Os tubos de Geradores de Vapor em Reatores Nucleares do tipo PWR são submetidos a diferentes níveis de tensões e carregamento em altas temperaturas, reduzindo sua vida útil devido o surgimento de defeitos e corrosão. A inspeção por Correntes Parasitas é um ensaio não destrutivo usado para diagnosticar defeitos de corrosão e descontinuidades na superfície externa e interna em tubos de trocadores de calor. Esses tubos estão sujeitos a danos por diferentes mecanismos de degradação mecânica e química, tais como trincas por fadiga e corrosão sob tensão. Os sinais de inspeção por Correntes Parasitas são afetados por diferentes ruídos dificultando sua análise pelo inspetor. Esse trabalho apresenta os resultados da análise dos sinais de Correntes Parasitas usando a Transformada de Hilbert-Huang (THH) funcionando como filtro de ruídos (De-noising), como uma técnica alternativa de processamento e análise de sinais. A Transformada de Hilbert-Huang teve esse nome atribuído pela agência espacial norte-americana (NASA) para o resultado da reunião de dois processos, um método de decomposição empiricamente modal (Empirical Mode Decomposition EMD), seguido da análise espectral de Hilbert (Hilbert Spectral Analysis HSA). Os sinais de inspeção por correntes parasitas possuem características de transiente, não estacionário e não linear. A transformada de Hilbert-Huang aplicada neste trabalho forneceu dois recursos alternativos em processamento de sinais; o pré-processamento que funcionou como filtro de ruídos, e outro de análise de sinais, responsável pela identificação das características tempo-frequência-energia do sinal. / The nuclear power plant steam generator tubes are subjected to different levels of stress and loading at high temperatures, reducing its lifetime due to the development of defects and corrosion. The Eddy Current Testing (ECT) is a nondestructive testing used to diagnose defects of corrosion and discontinuities in the inner and outer surface of heat exchanger tubes. These tubes are subject to failure by different mechanisms of chemical and mechanical degradation such as fatigue and stress corrosion crack. The ECT signals are affected by different noises making the analysis a difficult task to the inspector. This dissertation presents the results of the main characteristics from the ECT signals using the Hilbert-Huang Transform (HHT) as an alternative method for the processing and signal analysis. The Hilbert-Huang Transform has its name given by the American National Aeronautics and Space Administration, NASA, as the result of Empirical Mode Decomposition (EMD) and the Hilbert Spectral Analysis (HSA) methods. The Eddy Current signals are transient, nonstationary and nonlinear. The Hilbert-Huang Transform applied in this work provided two alternative proceedings in signal processing, one in signal pre-processing acting as noise filter (De-noising) and another as signal analysis, which identifies the characteristics of signal time-frequency-energy.

Superligas à base de níquel vêm sendo extensivamente utilizadas em diversas aplicações nas indústrias devido ao excelente comportamento mecânico e anticorrosivo. No entanto, essas ligas possuem certas particularidades que levam à necessidade de desenvolvimento de técnicas de inspeção e caracterização metalúrgica, como forma de garantir a integridade estrutural dos componentes fabricados com essas ligas. Neste trabalho, a técnica de correntes parasitas foi aplicada à superligas à base de níquel com duas propostas distintas: 1) Em um primeiro momento foi realizado o estudo da evolução microestrutural da liga Inconel 718 durante o processo de envelhecimento através da combinação do ensaio por correntes parasitas, análise de difração de raios-X, análise metalográfica, medidas de dureza e tamanho de grão. As medidas foram realizadas em amostras submetidas a diferentes ciclos de tratamentos térmicos variando entre 620-1035°C. Os resultados mostraram que as diferentes microestruturas do Inconel 718 têm efeitos distintos na condutividade elétrica quando medidos através da técnica de correntes parasitas. A influência da microestrutura na condutividade pode ser mostrada sendo devido à competição de dois efeitos sobre o espalhamento de elétrons: a purificação da matriz e a morfologia, distribuição e tamanho dos precipitados. A combinação dos valores de dureza e condutividade elétrica provou ser uma forma rápida e prática de determinar o nível de envelhecimento da liga; 2) Em um segundo momento foi desenvolvido um processo de otimização de sensores através de modelagem por elementos finitos (MEF). Através de uma metodologia de otimização, os parâmetros de construção e operação de um sensor foram otimizados para inspeção de defeitos superficiais e subsuperficiais esperados em materiais cladeados com Inconel 625. O sensor com a geometria ótima foi construído e testado a fim de verificar a eficiência do processo de otimização. Uma ótima correlação entre os resultados numéricos e experimentais foi encontrada e o sensor ótimo se mostrou eficiente na inspeção de pequenos defeitos superficiais e subsuperficiais na liga Inconel 625 quando operado nas frequências apropriadas. / Nickel-based superalloys have been extensively used in various industries due to its unique mechanical and corrosion behavior. However, these alloys show particular characteristics which lead to the need for specific inspection and metallurgical characterization techniques in order to ensure the structural integrity of components manufactured from these alloys. In this work , the eddy current technique was applied to nickel-base superalloys with two aims: 1 ) Firstly, the microstructural evolution of Inconel 718 during aging processes has been studied through a combination of eddy current testing, X-ray diffraction analysis, metallography, hardness and grain size measurements. Measurements were carried out in samples subjected to different heat treatment cycles between 620-1035°C. Results show that different microstructures of Inconel 718 have a distinguishable effect on electrical conductivity when this is measured through an appropriately sensitive technique (i.e. eddy current testing). The influence of microstructure on conductivity could be shown to be due to the competition between two effects on the scattering of electrons: matrix purification and precipitate size, distribution and morphology. A combination of hardness values and electrical properties proved to be a fast and practical way of determining the stage of aging of the alloy; 2) An optimization method of eddy current sensor design was developed through finite element modeling (FEM). Through a methodology of optimization, the construction and operation parameters of the sensor were optimized for inspection of superficial and subsuperficial defect, commonly found in weld overlay Inconel 625 claddings. A prototype of this sensor with the optimum geometry was built and tested on blocks identical to those considered in the models in order to verify the efficiency of the optimization process. A very good agreement between numerical and experimental results was found. Moreover, the optimal sensor was efficient to detect small surface and subsurface defects in Inconel 625 when operated at appropriate frequencies.

