This dissertation investigates the use of advanced acoustical communication techniques for wireless downhole telemetry systems. Using acoustic waves for downhole telemetry systems is investigated in order to replace the wired communication systems currently being used in oil and gas wells. While the acoustic technology offers great benefits, a clear understanding of its propagation aspects inside the wells is lacking. This dissertation describes a testbed that was designed to study the propagation of acoustic waves over production pipes. The wireless communication system was built using an acoustic transmitter, five connected segments of seven inch production pipes, and an acoustic receiver. The propagation experiments that were conducted on this testbed in order to characterize the channel behavior are explained as well. Moreover, the large scale statistics of the acoustic waves along the pipe string are described. Results of this work indicate that acoustic waves experience a frequency- dependent attenuation and dispersion over the pipe string. In addition, the testbed was modified by encasing one pipe segment in concrete in order to study the effect of concrete on wave propagation. The concrete was found to filter out many of the signal harmonics; accordingly, the acoustic waves experienced extra attenuation and dispersion. Signal processing techniques are also investigated to address the effects of multipaths and attenuation in the acoustic channel; results show great enhancements in signal qualities and the usefulness of these algorithms for downhole communication systems. Furthermore, to explore an alternative to vibrating the body of a cemented pipe string, a testbed was designed to investigate the propagation aspects of sound waves inside the interior of the production pipes. Results indicate that some low-frequency sound waves can travel for thousands of feet inside a cemented pipe string and can still be detected reliably.

Detection of conformational and structural shifts in biomolecules is of great importance in bioanalytical chemistry and pharmaceutical sciences. Transverse shear mode acoustic wave devices have been used as real-time, label-free detectors of conformational shifts in biomolecules on surfaces. However, material changes in the biochemical monolayer and coupling between the substrate and the surrounding liquid make it difficult to isolate the desired signal, so an understanding of these phenomena is required. In this thesis, interfacial slip, viscoelasticity, and structural changes are used to model acoustic signals due to surface adsorption of the protein neutravidin, immobilisation of HIV-1 TAR RNA, and subsequent interaction of the RNA with tat peptide fragments. Binding of tat peptides induces conformational changes in the TAR. Similar modelling is performed to describe experiments involving the binding of calcium to surface-attached calmodulin, which is also known to result in a conformational shift. The aim of the modelling is to isolate the sensor response due to conformational shifts. The biomolecules are described as hydrated, viscoelastic monolayers and slip is allowed at all interfaces. All models are numerically fit to experimental values using a two-parameter minimisation algorithm. Slip is found on the electrode surface prior to neutravidin adsorption. Neutravidin and TAR are described as distinct viscoelastic monolayers. Binding of tat peptide fragment to the TAR monolayer is modelled using a complex slip parameter and a change in length, corresponding to a straightening of the molecule. Similarly, numerical modelling of calmodulin results reveals a length change in the molecule upon calcium binding. Molecular dynamics (MD) simulations of the TAR-tat fragment system are performed to corroborate the modelling results. Starting structures are computed by molecular docking, and MD simulations of TAR complexed with various length tat fragments are described. The simulations are in general agreement with the modelling results and literature values from similar molecular dynamics experiment. A new parameter is introduced to describe biomolecule-solvent affinity, and is compared to interfacial coupling values obtained from modelling. This research demonstrates that acoustic wave devices can be used to detect conformational shifts in surface-attached biomolecules, provided molecular details about the shifts are known.

