Thesis (Ph. D.)--University of Wisconsin, 1967. / Typescript. Vita. eContent provider-neutral record in process. Description based on print version record. Includes bibliography.

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Thesis (M. Sc.)--University of Canterbury, 2006. / Typescript (photocopy). Includes bibliographical references (p. 109-111). Also available via the World Wide Web.

This thesis details the design and construction of an experiment to measure the radial distribution of laser gain in a cylindrical Helium-Neon laser gain tube. This distribution is important as it can effect the transverse mode structure of a running ring laser. Earlier theoretical models of the distribution were not supported by high quality experimental data and fail to take into account some physical processes. A resolution of 8 parts per million in gain and 50 μm in radial position has been achieved. Gain distributions have been measured and are shown to be well modeled by a 0th order Bessel function with first roots at the tube walls and a central dip depending on excitation power; except for the region very near to the tube walls where a very rapid increase in gain has been observed. Hydrogen has been identified by spectroscopic analysis as the primary constituent of gas contamination and cause of the long term reduction in gain of large ring lasers. Additional work has been done to detect a proposed non-classical Lense-Thirring field around a spinning lead superconductor. It was found that any effect is at least 20 times smaller than predicted. Techniques and tools for data acquisition programming have been reviewed focusing on difficulties with coupling of user interface and application logic, monolithicity, difficulties with scripting and algorithm implementation.

This thesis details the design and construction of an experiment to measure the radial distribution of laser gain in a cylindrical Helium-Neon laser gain tube. This distribution is important as it can effect the transverse mode structure of a running ring laser. Earlier theoretical models of the distribution were not supported by high quality experimental data and fail to take into account some physical processes. A resolution of 8 parts per million in gain and 50 μm in radial position has been achieved. Gain distributions have been measured and are shown to be well modeled by a 0th order Bessel function with first roots at the tube walls and a central dip depending on excitation power; except for the region very near to the tube walls where a very rapid increase in gain has been observed. Hydrogen has been identified by spectroscopic analysis as the primary constituent of gas contamination and cause of the long term reduction in gain of large ring lasers. Additional work has been done to detect a proposed non-classical Lense-Thirring field around a spinning lead superconductor. It was found that any effect is at least 20 times smaller than predicted. Techniques and tools for data acquisition programming have been reviewed focusing on difficulties with coupling of user interface and application logic, monolithicity, difficulties with scripting and algorithm implementation.

Thesis (Ph. D.)--Ohio University, June, 2004. / Includes bibliographical references (leaves 194-200).

Made available in DSpace on 2014-10-09T12:53:06Z (GMT). No. of bitstreams: 0 / Made available in DSpace on 2014-10-09T13:58:57Z (GMT). No. of bitstreams: 0 / Tese (Doutoramento) / IPEN/T / Instituto de Pesquisas Energeticas e Nucleares - IPEN/CNEN-SP

Made available in DSpace on 2014-10-09T12:53:06Z (GMT). No. of bitstreams: 0 / Made available in DSpace on 2014-10-09T13:58:57Z (GMT). No. of bitstreams: 0 / O colágeno é a forma funcional de um oligômero biológico, cujos monômeros são aminoácidos quirais. Tecidos ricos em colágeno são estruturas opticamente anisotrópicas, birrefringentes e não-lineares. O objetivo deste trabalho foi caracterizar o colágeno tipo I não irradiado e após irradiação com laser de He-Ne polarizado, utilizando a microscopia de polarização para investigação da birrefringência, e a geração de segundo harmônico (GSH) para análise da susceptibilidade não-linear. Doze ratos Wistar foram divididos em quatro grupos, de acordo com as idades: 34, 48, 62 e 76 dias. Os grupos receberam, respectivamente, 1; 5; 9 e 13 irradiações de D= 1J/cm2, durante 46s, no tendão de Aquiles que, aleatoriamente, foi escolhido ser o direito ou esquerdo. Os animais foram então sacrificados e os tendões extraídos para a preparação das amostras. Para a microscopia de polarização foram obtidos cortes com 8μm de espessura, e as birrefringências de forma e intrínseca foram avaliadas. Para a GSH foi utilizado um laser de Ti:Safira (150fs) com 76MHz de taxa de repetição, diâmetro do feixe φ= 40μm, comprimento de onda central λ= 800nm e Δλ= 10nm e Pp= 110mW. Um polarizador linear foi posicionado no caminho do feixe. Duas objetivas foram utilizadas para focalizar e coletar a radiação incidente e emergente da amostra, respectivamente. Um analisador, também linear, foi introduzido logo após a objetiva coletora. Um filtro absorvedor na faixa infravermelha do espectro eletromagnético, mas transmissor na faixa azul, foi utilizado para garantir que apenas λ= 400nm era medido. A razão, ρ, entre dois tensores de hiperpolarizabilidade independentes foi estudada. As amostras irradiadas apresentaram maior birrefringência (Δn) e maior susceptibilidade não-linear (ρ), em comparação com as não irradiadas. Estes resultados indicam que o laser de He-Ne polarizado alinha as fibrilas de colágeno ao longo eixo do tendão. / Tese (Doutoramento) / IPEN/T / Instituto de Pesquisas Energeticas e Nucleares - IPEN/CNEN-SP