While evaluating the depth of corrosive defect through Remote Field Eddy Current (RFEC) Testing technology, the researcher tried to investigate the signals of supporting plate which may produce variations by the thickness of supporting plate, diameter of tube hole in supporting plate, the value of crevice between tube and tube hole and tube wall thickness. Errors of evaluation of defect depth may consequently be identified or measured by the variations of the support plate signal. This study explores the effects of above four factors by experiments and an analysis of variance in statistics. By the analysis of experimental results, the researcher found the four influential factors would cause angle deviation of supporting plate signals. Except the factor of tube wall thickness, the deviation is not so substantial that the difference of evaluation in depth was consequently fallen into an acceptable range of engineering practices. When utilizing the remote field eddy current testing technique to test inservice tubes, the researcher found the thickness of inservice tube is normally different from the specified thickness of a standard tube. This variation consequently resulting in an evaluation curve produced by a standard tube may not lead to proper assessment of defects in inservice tube. To deal with the problem many researchers used a frequency compensation method to compensate for the evaluation error contributed by the variation of tube thickness on the basis of the standard ASTM E2096-00(2000). But the use of the frequency compensation method did not measure the inservice tube thickness and thus produced a drawback of consuming much time for the adjustment steps of compensation. Therefore, a mathematical compensation method was introduced in this study for the compensation of thickness variation derived from skin depth theory. This method in the present experiment is proven to be both feasible and reasonable through the derivation of the methodology. Generally, this study aims to apply the mathematical compensation method to overcome the drawback of frequency compensation method and to solve the problem of the difficulty in measuring inservice tube wall thickness in heat exchanger bundles.

In this research, in order to realize such nanolaminated magnetic cores for high frequency and high power conversion, the following key tasks have been accomplished: 1) electrodeposition of metallic alloy materials such as NiFe, CoNiFe, and anisotropic CoNiFe; 2) development of new fabrication technologies to realize nanolaminated cores based on metallic alloy electrodeposition; 3) reliable characterization of the structural, magnetic, and electrical properties of the nanolaminated metallic alloy cores; 4) development of microfabricated inductor windings to integrate the nanolaminated cores; 5) demonstration of high-frequency and high-flux ultracompact DC-DC power conversion using inductors integrated with nanolaminated metallic alloy cores. By achieving these tasks, nanolaminated cores comprising tens to hundreds of layers of metallic alloy films (Ni80Fe20 and Co44Ni37Fe19) has been developed. The fabricated nanolaminated core consists of sufficiently thin nanolaminations (100 – 1000 nm) that can suppress eddy currents in the MHz range, while simultaneously achieving the overall magnetic thickness (35 – 2000 µm) such that substantial power can be handled. The nanolaminated metallic alloy cores were further integrated into microfabricated inductors using CMOS-compatible fabrication processes. Finally, an ultracompact DC-DC buck converter with the nanolaminated metallic alloy cores has been developed on PCB having footprint of 14 × 7.1 mm2. The input voltage of the converter varied from 30 to 70 V and the output voltage was fixed at 20 V. The converter operated with output power of approximately 11 W and the switching frequencies of 0.7 – 1.4 MHz, demonstrating conversion efficiency of 94.2% at 30 V input and 80.8% at 60 V input.