I propose two Galerkin methods based on the transfer-of-approximation property for static and dynamic acoustic boundary value problems in seismic applications. For problems with heterogeneous coefficients, the polynomial finite element spaces are no longer optimal unless special meshing techniques are employed. The transfer-of-approximation property provides a general framework to construct the optimal approximation subspace on regular grids. The transfer-of-approximation finite element method is theoretically attractive for that it works for both scalar and vectorial elliptic problems. However the numerical cost is prohibitive. To compute each transfer-of-approximation finite element basis, a problem as hard as the original one has to be solved. Furthermore due to the difficulty of basis localization, the resulting stiffness and mass matrices are dense. The 2D harmonic coordinate finite element method (HCFEM) achieves optimal second-order convergence for static and dynamic acoustic boundary value problems with variable coefficients at the cost of solving two auxiliary elliptic boundary value problems. Unlike the conventional FEM, no special domain partitions, adapted to discontinuity surfaces in coe cients, are required in HCFEM to obtain the optimal convergence rate. The resulting sti ness and mass matrices are constructed in a systematic procedure, and have the same sparsity pattern as those in the standard finite element method. Mass-lumping in HCFEM maintains the optimal order of convergence, due to the smoothness property of acoustic solutions in harmonic coordinates, and overcomes the numerical obstacle of inverting the mass matrix every time update, results in an efficient, explicit time step.

In this thesis, the study focuses on the tunable frequency ratio of Sierpinski Gasket fractal antennas and we use the SAW substrate of piezoelectric material. By using the fractal structure and the substrate of piezoelectric material, the goal of the miniaturized antenna is achieved. The proposed antenna can be widely used in wireless communication products. Firstly, we design the Sierpinski Gasket fractal antenna on the FR4 substrate. The asymmetric geometry of Sierpinski Gasket fractal structure is proposed and we choose the proper discontinuity locations to design the three-band and tunable antenna for IEEE 802.11b/g/a wireless communication systems. The preliminary design of the Sierpinski Gasket fractal structure on the piezoelectric substrate allows us to compare simulated and measured results to improve the non-ideal processing factors. Finally, comparing with the existing products, we reduce the size of the miniaturized fractal antenna to 5x5mm^2 on the SAW substrate by coplanar waveguide, coupled-fed, shorting with conductive adhesive and high iteration stage of half-Sierpinski Gasket fractal structure for GPS band and IEEE 802.11b/g applications.

This study describes the design and fabrication of dual-mode film bulk acoustic resonator (TFBAR) devices to construct wafer level T-ladder type filters. Reactive radio-frequency (RF) magnetron sputtering method was used to deposit c-axis- tilted ZnO piezoelectric thin films. The piezoelectric ZnO thin films were deposited by a two-step method at room temperature with off-axis. In this investigation, off-axis distance was varied to determine the optimal growth parameters of the tilted piezoelectric thin film. The SEM and XRD analysis reveal that ZnO thin films deposited at off-axis distances of 35 mm yielded a highly textured and sufficiently-tilted ZnO piezoelectric layer for dual-mode TFBAR. Additionally, the ZnO piezoelectric layer with off-axis distances of 35 mm exhibited enhanced competitive growth, and had a c-axis-tilted angle of 5¢X. To explore the relationship between the c-axis-tilted angle and the dual-mode resonance frequency responses (fL and fS) of TFBAR, two TFBAR devices were fabricated with ZnO c-axis tilted at 4.4¢X and 5¢X, respectively. The TFBAR device with 5¢X-tilted ZnO layer exists shear and longitudinal resonant modes. The center-frequency of longitudinal resonant mode is 2.2 times that of the shear resonant mode. The longitudinal mode is suitable for designing as a communication receiver (Rx) device at WCDMA band. On the other hand, the shear mode of TFBAR is suitable for EGSM-900 band. To optimize the characteristics, the filter was annealed by CTA treatment in 400 ¢J. For the frequency responses of the longitudinal wave, the insertion loss was upgraded from -5.77 dB without annealing to -4.85 dB as annealed, the band rejection was reduced from 13.57 dB to 12.65 dB, the bandwidth was broaden from 69.69 MHz to 73.12 MHz. On the other hand, for the frequency responses of the shear wave, the insertion loss was upgraded from -9.94 dB to -8.21 dB, the band rejection was reduced from 13.74 dB to 13 dB, the bandwidth was decreased from 28.13 MHz to 28.12 MHz.