In der vorliegenden Arbeit werden anhand der Edelgaszusammensetzung von Kimberliten und Lamproiten sowie ihrer gesteinsbildenden Minerale die Wechselwirkungen dieser Gesteine mit Fluiden diskutiert. Die untersuchten Proben stammen vom östlichen Baltischen Schild, vom Kola-Kraton (Poria Guba und Kandalaksha) und vom karelischen Kraton (Kostamuksha). Edelgasanalysen nach thermischer oder mechanischer Gasextraktion von 23 Gesamtgesteinsproben und 15 Mineralseparaten ergeben folgendes Bild: Helium- und Neon-Isotopendaten der Fluideinschlüsse von Lamproiten aus Kostamuksha lassen auf den Einfluss einer fluiden Phase krustaler Herkunft schliessen. Diese Wechselwirkungen fanden wahrscheinlich schon während des Magmenaufstiegs statt, denn spätere Einflüsse krustaler Fluide auf die Lamproite und ihr Nebengestein (Quarzit) sind gering, wie anhand der C/³⁶Ar-Zusammensetzung gezeigt wird. Auch sind die mit verschiedenen Datierungsmethoden (Rb-Sr, Sm-Nd, K-Ar) an Mineralseparaten und teilweise an Gesamtgestein ermittelten Alter konsistent und machen eine metamorphe Überprägung unwahrscheinlich. Aufgrund der Verteilung der primordialen Edelgasisotope zwischen Fluideinschlüssen und Gesteinsmatrix ist ein langsamer Magmenaufstieg anzunehmen, was die Möglichkeit der Kontamination mit einem krustalen Fluid während des Magmenaufstiegs erhöht.<br /> <br>Die Gasextraktion aus Mineralseparaten erfolgte thermisch, wodurch eine Freisetzung der Gase ausschließlich aus Fluideinschlüssen nicht möglich ist. Hierbei zeigen Amphibol und Klinopyroxen, separiert aus Kostamuksha-Lamproiten, in ihrer Neon-Isotopenzusammensetzung im Vergleich zur krustalen Zusammensetzung (Kennedy et al., 1990) ein leicht erhöhtes Verhältnis von ²⁰Ne/²²Ne, was ein Hinweis auf Mantel-Neon sein könnte. Kalifeldspäte, Quarz und Karbonate enthalten dagegen nur Neon krustaler Zusammensetzung. Phlogopite haben sehr kleine Verhältnisse von ²⁰Ne/²²Ne und ²¹Ne/²²Ne, zurückzuführen auf in-situ-Produktion von ²²Ne in Folge von U- und Th-Zerfallsprozessen.<br><br /> Wie unterschiedliche thermische Entgasungsmuster für ⁴⁰Ar und ³⁶Ar zeigen, ist ³⁶Ar in Fluideinschlüssen konzentriert. Das ⁴⁰Ar/³⁶Ar-Isotopenverhältnis der Fluideinschlüsse von Lamproiten aus Kostamuksha ist antikorreliert mit der durch thermische Extraktion bestimmten Gesamtmenge an ³⁶Ar. Argon aus Fluideinschlüssen setzt sich daher aus zwei Komponenten zusammen: Einer Komponente mit atmosphärischer Argon-Isotopenzusammensetzung und einer krustalen Komponente mit einem Isotopenverhältnis ⁴⁰Ar/³⁶Ar > 6000. Diffusion von radiogenem ⁴⁰Ar aus der Kristallmatrix in die Fluideinschlüsse spielt keine wesentliche Rolle.<br /> <br>Kimberlite aus Poria Guba und Kandalaksha zeigen anhand der Helium- und z. T. auch der Neon-Isotopenzusammensetzung eine Mantelkomponente in den Fluideinschlüssen an. Bei einem angenommenen ²⁰Ne/²²Ne-Isotopenverhältnis von 12,5 in der Mantelquelle ergibt sich ein ²¹Ne/²²Ne-Isotopenverhältnis von 0,073 ± 0,011 sowie ein ³He/⁴He-Isotopenverhältnis, welches im Vergleich zum subkontinentalem Mantel (Dunai und Baur, 1995) stärker radiogen geprägt ist. Solche Isotopensignaturen sind mit höheren Konzentrationen an Uran und Thorium in der Mantelquelle der Kimberlite zu erklären.<br /> <br>Rb-Sr- und Sm-Nd-Altersbestimmungen erfolgten von russischer Seite (Belyatskii et al., 1997; Nikitina et al., 1999) und ergeben ein Alter von 1,23 Ga für den Lamproitvulkanismus in Kostamuksha. Eigene K-Ar-Datierungen an Phlogopiten und Kalifeldspäten stimmen mit einem Alter von 1193 ± 20 Ma fast mit den Rb-Sr- und Sm-Nd-Altern überein. Die K-Ar-Datierung an einem Phlogopit aus Poria Guba, separiert aus dem Kimberlit PGK 12a, ergibt ein Alter von 396 Ma, ebenfalls in guter Übereinstimmung mit Rb-Sr-und Sm-Nd-Altern (ca. 400 Ma, Lokhov, pers. Mitteilung). K-Ar-Altersbestimmungen an Gesamtgestein aus Poria Guba erbrachten kein schlüssiges Alter. Die Rb-Sr- und Sm-Nd-Alter des Lamproitmagmatismus in Poria Guba betragen 1,72 Ga (Nikitina et al., 1999).