We consider the problem of extracting a specific feature from a noisy signal generated by a multi-channels Remote Field Eddy Current Sensor. The sensor is installed on a mobile robot whose mission is the detection of anomalous regions in metal pipelines. Given the presence of noise that characterizes the data series, anomaly signals could be masked by noise and therefore difficult to identify in some instances. In order to enhance signal peaks that potentially identify anomalies we consider an entropy filter built on a-posteriori probability density functions associated with data series. Thresholds based on the Neyman-Pearson criterion for hypothesis testing are derived. The algorithmic tool is applied to the analysis of data from a portion of pipeline with a set of anomalies introduced at predetermined locations. Critical areas identifying anomalies capture the set of damaged locations, demonstrating the effectiveness of the filter in detection with Remote Field Eddy Current Sensor.

This thesis presents a method for optimizing cable configuration inside a large magnetic cylindrical steel casing, from the total ampacity point of view. The method is comprised of two main parts, namely: 1) analytically calculating the electromagnetic losses in the steel casing and sheathed cables, for an arbitrary cables configuration, and 2) implementing an algorithm for determining the optimal cables configuration to obtain the best total ampacity. The first part involves approximating the eddy current and hysteresis losses in the casing and cables. The calculation is based on the theory of images, which this thesis expands to apply to casings having both high magnetic permeability and high electric conductivity at the same time. The method of images, in combination with approximating the cable conductors and sheaths as multiple physical filaments, is used to compute the final current distributions in the cables and pipe and thus the associated losses. The accuracy of this computation is assessed against numerical solutions obtained using the Maxwell finite element program by Ansoft. Next, the optimal cable configuration is determined by applying a proposed two-level optimization algorithm. At the outer level, a combinatorial optimization based on a genetic algorithm explores the different possible configurations. The performance of every configuration is evaluated according to its total ampacity, which is calculated using a convex optimization algorithm. The convex optimization algorithm, which forms the inner level of the overall optimization procedure, is based on the barrier method. This proposed optimization procedure is tested for a duct bank installation containing twelve cables and fifteen ducts, comprising two circuits and two cables per phase, and compared with a brute force method of considering all possible configurations. The optimization process is also applied to an installation consisting of a single circuit inside a large magnetic steel casing.

Made available in DSpace on 2014-10-09T12:46:54Z (GMT). No. of bitstreams: 0 / Made available in DSpace on 2014-10-09T14:09:44Z (GMT). No. of bitstreams: 1 09057.pdf: 12808764 bytes, checksum: 970b3a8c12068b9ea0e88948bbcda318 (MD5) / Tese (Doutoramento) / IPEN/T / Instituto de Pesquisas Energeticas e Nucleares - IPEN/CNEN-SP

Superligas à base de níquel vêm sendo extensivamente utilizadas em diversas aplicações nas indústrias devido ao excelente comportamento mecânico e anticorrosivo. No entanto, essas ligas possuem certas particularidades que levam à necessidade de desenvolvimento de técnicas de inspeção e caracterização metalúrgica, como forma de garantir a integridade estrutural dos componentes fabricados com essas ligas. Neste trabalho, a técnica de correntes parasitas foi aplicada à superligas à base de níquel com duas propostas distintas: 1) Em um primeiro momento foi realizado o estudo da evolução microestrutural da liga Inconel 718 durante o processo de envelhecimento através da combinação do ensaio por correntes parasitas, análise de difração de raios-X, análise metalográfica, medidas de dureza e tamanho de grão. As medidas foram realizadas em amostras submetidas a diferentes ciclos de tratamentos térmicos variando entre 620-1035°C. Os resultados mostraram que as diferentes microestruturas do Inconel 718 têm efeitos distintos na condutividade elétrica quando medidos através da técnica de correntes parasitas. A influência da microestrutura na condutividade pode ser mostrada sendo devido à competição de dois efeitos sobre o espalhamento de elétrons: a purificação da matriz e a morfologia, distribuição e tamanho dos precipitados. A combinação dos valores de dureza e condutividade elétrica provou ser uma forma rápida e prática de determinar o nível de envelhecimento da liga; 2) Em um segundo momento foi desenvolvido um processo de otimização de sensores através de modelagem por elementos finitos (MEF). Através de uma metodologia de otimização, os parâmetros de construção e operação de um sensor foram otimizados para inspeção de defeitos superficiais e subsuperficiais esperados em materiais cladeados com Inconel 625. O sensor com a geometria ótima foi construído e testado a fim de verificar a eficiência do processo de otimização. Uma ótima correlação entre os resultados numéricos e experimentais foi encontrada e o sensor ótimo se mostrou eficiente na inspeção de pequenos defeitos superficiais e subsuperficiais na liga Inconel 625 quando operado nas frequências apropriadas. / Nickel-based superalloys have been extensively used in various industries due to its unique mechanical and corrosion behavior. However, these alloys show particular characteristics which lead to the need for specific inspection and metallurgical characterization techniques in order to ensure the structural integrity of components manufactured from these alloys. In this work , the eddy current technique was applied to nickel-base superalloys with two aims: 1 ) Firstly, the microstructural evolution of Inconel 718 during aging processes has been studied through a combination of eddy current testing, X-ray diffraction analysis, metallography, hardness and grain size measurements. Measurements were carried out in samples subjected to different heat treatment cycles between 620-1035°C. Results show that different microstructures of Inconel 718 have a distinguishable effect on electrical conductivity when this is measured through an appropriately sensitive technique (i.e. eddy current testing). The influence of microstructure on conductivity could be shown to be due to the competition between two effects on the scattering of electrons: matrix purification and precipitate size, distribution and morphology. A combination of hardness values and electrical properties proved to be a fast and practical way of determining the stage of aging of the alloy; 2) An optimization method of eddy current sensor design was developed through finite element modeling (FEM). Through a methodology of optimization, the construction and operation parameters of the sensor were optimized for inspection of superficial and subsuperficial defect, commonly found in weld overlay Inconel 625 claddings. A prototype of this sensor with the optimum geometry was built and tested on blocks identical to those considered in the models in order to verify the efficiency of the optimization process. A very good agreement between numerical and experimental results was found. Moreover, the optimal sensor was efficient to detect small surface and subsurface defects in Inconel 625 when operated at appropriate frequencies.

