such as multilevel data storage devices. The work can be grouped into three main activities: micromagnetic simulation, fabrication and characterization of proof-of-concept prototype devices, and efforts to scale down the structures by creating the hierarchical structures with the aid of diblock copolymer self assembly. Theoretical micromagnetic studies and simulations based on Landau-Lifshitz-Gilbert (LLG) equation were conducted on nanoscale single domain magnetic entities. For the simulated nanomagnet clusters with perpendicular uniaxial anisotropy, the simulation showed the switching field distributions, the stability of the magnetostatic states with distinctive total cluster perpendicular moments, and the stepwise magnetic switching curves. For simulated nanomagnet clusters with in-plane shape anisotropy, the simulation showed the stepwise switching behaviors governed by thermal agitation and cluster configurations. Proof-of-concept cluster devices with three interacting Co nanomagnets were fabricated by e-beam lithography (EBL) and pulse-reverse electrochemical deposition (PRECD). EBL patterning on a suspended 100 nm SiN membrane showed improved lateral lithography resolution to 30 nm. The Co nanomagnets deposited using the PRECD method showed perpendicular anisotropy. The switching experiments with external applied fields were able to switch the Co nanomagnets through the four magnetostatic states with distinctive total perpendicular cluster magnetization, and proved the feasibility of multilevel data storage devices based on the cluster concept. Shrinking the structures size was experimented by the aid of diblock copolymer. Thick poly(styrene)-b-poly(methyl methacrylate) (PS-b-PMMA) diblock copolymer templates aligned with external electrical field were used to fabricate long Ni/Fe magnetic nanowire array, dominant shape anisotropy was observed and compared to the result from previously reported Co nanowire array with strong crystalline anisotropy. Guided diblock copolymer poly(styrene)-b-poly(4-vinyl pyridine) (PS- b-P4VP) self assembly was performed to generate clustered microdomains. Direct e-beam patterning on PS-b-P4VP thin film showed precise and arbitrary patterning on the lateral ordering of the self assembly. Graphoepitaxy of self-assembled PS-b-P4VP copolymers on isolated SiN triangular plateaus successfully resulted in the exact clusters of three microdomains. Theoretical consideration and system modeling based on the micellar configuration of the microdomains were done, and the distribution of the cluster’s size and number of elements were explained qualitatively.

abstract: Microwave circuits are an essential part of technology in the modern day. Everything from cell phone communications, television and radio reception, medical imaging, and radar surveillance depend on microwave circuitry. Constant efforts are being made to introduce new methods of implementing more efficient microwave circuitry while maintaining well known fabrication methods. These improvements typically focus on lower loss, smaller size, and higher operating frequencies [1-6]. This thesis will focus on the specific application of a planar orthomode transducer (OMT) in Home Direct Broadcast (DBS) Systems used in residential satellite receivers. The need for low-loss circuitry becomes increasingly important in the realm of satellite reception, as the carrier to noise levels at the receiver can be as low as 10dB [7]. Interference and loss of signal integrity can occur very easily if the receiving network is not properly designed. This thesis will investigate the design of a planar transmission media that produces ultra-low losses when compared to more conventional planar transmission media. This design, which is called Double Sided Suspended Stripline (DSSL), utilizes air as its primary propagation medium. The design will be similar to standard suspended stripline in geometry, but has signal traces on the top and bottom of the substrate. The traces are connected using plated through-hole vias. This geometry is hugely beneficial because it virtually eliminates one of the major loss mechanisms in classical microwave structures: dielectric loss. This thesis will focus mainly on empirically derived equations and performance metrics obtained through rigorous simulation. / Dissertation/Thesis / Masters Thesis Electrical Engineering 2019