Omni-directional acoustic wave source interactions with a rough seabed with a continuously varying density and sound speed in a fluid-like sediment layer. The acoustic properties in the sediment layer possess an exponential type of variation in density and one of the three classes of sound speed profiles, which are constant,~$k^2$-linear, or inverse-square variations. Analytical solution of mean field. The mean field reflection coefficients corresponding to the aforementioned density and sound speed profiles for various frequencies, roughness parameters, are numberically generated and analyzed. Physical interpretations are provided for various results. This simple model characterizes two important features of sea floor, including seabed roughness, sediment inhomogenieties, therefore, provide a canonical analysis in seabed acoustics.

The temperature coefficient of frequency (TCF), electromechanical coupling coefficient (K2) and surface acoustic wave (SAW) velocity are the major factors when choosing the substrates for surface acoustic wave devices. There exist a wide range for the designer to controll the above factors. This thesis adopted several methods to change the properties of SAW devices. First, the SAW velocity is increased using aluminum nitride (AlN) thin films deposited on z-cut LiNbO3 substrates. Besides, the ST-quartz is adopted as substrate for comparison to clarify the temperature characteristic of AlN itself. The well-known positive TCF material, silicon dioxide (SiO2), is also deposited on z-cut LiNbO3 substrates for the purpose of improving the TCF of SAW devices. Finally, the optimal piezoelectric bilayer structures will be conducted for the improvement of the properties of SAW devices on LiNbO3 substrate. AlN and SiO2 thin films are selected to be deposited on z-cut LiNbO3 and ST-cut quartz substrates using the reactive RF magnetron sputtering. The characteristics of AlN thin films are evaluated using the analyses of XRD, SEM and AFM. The optimized growth parameters of highly c-axis oriented AlN films deposited on LiNbO3 substrate are sputtering pressure of 3.5 mTorr, nitrogen concentration (N2/N2+Ar) of 60%, RF power density of 8.1 W/cm2 and substrate temperature of 400¢J. On the other hand, the optimal parameters for highly c-axis oriented AlN films deposited on quartz substrate are sputtering pressure of 15 mTorr, nitrogen concentration of 30%, RF power density of 8.1 W/cm2 and substrate temperature of 400¢J. In addition, the interdigital transducers (IDTs) are fabricated on LiNbO3, AlN/LiNbO3, SiO2/LiNbO3, quartz and AlN/quartz substrates, respectively. The characteristic parameters of SAW devices are measured by Hewlett-Packard (HP) 8720 network analyzer. For SiO2/LiNbO3 SAW devices, the SiO2 thin films reveal the compensation of TCF, but the surface wave velocity remain almost unchanged. For AlN/quartz SAW devices, the positive temperature coefficient of AlN is clarfied by taking ST-quartz substrates as comparison. For AlN/LiNbO3 SAW devices, the characteristic improvements of frequency increase and TCF compensation of LiNbO3 SAW devices are achieved at the same time.

This paper studies is considered the problem of coherent re ection of an acoustic plane wave from a rough seabed with a randomly inhomogeneous sediment layer overlying a uniform elastic basement. The randomness of the sound eld is attributable to the rough- ness of the seabed and the sound-speed perturbation in the sediment layer, resulting in a joint rough surface and volume scattering problem. An approach based upon perturbation theory, combined with a derived Green's function for a slab bounded above and below by a uid and an elastic half space, respectively, is employed to obtain an analytic solution for the coherent eld in the sediment layer. Furthermore, a boundary perturbation the- ory developed by Kuperman and Schmidt [22] is applied to treat the problem of rough surface scattering. A linear system is then established to facilitate the computation of the coherent re ection eld. The coherent re ection coe cients for various surface roughness, sediment randomness, frequency, sediment thickness, and basement elasticity have been generated numerically and analyzed. It was found that the higher/larger size of surface and/or medium randomness, frequency, thickness, and shear-wave speed, the lower the coherent re ection. Physical interpretations of the various results are provided.

