The matrix-fiber stress transfer in glass/epoxy composite materials was studied using analytical and experimental methods. The mathematical model that was developed calculates the stress fields in the fiber, interphase, and neighboring matrix near a fiber break. This scheme takes into account the elastic-plastic behavior of both the matrix and the interphase, and it includes the treatment of stress concentration near the discontinuities of the fibers. The radius of the fibers and the mechanical properties of the matrix were varied in order to validate the mathematical model. The computed values for the lengths of debonding, plastic deformation, and elastic deformation in the matrix near the fiber tip were confirmed by measurements taken under polarized light on loaded and unloaded single fiber samples. The fiber-fiber interaction was studied experimentally using dog-bone samples that contained seven fibers forming an hexagonal pattern. / Master of Science

Submitted in fulfilment of the requirements for the degree of Master of Engineering: Mechanical Engineering, Department of Mechanical Engineering, Faculty of Engineering and the Built Environment, Durban University of Technology, Durban, South Africa. 2017. / In this study, the fatigue life of fiber reinforced composite (FRC) materials system was investigated. A nano-filler was used to increase the service life of the composite structures under cyclical loading since such structures require improved structural integrity and longer service life. Behaviour of glass fiber reinforced composite (GFRC) enhanced with various weight percentages (1 to 5 wt. %) of Cloisite 30B montmorillonite (MMT) clay was studied under static and fatigue loading. Epoxy clay nanocomposite (ECN) and hybrid nanoclay/GFRC laminates were characterised using differential scanning calorimetry (DSC) and dynamic mechanical analysis (DMA). The mechanical properties of neat GFRC and hybrid nanoclay/GFRC laminates were evaluated. Fatigue study of the composite laminates was conducted and presented using the following parameter; matrix crack initiation and propagation, interfacial debonding, delamination and S–N relationship. Residual strength of the materials was evaluated using DMA to determine the reliability of the hybrid nanoclay/GFRC laminates. The results showed that ECN and hybrid nanoclay/GFRC laminates exhibited substantial improvement in most tests when compared to composite without nanoclay. The toughening mechanism of the nanoclay in the GFRC up to 3 wt. % gave 17%, 24% and 56% improvement in tensile, flexural and impact properties respectively. In the fatigue performance, less crack propagations was found in the hybrid nanoclay/GFRC laminates. Fatigue life of hybrid nanoclay/GFRC laminate was increased by 625% at the nanoclay addition up to 3 wt. % when compared to neat GFRC laminate. The residual strength of the composite materials revealed that hybrid nanoclay/GFRC showed less storage modulus reduction after fatigue. Likewise, a positive shift toward the right was found in the tan delta glass transition temperature (Tg) of 3 wt. % nanoclay/GFRC laminate after fatigue. It was concluded that the application of nanoclay in the GFRC improved the performance of the material. The hybrid nanoclay/GFRC material can therefore be recommended mechanically and thermally for longer usage in structural application. / M

The ability to predict potential strength degradation of a filament wound sphere was developed using an incremental finite element model of the composite during fabrication. The sphere was modeled taking into account the winding/loading pattern and the resulting internal layer boundaries. The thickness profile of the sphere's layers were computed using a thickness profile/pattern simulation program. This thickness profile was used by the mesh generating program to ensure that the elements generated did not cross , layer boundaries. The elements used were four noded isoparametric quadrilateral elements and these were collapsed to triangular elements for transitions. The input to the finite element program was prepared by an interface program which combines the mesh generator output with the loading and option control data. The main feature of the finite element program was the incremental construction and loading of the model. Strength degradation definitely occurs when the average fiber layer strain is negative. The negative strain means that all the winding tension has been lost from the layer and the fibers in uncured resin will buckle when they try to support compressive loading. Then when the resin cures the buckled region of fibers are degraded in strength. This model gives a layer-by-layer analysis of the potential strength loss of the composite. / Ph. D.

No description available.