abstract: In this thesis, the synergy between millimeter-wave (mmWave) imaging and wireless communications is used to achieve high accuracy user localization and mapping (SLAM) mobile users in an uncharted environment. Such capability is enabled by taking advantage of the high-resolution image of both line-of-sight (LoS) and non-line-of-sight (NLoS) objects that mmWave imaging provides, and by utilizing angle of arrival (AoA) and time of arrival (ToA) estimators from communications. The motivations of this work are as follows: first, enable accurate SLAM from a single viewpoint i.e., using only one antenna array at the base station without any prior knowledge of the environment. The second motivation is the ability to localize in NLoS-only scenarios where the user signal may experience more than one reflection until it reaches the base station. As such, this proposed work will not make any assumptions on what region the user is and will use mmWave imaging techniques that will work for both near and far field region of the base station and account for the scattering properties of mmWave. Similarly, a near field signal model is developed to correctly estimate the AoA regardless of the user location. This SLAM approach is enabled by reconstructing the mmWave image of the environment as seen by the base station. Then, an uplink pilot signal from the user is used to estimate both AoA and ToA of the dominant channel paths. Finally, AoA/ToA information is projected into the mmWave image to fully localize the user. Simulations using full-wave electromagnetic solvers are carried out to emulate an environment both in the near and far field. Then, to validate, an experiment carried in laboratory by creating a simple two-dimensional scenario in the 220-300 GHz range using a synthesized 13-cm linear antenna array formed by using vector network analyzer extenders and a one-dimensional linear motorized stage that replicates the base station. After taking measurements, this method successfully reconstructs the image of the environment and localize the user position with centimeter accuracy. / Dissertation/Thesis / Masters Thesis Electrical Engineering 2019

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This thesis discusses experimental research and theoretical analysis on exploring the physics and techniques of manipulation of magnetization states of ferromagnetic nanorings in both homogeneous and non-homogeneous applied magnetic field. Magnetization states and their switching processes are fundamental properties of magnetic systems. The ring shape is particularly interesting because of the existence of the closed-flux vortex state, which can be used to encode binary information. The understanding and control of the magnetization switching of ferromagnetic nanorings could lead to new designs of practical magnetic data storage devices. The work in this thesis is grouped into three main activities: theoretical analysis and micromagnetic simulation, fabrication techniques, and characterization of magnetization switching by applied magnetic field. Ferromagnetic rings with different geometric parameters were fabricated by electron beam lithography (EBL), electron beam evaporation and lift-off techniques. EBL patterning on double layer photo resist improved lithography and lift-off resolution. The experiments with applied homogeneous and non-homogeneous fields were able to manipulate the ferromagnetic nanorings through different magnetic configurations. The key accomplishment of this work is we experimentally achieved direct switching between two magnetic vortex states of opposite circulation of magnetization, by using an applied azimuthal (circular) Oersted magnetic field. Such field was generated by applying current through the center of a ring using a platinum atomic force microscopy tip. We used magnetic force microscope imaging to demonstrate the controllability of magnetic switching from onion state to vortex state and for the first time, direct switching between two opposite vortex states. Moreover, we investigated the switching mechanisms associated with nucleation, annihilation, and propagation of domain walls. The magnetic switching properties were found to be sensitive to the ring geometrical parameters. Smaller rings require less circular field to complete the switching than bigger rings. Asymmetric rings require less circular field to complete the switching than symmetric rings with the same dimensions. Theoretical analysis and micromagnetic simulations were conducted on symmetric and asymmetric nanorings, with the purpose of helping us better understand the physics behind the experimental results. Those systematic studies investigated the energy and stability of different magnetization states, the switching field required as a function of the ring geometric designs, as well as switching mechanism and the evolutions among different magnetic states, in both in-plane and azimuthal Oersted magnetic fields. We found the simulations results are in a good agreement with the characterization results.

