The article at hand presents a novel approach to accelerating the early strength development of mineralimpregnated carbon-fibre composites (MCF) by electrical Joule heating. MCF were produced with a metakaolin-based geopolymer suspension and subsequently cured using Ohmic heating under systemically varied voltages and durations. The MCF produced were characterised in respect of their mechanical and morphological properties. Threepoint-bending and uniaxial tension tests yielded significant enhancement of MCF mechanical properties due to curing within only a few hours. Thermogravimetric analysis (TGA), mercury intrusion porosimetry (MIP), environmental scanning electron microscope (ESEM) as well as micro-computed tomography (μCT) confirmed advanced geopolymerisation by the electrical heating process and a strong sensitivity to parameter selection. After only two hours of resistance heating MCF could demonstrate tensile strength of up to 2800 MPa, showing the great potential for applying the Joule effect as a possibility to enhance the strength development of geopolymer-based MCF. Moreover, the applied method offers a huge potential to manufacture automated fast out-of-oven cured MCF with a variety of shapes and dimensions.

One major step needed for fusion to become a reliable energy source is the development of materials for the extreme conditions (high temperature, radioactivity and erosion) caused by hot plasmas. The main goal of the present study is to use and optimise ion beam methods (lateral resolution and sensitivity) to characterise the distribution of hydrogen isotopes that act as fuel. Materials from the test reactors JET (Joint European Torus), TEXTOR (Tokamak Experiment for Technology Oriented Research) and Tore Supra have been investigated. Deuterium, beryllium and carbon were measured by elastic recoil detection analysis (ERDA) and nuclear reaction analysis (NRA). To ensure high 3D spatial resolution a nuclear microbeam (spot size <10 µm) was used with 3He and 28Si beams. The release of hydrogen caused by the primary ion beam was monitored and accounted for. Large variations in surface (top 10 µm) deuterium concentrations in carbon fibre composites (CFC) from Tore Supra and TEXTOR was found, pointing out the importance of small pits and local fibre structure in understanding fuel retention. At deeper depths into the CFC limiter tiles from Tore Supra, deuterium rich bands were observed confirming the correlation between the internal material structure and fuel storage in the bulk. Sample cross sections from thick deposits on the JET divertor showed elemental distributions that were dominantly laminar although more complex structures also were observed. Depth profiles of this kind elucidate the plasma-wall interaction and material erosion/deposition processes in the reactor vessel. The information gained in this thesis will improve the knowledge of first wall material for the next generation fusion reactors, concerning the fuel retention and the lifetime of the plasma facing materials which is important for safety as well as economical reasons.