Filament wound composite structures are becoming more and more attractive to designers in the aircraft and aerospace industries due to increasing strength- and stiffness-to-weight ratios and falling fabrication costs. However, the interaction of some of the manufacturing process variables such as mandrel stiffness and thickness, winding tension and pattern, and cure cycle characteristics can lead to common defects such as delamination, matrix cracking and fiber buckling. A model of the filament winding process was developed to better understand the behavior of wound structures during fabrication. Specifically, the residual stress state at the end of winding, heat-up and cool-down was determined. This information is important because adverse stress states are the mechanism through which the process variables cause fabrication defects. The process model utilized an incremental finite-element analysis to simulate the addition of material during winding. Also, the model was refined and extended to include changes that occur in the material behavior during the cure. A fabrication analysis was performed for an 18 in. (457 mm) graphite/epoxy filament wound bottle. Two different mandrel models were examined, a rigid steel and a soft sand/rubber mandrel. At the end of winding, the composite layers in the model retained all of their initial winding tension for the steel mandrel but did exhibit significant loss of tension for the sand/rubber mandrel. The composite layers experienced a large increase in tension during heating for the steel mandrel but showed no significant recovery of tension for the sand/rubber system. / M.S.

Thesis (M.Tech.: Mechanical Engineering)-Dept. of Mechanical Engineering, Durban University of Technology, 2007 xvi, 123 leaves / Interlaminar cracking or delamination is an inherent disadvantage of composite materials. In this study the fracture properties of nano and fibre-reinforced polypropylene and epoxy composite structures are examined. These structures were subjected to various tests including Single Edge Notched Bend (SENB) and Mixed Mode Bending (MMB) tests. Polypropylene nanocomposites infused with 0.5, 1, 2, 3 and 5 weight % nanoclays showed correspondingly increasing fracture properties. The 5 weight % specimen exhibited 161 % improvement in critical stress intensity factor (KIC) over virgin polypropylene. XRD and TEM studies show an increase in the intercalated morphology and the presence of agglomerated clay sites with an increase in clay loading. The improvement in KIC values may be attributed to the change in structure. Tests on the fibre-reinforced polypropylene composites reveal that the woven fibre structure carries 100 % greater load and exhibits 275 % lower crack propagation rate than the chopped fibre specimen. Under MMB conditions, the woven fibre structure exhibited a delamination propagation rate of 1.5 mm/min which suggests delamination growth propagates slower under Mode I dominant conditions. The woven fibre / epoxy structure shows 147 % greater tensile modulus, 63 % greater critical stress intensity factor (KIC), and 184 % lower crack propagation rate than the chopped fibre-reinforced epoxy composite. MMB tests reveal that the load carrying capability of the specimens increased as the mode-mix ratio decreased, corresponding to an increase in the Mode II component. Delamination was through fibre–matrix interface with no penetration of fibre layers. A failure envelope was developed and tested and may be used to determine the critical applied load for any mode-mix ratio. The 5 weight % nanocomposite specimen exhibited a greater load carrying capability and attained a critical stress intensity factor that was 10 % less than that of the fibre-reinforced polypropylene structure, which had three times the reinforcement weight. Further, the nanocomposite exhibited superior strain energy release rates to a material with ten times the reinforcement weight. The hybrid structure exhibited 27 % increase in tensile modulus over the conventional fibre-reinforced structure. Under MMB conditions, no significant increase in load carrying capability or strain energy release rate over the conventional composite was observed. However, the hybrid structure was able to resist delamination initiation for a longer period, and it also exhibited lower delamination propagation rates.