Photonic lattices consisting of arrays of evanescently coupled waveguides fabricated with precisely controlled parameters have enabled the study of discrete optical phenomena, both classical and quantum, and the simulation of other physical phenomena governed by the same dynamics. In this dissertation, I have experimentally demonstrated transverse Anderson localization of classical light in arrays with off-diagonal coupling disorder and investigated theoretically and experimentally the propagation of entangled photon pairs through such disordered systems. I discovered a new phenomenon, Anderson co-localization, in which a spatially entangled photon pair in a correlated transversally extended state localizes in the correlation space, though neither photon localizes on its own. When the photons of a pair are in an anti-correlated state, they maintain their anti-correlation upon transmission through the disordered lattice, exhibiting Anderson anti-localization. These states were generated by use of parametric down conversion in a nonlinear crystal. The transition between the correlated and anti-correlated states was also explored by using a lens system in a configuration intermediate between imaging and Fourier transforming. In the course of this research, I discovered a curious aspect of light transmission through such disordered discrete lattices. An excitation wave of a single spatial frequency (transverse momentum) is transmitted through the system and is accompanied by another wave with the same spatial frequency but opposite sign, indicating some form of internal reflection facilitated by the disordered structure.

The dissertation is concerned with the design of high-efficiency permanent magnet synchronous machinery and the control system. The dissertation first talks about the basic concept of the permanent magnet synchronous motor (PMSM) design and the mathematics design model of the advanced design method. The advantage of the design method is that it can increase the high load capacity at no cost of increasing the total machine size. After that, the control method of the PMSM and Permanent magnet synchronous generator (PMSG) is introduced. The design, simulation, and test of a permanent magnet brushless DC (BLDC) motor for electric impact wrench and new mechanical structure are first presented based on the design method. Finite element analysis based on the Maxwell 2D is built to optimize the design and the control board is designed using Altium Designer. Both the motor and control board have been fabricated and tested to verify the design. The electrical and mechanical design are combined, and it provides an analytical IPMBLDC design method and an innovative and reasonable mechanical dynamical calculation method for the impact wrench system, which can be used in whole system design of other functional electric tools. A 2kw high-efficiency alternator system and its control board system are also designed, analyzed and fabricated applying to the truck auxiliary power unit (APU). The alternator system has two stages. The first stage is that the alternator three-phase outputs are connected to the three-phase active rectifier to get 48V DC. An advanced Sliding Mode Observer (SMO) is used to get an alternator position. The buck is used for the second stage to get 14V DC output. The whole system efficiency is much higher than the traditional system using induction motor.

Liquid crystal (LC) has been widely used for displays, spatial light modulators, variable optical attenuators (VOAs) and other tunable photonic devices. The response time of these devices is mainly determined by the employed liquid crystal material. How to obtain fast response for the LC devices is a fundamentally important and technically challenging task. In this dissertation, we investigate several methods to improve liquid crystal response time, for examples, using dual-frequency liquid crystals, polymer stabilized liquid crystals, and sheared polymer network liquid crystals. We discover a new class of material, denoted as sheared polymer network liquid crystal (SPNLC) which exhibits a submillisecond response time. First, dual-frequency liquid crystals and polymer network methods are demonstrated as examples for the variable optical attenuators. Variable optical attenuator (VOA) is a key component in optical communications. Especially, the sheared PNLC VOA shows the best result; its dynamic range reaches 43 dB while the response time is in the submillisecond range at 1550 nm wavelength, which is 50 times faster than the commercial LC-based VOA. Second, we report a new device called axially-symmetric sheared polymer network liquid crystals (AS-SPNLC) and use it as LC devices. An axially-symmetric sheared polymer network liquid crystal has several attractive features: 1) it is polarization independent, 2) it has gradient phase change, and 3) its response time is fast. It can be used for polarization converter and divergent LC lens. In addition, a new method for simultaneously measuring the phase retardation and optic axis of a compensation film is demonstrated using an axially-symmetric sheared polymer network liquid crystal. This simple technique can be used for simultaneously measuring the optic axis and phase retardations of both A- and C-plates. These compensation films have been used extensively in wide-view LCD industry. Therefore, this method will make an important impact to the LCD industry.