<br /> <br>Vergleiche von gemessenen mit berechneten Edelgaskonzentrationen aus in-situ-Produktion zeigen weiterhin, dass in Abhängigkeit vom Alter der Probe Diffusionsprozesse stattgefunden haben, die zu unterschiedlichen und z. T. erheblichen Verlusten an Helium und Neon führten. Diffusionsverluste an Argon sind dagegen kaum signifikant. Unterschiedliche Diffusionsverluste in Abhängigkeit von Alter und betrachtetem Edelgas zeigen auch die primordialen Edelgase. / In the present thesis, interactions of kimberlites and lamproites as well as their constituent minerals with fluids are discussed based on noble gas compositions. The samples originate from the eastern Baltic Shield, more specifically from the Kola craton (Poria Guba and Kandalaksha) and the Karelia craton (Kostamuksha). Gas was extracted by stepwise heating and crushing from 23 whole rock samples and 15 mineral separates. These two techniques allow differential extraction of gas from fluid inclusions (crushing technique) and from the bulk sample (stepwise heating). The noble gas analyses provide the following information:</P> <P>Helium and neon isotopic compositions of fluid inclusions in lamproites reveal the presence of a crustal fluid phase. Fluid interaction probably ocurred already during the process of magma ascent. Interaction after lamproite emplacement seems unlikely. The lamproites and their host rock differ in the degree of fluid-rock interaction, as demonstrated by the C/³⁶Ar composition. In addition, various dating methods (Rb-Sr, Sm-Nd, K-Ar) yield almost the same age within analytical error. Thus, a metamorphic overprint can be excluded. The distribution of primordial noble gases between fluid inclusions and crystal lattice suggests a relatively slow magma ascent, making an interaction of the lamproitic magma with crustal fluids even more likely. Since noble gases from mineral separates were extracted only by the stepwise heating method, gases stored in fluid inclusions could not be released separately.</P> <P>Amphibole and clinopyroxene separates yielded a higher ²⁰Ne/²²Ne ratio in comparison to crustal composition (Kennedy et al., 1990). This presumably is an indication of a mantle derived fluid phase. On the other hand, neon isotopic composition of K-feldspar, quartz and carbonate separates are indistinguishable from the crustal composition. In comparison to other mineral separates, phlogopite yields very low ratios of ²⁰Ne/²²Ne and ²¹Ne/²²Ne due to in situ production of ²²Ne, which is a result of nuclear reactions.</P> <P>The distinct thermal gas release patterns of ⁴⁰Ar and ³⁶Ar indicates that ³⁶Ar is concentrated in fluid inclusions. The ⁴⁰Ar/³⁶Ar isotopic ratio in fluid inclusions shows a negative correlation with the total amount of ³⁶Ar released by thermal extraction. Therefore, argon from fluid inclusions is a simple 2-component mixture of air and a crustal component with an ⁴⁰Ar/³⁶Ar ratio > 6000. It can be shown that diffusion of ⁴⁰Ar from the matrix into fluid inclusions is negligible.</P> <P>In contrast to lamproites, whole rock kimberlite samples from Poria Guba and Kandalaksha show clear evidence in helium and, to a certain extentalso in neon isotope ratios, of interaction with a mantle derived fluid phase. Assuming a ²⁰Ne/²²Ne ratio of 12.5 for the mantle endmember, a ²¹Ne/²² Ne ratio of 0.073 ± 0.011 can be calculated. Likewise, the resulting ³He/⁴He ratio is more strongly influenced by radiogenic helium in comparison to the mean subcontinental mantle (Dunai und Baur, 1995). Such behaviour reflects higher concentrations of uranium and thorium in the magma source of kimberlites than the subcontinental mantle.</P> <P>Rb-Sr and Sm-Nd age determinations (Belyatskii et al., 1997; Nikitina et al., 1999) yield 1.23 Ga for the lamproite magmatism in Kostamuksha. K-Ar dating of phlogopite and K-feldspar provides similar ages (1.19 Ga). K-Ar dating of a single phlogopite separate from the Kimberlite sample PGK12a from Poria Guba, yields an age of 396 Ma which corresponds well with Rb-Sr and Sm-Nd ages.</P> <P>Depending on sample age, distinct and partly extensive diffusive loss of helium and neon has occurred, as shown by comparison of measured and calculated concentrations of in situ produced isotopes. Diffusion loss is negligible for argon. This is also strongly supported by primordial noble gas composition.