Thesis (M.Tech.: Mechanical Engineering)-Dept. of Mechanical Engineering, Durban University of Technology, 2007 xvi, 123 leaves / Interlaminar cracking or delamination is an inherent disadvantage of composite materials. In this study the fracture properties of nano and fibre-reinforced polypropylene and epoxy composite structures are examined. These structures were subjected to various tests including Single Edge Notched Bend (SENB) and Mixed Mode Bending (MMB) tests. Polypropylene nanocomposites infused with 0.5, 1, 2, 3 and 5 weight % nanoclays showed correspondingly increasing fracture properties. The 5 weight % specimen exhibited 161 % improvement in critical stress intensity factor (KIC) over virgin polypropylene. XRD and TEM studies show an increase in the intercalated morphology and the presence of agglomerated clay sites with an increase in clay loading. The improvement in KIC values may be attributed to the change in structure. Tests on the fibre-reinforced polypropylene composites reveal that the woven fibre structure carries 100 % greater load and exhibits 275 % lower crack propagation rate than the chopped fibre specimen. Under MMB conditions, the woven fibre structure exhibited a delamination propagation rate of 1.5 mm/min which suggests delamination growth propagates slower under Mode I dominant conditions. The woven fibre / epoxy structure shows 147 % greater tensile modulus, 63 % greater critical stress intensity factor (KIC), and 184 % lower crack propagation rate than the chopped fibre-reinforced epoxy composite. MMB tests reveal that the load carrying capability of the specimens increased as the mode-mix ratio decreased, corresponding to an increase in the Mode II component. Delamination was through fibre–matrix interface with no penetration of fibre layers. A failure envelope was developed and tested and may be used to determine the critical applied load for any mode-mix ratio. The 5 weight % nanocomposite specimen exhibited a greater load carrying capability and attained a critical stress intensity factor that was 10 % less than that of the fibre-reinforced polypropylene structure, which had three times the reinforcement weight. Further, the nanocomposite exhibited superior strain energy release rates to a material with ten times the reinforcement weight. The hybrid structure exhibited 27 % increase in tensile modulus over the conventional fibre-reinforced structure. Under MMB conditions, no significant increase in load carrying capability or strain energy release rate over the conventional composite was observed. However, the hybrid structure was able to resist delamination initiation for a longer period, and it also exhibited lower delamination propagation rates.

It has been known that the nucleation and growth of cracks and defects dominate the fatigue damage process in brittle or quasi-brittle materials, such as woven fabric composites and concrete. The behaviors of these materials under multiaxial tensile or compression fatigue loading conditions are quite complex, necessitating a unified approach based on principles of mechanics and thermodynamics that offers good predictive capabilities while maintaining simplicity for robust engineering calculations. A unified approach has been proposed in this dissertation to simulate the change of mechanical properties of the woven fabric composite and steel fiber reinforced concrete under uniaxial and biaxial fatigue loading. The boundary surface theory is used to describe the effect of biaxial fatigue loading. A fourth-order response tensor is used to reflect the high directionality of the damage development, and a second-order response tensor is used to describe the evolution of inelastic deformation due to damage. A direction function is used to capture the strength anisotropic property of the woven fabric composite. The comparisons between model prediction results and experimental data show the good prediction capability of models proposed in this dissertation.

A dissertation submitted to the Faculty of Engineering and the Built Environment, University of the Witwatersrand, Johannesburg, in fulfilment of the requirements for the degree of Master of Science in Engineering. Johannesburg, October 2017 / This research looks into the manufacturing process of complex geometries using continuous fibre reinforced thermoplastics (CFRTP). The purpose of this work was to develop methods that will enable the production of defect free complex components. This was achieved by investigating the key process parameters in the CFRTP manufacturing process, and optimizing them in order to improve the quality of components. The investi- gations were performed with the aid of software making use of the finite element method, and this was found to be instrumental in predicting the formability of geometries. The re- search showed that the formability of complex geometry is largely determined by the ability of the laminate to be draped into the required geometry. The forming mechanisms that take place during the draping process can be linked to the formation of defects where draping is unsuccessful. The study also showed that the quality of the drape can be influenced by blank and tool design factors. It was also shown that the blank can be manipulated using a restraint mechanism to improve the formability of geometries. The effect of processing parameters such as forming speed, forming pressure and tool temperature were also investigated. The research resulted in the formulation of guidelines to follow when manufacturing CFRTP components. The developments that were made were successfully implemented to improve the formability of a complex component that had previously been difficult to form without defects. / MT2018