Rapid prototyping has in the last few years gained an ever increasing central role in projects thanks to its agile benefits. Because of that, boundaries regarding what can be accomplished can be pushed and new techniques for achieving goals can be explored at a reasonable cost. A challenge that remains though, is to be able to prototype rapidly with advanced materials such as fibre composites, in a cost effective and reliable manner. The Maritime Robotics Laboratory at KTH Royal Institute of Technology is developing an unmanned fixed-wing aerial vehicle that is also submersible and takes off from the water surface. The design for the craft is completely novel in order to meet the necessary requirements.  The goal of this master's thesis is to assist with the design of the craft in order to ensure its manufacturability. When the design was finished, a structural analysis of said design was performed, utilizing finite element software. This ensured that the correct amount of material was used, where it was needed. Lastly, and the main scope of this thesis, is the manufacture of the components which make up the craft. Several options were considered during the manufacturing process, like vacuum infusion and prepreg due to the varying size and complexity of all the components which are to be manufactured.  More conventional materials (such as medium density fibreboard) was decided upon when manufacturing the molds for the main airframe of the craft due to its sheer size. The method which was decided upon for building all auxiliary components was to use inexpensive 3D-printed polylactic acid molds, coated with glass fibre reinforce adhesive polytetrafluoroethylene film, in conjunction with a low-temperature prepreg. The trials eventually turned out successful and the components which were built using this technique came out according to their specified dimensions that were provided and in accordance to the structural analysis which was conducted. This is promising for rapid prototyping in where only entry-level composites manufacturing equipment is accessible. / "Rapid prototyping" (Snabb prototyptillverkning) har under de senaste åren fått en allt mer central roll i projekt tack vare dess agila fördelar. På grund av detta kan gränser för vad som kan åstadkommas tänjas på och nya tekniker för att uppnå mål kan undersökas till en rimlig kostnad. En utmaning som dock kvarstår är att snabbt kunna ta fram prototyper med avancerade material som fiberkompositer på ett kostnadseffektivt och pålitligt sätt. Maritime Robotics Laboratory vid KTH utvecklar en drönare som är nedsänkbar under vatten och lyfter från vattenytan. Designen för detta är helt ny för att uppfylla den önskade kravspecifikation. Målet med detta examensarbetet är att hjälpa till med utformningen av drönaren för att säkerställa dess tillverkbarhet. Designarbetet omfattar en strukturanalys med användning av finita elementmetoder. Detta för att säkerställa att rätt mängd material används där det behövs. Slutligen, och huvuduppgiften för detta projekt, är tillverkningen av de komponenter som utgör drönaren. Flera alternativ övervägdes under tillverkningsprocessen, som vakuuminjektion och prepreg på grund av den varierande storleken och komplexiteten hos alla komponenter som ska tillverkas. Mer konventionella material (som t.ex. medium density fibre, fiberspånskiva) valdes vid tillverkning av formarna för drönarens skrov på grund av dess stora storlek. Metoden som beslutades för att bygga alla hjälpkomponenter var att använda billiga 3D-printade polylaktid-formar, belagda med glasfiberarmerade självhäftande polytetrafluoreten-film, i kombination med en lågtemperatur prepreg. Försöken blev så småningom framgångsrika och komponenterna som byggdes med dessa metoder blev producerade enligt deras angivna dimensioner som gavs och i enlighet med den strukturella analys som utfördes. Detta är lovande för snabb prototyping där utrustning för produktion med kompositmaterial är begränsad till inträdesnivå.

A key challenge facing the nuclear fusion community is how to design a reactor that will operate in environmental conditions not easily reproducible in the laboratory for materials testing. Finite element analysis (FEA), commonly used to predict components’ performance, typically uses idealised geometries. An emerging technique shown to have improved accuracy is image based finite element modelling (IBFEM). This involves converting a three dimensional image (such as from X ray tomography) into an FEA mesh. A main advantage of IBFEM is that models include micro structural and non idealised manufacturing features. The aim of this work was to investigate the thermal performance of a CFC Cu divertor monoblock, a carbon fibre composite (CFC) tile joined through its centre to a CuCrZr pipe with a Cu interlayer. As a plasma facing component located where thermal flux in the reactor is at its highest, one of its primary functions is to extract heat by active cooling. Therefore, characterisation of its thermal performance is vital. Investigation of the thermal performance of CFC Cu joining methods by laser flash analysis and X ray tomography showed a strong correlation between micro structures at the material interface and a reduction in thermal conductivity. Therefore, this problem leant itself well to be investigated further by IBFEM. However, because these high resolution models require such large numbers of elements, commercial FEA software could not be used. This served as motivation to develop parallel software capable of performing the necessary transient thermal simulations. The resultant code was shown to scale well with increasing problem sizes and a simulation with 137 million elements was successfully completed using 4096 cores. In comparison with a low resolution IBFEM and traditional FEA simulations it was demonstrated to provide additional accuracy. IBFEM was used to simulate a divertor monoblock mock up, where it was found that a region of delamination existed on the CFC Cu interface. Predictions showed that if this was aligned unfavourably it would increase thermal gradients across the component thus reducing lifespan. As this was a feature introduced in manufacturing it would not have been accounted for without IBFEM.The technique developed in this work has broad engineering applications. It could be used similarly to accurately model components in conditions unfeasible to produce in the laboratory, to assist in research and development of component manufacturing or to verify commercial components against manufacturers’ claims.