The composition-dependent Curie temperature and bias-dependant dielectric permittivity of Barium Strontium Titanate (BST) makes it very attractive for tunable application in the RF/Microwave regime. In this research work, the performance of BST varactors fabricated on the conventional Pt/Ti/SiO2/Si bottom electrode stack were compared with those fabricated using chemical vapor deposited Nanocrystalline Diamond (NCD) as the diffusion barrier layer instead of SiO2. The varactors fabricated on NCD films displayed much better symmetry in capacitance-voltage behavior and better overall quality factors than varactors fabricated on SiO2. The improvement in performance can be attributed to existence of stable interfaces in the devices fabricated on NCD which reduced the bottom electrode losses at high frequencies. The SiO2 based BST varactors on the other hand displayed better reliability and breakdown fields. The main purpose of this research work is to develop a robust Metal Insulator Metal (MIM) structure to achieve better all round performance of BST varactors. In the second part of this research work, the prospect of developing diamond based layered Surface Acoustic Wave (SAW) devices using Ba0.8Sr0.2TiO3 as the piezoelectric layer is investigated. Structural characterization of BST thin films deposited on Si/NCD/Pt and Si/SiO2/Ti/Pt stack were performed using X-Ray Diffraction (XRD) and Atomic Force Microscopy (AFM). Cross-sectional studies on the two stacks were performed using Scanning Electron Microscopy (SEM). X-Ray Mapping (XRM) was then done to ascertain the quality of the interfaces and to check for interdiffusion between layers. MIM structures in the Coplanar Waveguide (CPW) configuration were fabricated using conventional lithography and etching techniques for high frequency measurements. The performance of the fabricated varactors was characterized from 100 MHz to 1 GHz. For the SAW application, structural characterization of Ba0.8Sr0.2TiO3 on Chemical Vapor Deposited (CVD) diamond was done and the deposition procedure was optimized to obtain thick BST films. SAW bandpass filters and resonators were designed wherein the device geometry was varied over a wide range in order to characterize the variation in device performance with geometry. Finally interdigital capacitor structures were fabricated and used for conducting Curie temperature measurements on the deposited BST films in order to determine the operation range of the deposited BST films.

Surface acoustic wave (SAW) sensors detect chemical and biological species by monitoring the shifts in frequency of surface acoustic waves generated on piezoelectric substrates. Incorporation of nanomaterials having increased surface area as sensing layer have been effective in improving the sensitivity as well as miniaturization of SAW sensors. Selectivity, sensitivity and speed of response are the three primary aspects for any type of sensor. This dissertation focuses on design and development of SAW devices with novel transducer configurations employing nanomaterial sensing layers for enhanced sensing, improved selectivity, and speed of response. The sensing mechanism in these SAW sensors is a complex phenomenon involving interactions across several different length and time scales. Surface acoustic wave propagation at the macro-scale is influenced by several kinetic phenomena occurring at the molecular scale such as adsorption, diffusion, reaction, and desorption which in turn depend on the properties of nanomaterials. This suggests the requirement of a multi-scale model to effectively understand and manipulate the interactions occurring at different length scales, thereby improving sensor design. Sensor response modeling at multiple time and length scales forms part of this research, which includes perturbation theories, and simulation techniques from finite element methods to molecular-level simulations for interpreting the response of these surface acoustic wave chemical and biosensors utilizing alloy nanostructures as sensing layers. Molecular modeling of sensing layers such as transition metal alloy nanoclusters and nanowires is carried out to gain insights into their thermodynamic, structural, mechanical and dynamic properties. Finite element technique is used to understand the acoustic wave propagation at the macroscale for sensing devices operating at MHz frequencies and with novel transducer designs. The findings of this research provide insights into the design of efficient surface acoustic wave sensors. It is expected that this work will lead to a better understanding of surface acoustic wave devices with novel transducer configurations and employing nanomaterial sensing layers.