Aside from energy, light carries linear and angular momenta that can be transferred to matter. The interaction between light and matter is governed by conservation laws that can manifest themselves as mechanical effects acting on both matter and light waves. This interaction permits remote, precise, and noninvasive manipulation and sensing at microscopic levels. In this dissertation, we demonstrated for the first time a complete set of opto-mechanical effects that are based on nonconservative forces and act at the interface between dielectric media. Without structuring the light field, forward action is provided by the conventional radiation pressure while a backward movement can be achieved through the natural enhancement of linear momentum. If the symmetry of scattered field is broken, a side motion can also be induced due to the transformation between spin and orbital angular momenta. In experiments, these opto-mechanical effects can be significantly amplified by the long-range hydrodynamic interactions that provide an efficient recycling of energy. These unusual opto-mechanical effects open new possibilities for efficient manipulation of colloidal microparticles without having to rely on intricate structuring or shaping of light beams. Optically-controlled transport of matter is sought after in diverse applications in biology, colloidal physics, chemistry, condensed matter and others. Another consequence of light-matter interaction is the modification of the optical field itself, which can manifest, for instance, as detectable shifts of the centroids of optical beams during reflection and refraction. The spin-Hall effect of light (SHEL) is one type of such beam shifts that is due to the spin-orbit transformation governed by the conservation of angular momentum. We have shown that this effect can be amplified by the structural anisotropy of random nanocomposite materials.

The main purpose of this dissertation to investigate photophysical properties, third order nonlinearity and free carrier absorption and refraction in organic materials and semiconductors. Special emphasis of this dissertation is on characterization techniques of molecules with enhanced intersystem crossing rate and study of different approaches of increasing triplet quantum yield in organic molecules. Both linear and nonlinear characterization methods are described. Linear spectroscopic characterization includes absorption, fluorescence, quantum yield, anisotropy, and singletoxygen generation measurements. Nonlinear characterization, performed by picosecond and femtosecond laser systems (single and double pump-probe and Z-scan measurements), includes measurements of the triplet quantum yields, excited-state absorption, two-photon absorption, nonlinear refraction and singlet and triplet-state lifetimes. The double pump-probe technique is a variant of the standard pump-probe method but uses two pumps instead of one to create two sets of initial conditions for solving the rate equations allowing a unique determination of singlet- and triplet-state absorption parameters and transition rates. The advantages and limitations of the the double pump-probe technique are investigated theoretically and experimentally, and the influences of several experimental parameters on its accuracy are determined. The accuracy with which the double pump-probe technique determines the triplet-state parameters improves when the fraction of the population in the triplet state relative to the ground state is increased. Although increased accuracy is in iv principle achievable by increasing the pump fluence in the reverse saturable absorption range, it is shown that the DPP is optimized by working in the saturable absorption regime. Two different approaches to increase intersystem crossing rates in polymethine-like molecules are presented: traditional heavy atom substitution and molecular levels engineering. Linear and nonlinear optical properties of a series of polymethine dyes with Br- and Se- atoms substitution, and a series of new squaraine molecules, where one or two oxygen atoms in a squaraine bridge are replaced with sulfur atoms, are investigated. A consequence of the oxygento-sulfur substitution in squaraines is the inversion of their lowest lying ππ* and nπ* states leading to a significant reduction of singlet-triplet energy difference and opening of an additional intersystem channel of relaxation. Experimental studies show that triplet quantum yields for polymethine dyes with heavy-atom substitutions are small (not more than 10%), while for sulfurcontaining squaraines these values reach almost unity. Experimental results are in agreement with density functional theory calculations allowing determination of the energy positions, spinorbital coupling, and electronic configurations of the lowest electronic transitions. For three different semiconductors: GaAs, InP and InAsP two photon absorption, nonlinear refraction and free carrier absorption and refraction spectrums are measured using Zscan technique. Although two photon absorption spectrum agrees with the shape of theoretical prediction, values measured with picosecond system are off by the factor of two. Nonlinear refraction and free carrier nonlinearities are in relatively good agreement with theory. Theoretical values of the third order nonlinearities in GaAs are additionally confirmed with femtosecond Z-scan measurements. v Due to large spectral bandwidth of femtosecond laser, three photon absorption spectrum of GaAs was additionally measured using picosecond Z-scan. Again, spectral shape is in excellent agreement with theory however values of three photon absorption cross sections are larger than theory predicts.