Made available in DSpace on 2014-10-09T12:46:54Z (GMT). No. of bitstreams: 0 / Made available in DSpace on 2014-10-09T14:09:44Z (GMT). No. of bitstreams: 1 09057.pdf: 12808764 bytes, checksum: 970b3a8c12068b9ea0e88948bbcda318 (MD5) / Tese (Doutoramento) / IPEN/T / Instituto de Pesquisas Energeticas e Nucleares - IPEN/CNEN-SP

Na área de Ensaios Não Destrutivos, o ensaio por eddy current (correntes parasitas) é uma técnica eletromagnética largamente utilizada nas indústrias aeroespacial, nuclear e petroquímica. Esse ensaio detecta descontinuidades superficiais e subsuperficiais, prevenindo acidentes. A técnica phased array surgiu para suprir carências, como o enorme tempo gasto para execução do ensaio em materiais de geometria complexa e falta de registro do ensaio. Essa técnica, já bastante utilizada em outros países, ainda é pouco utilizada no Brasil, por não haver estudos que comprovem a viabilidade econômica, os níveis de detectabilidade de descontinuidades e a confiabilidade dos resultados. Este trabalho tem como objetivo comparar as técnicas do ensaio por Correntes Parasitas convencional com a técnica por phased array, em materiais e peças especificamente utilizados no setor aeronáutico e espacial. Foram selecionadas amostras de materiais e peças, para que pudessem ser aplicadas ambas as técnicas e comparados os resultados. Foi realizado um levantamento bibliográfico das principais normas e especificações utilizadas neste segmento, para verificar a compatibilidade dos métodos. Para atender ao objetivo deste trabalho, foram realizados sete experimentos, variando o material e as técnicas. Após a realização dos ensaios, observou-se uma grande redução de tempo na execução do ensaio, com consequente redução de custos e maior detectabilidade das descontinuidades, com o uso da técnica por phased array. Portanto, baseado nos resultados encontrados, pode-se afirmar que a técnica por phased array pode ser utilizada neste segmento, com vantagens sobre a técnica convencional. / In the area of nondestructive testing, eddy current testing is an electromagnetic technique widely used in aerospace, nuclear and petrochemical industries. This test detects surface and subsurface discontinuities, preventing accidents. Phased array technique has emerged to fill in the gaps, as the enormous time spent implementing the test of large parts or complex geometry and lack of trial registration. This technique, already widely used in others countries, is not used in Brazil, there is no studies proving the economic viability, levels of detectability of discontinuities and reliability of the results. This study aims to compare the conventional technique by eddy current testing with phased array technique, in particular materials and parts used in aeronautics and space sector. Samples of materials and parts were prepared, so that could be applied both techniques and compared the results. A literature survey of the main standards and specifications for this segment was conducted to verify the compatibility of the methods. To meet the objective of this work, seven experiments were performed, varying the material and techniques. After the tests, there was a significant time reduction with the use of phased array technique, costs reduction and increased detectability of discontinuities. Based on the results, it can be said that phased array technique can be used in this segment, with advantages over the conventional technique.