De nos jours, la sécurité des installations publiques, industrielles ou militaires est une problématique majeure. Les phénomènes de détonations en champ libre sont bien connus et documentés. Néanmoins les modèles et les lois mises en place ne s’appliquent pas dans le cas d’explosions confinées.Les travaux présentés dans ce mémoire de thèse portent sur l’étude de la propagation des ondes de choc dans des géométries simples et fermées. Différents paramètres ont été étudiés tels que l’influence du volume, de la position d’amorçage ou encore de la taille de l’évent.Les essais réalisés à petite échelle, dans deux maquettes expérimentales ont permis de mettre en place des lois prédictives portant sur les principaux paramètres de l’onde de choc incidente et réfléchie que sont la surpression maximale, le temps d’arrivée ainsi que l’impulsion.Ces lois ont ensuite été implémentées dans un code de calculs permettant d’automatiser la recherche des réflexions et des différents paramètres associés dans des configurations géométriques simples. / Nowadays, the security of public, industrial or military area is a major concern. Free-field blast are well known and documented. Nevertheless, the models and laws developed do not apply in case of confined explosions. The study focuses on the propagation of shock waves in simple closed geometries. Various parameters have been studied such as the volume, the charge position or the size of vents. The small scales experiments carried out in two experimental models, made it possible to set up predictive laws on the main parameters of the incident and reflective shock wave, such as the maximum overpressure, the arrival time and the impulse.These laws were then implemented in a calculation program to automate the search of reflections and associated parameters in simple geometric setup.

El texto completo de este trabajo no está disponible en el Repositorio Académico UPC por restricciones de la casa editorial donde ha sido publicado. / In the mining industry of Peru, as a consequence of large scale mineral extraction and a dynamic process of ore dressing, the different activities of the operation are neglected. This neglect, in some cases, generates collateral damages that affect the structures, generate extra costs, and result in constant accidents due to rock-fall and delays in the activities of the mining cycle and the ones following it, which seriously harms the Mining Unit and directly affects the workers. In addition, this is directly related to the progress of the daily work and, in turn, it is related to the design of the mine mesh that is prepared to extract the largest possible mineral amounts per shift. This means that, by modifying the design of the mine mesh, the blasting method, and the type of explosive used, the current scenario and the results could be modified. In this respect, a research was conducted, exclusively based on simulations using the JK Simblast software, applying the pre-splitting blast method in the underground mine of the Minera Aurífera Retamas SA company, resulting in a reduction of over break in more than 60% as compared to the mesh used initially. This has an impact on the level of support to be used, and therefore, on the maintenance costs, which were reduced by 18%. Therefore, this article presents the possibility of reducing maintenance costs in underground mining using pre-splitting blasting. Copyright 2019.

During the past two decades many efforts have been made to increase the control of blast furnace conditions to ensure a homogeneous product. The dissections on blast furnaces by various iron and steel companies in Japan in the early 70s provided valuable information on the high temperature properties of charging material. Standard tests (ISO) to determine ore, sinter and pellet qualities only provide information of up to 1100°C . By using the REAS apparatus - a high temperature reduction vessel that simulates the blast furnace process from stockline to melting - the high temperature properties of burden materials have been investigated. The REAS process not only provides an insight into the reactions occurring during the softening and melting process but a range of indices with which to judge the blast furnace performance. Since 1993 new developments started and a test method for Iscor blast furnaces was specifically developed. Although certain indices have been established, uncertainties around the melting mechanisms still existed. These uncertainties include: • Why does the maximum pressure over the sample bed vary extensively between different samples? • Why does a temperature decrease occur only in certain samples and what determines the extent of the temperature decrease? • Which low melting phase forms that causes the initial rise in pressure drop over the sample bed? Four tests were performed on a mixture of Sishen and Thabazimbi ore to determine the phase changes in the test sample. During the reduction of the iron ore, five distinct phases are present. Above 1200°C two liquid phases, an alkali rich phase and a liquid phase with a fayalite composition is present. The rest of the iron reports at different stages in various forms of metallic iron and wustite. Small amounts of a high melting oxide phase, hercynite, also occurs. Softening of the sample is said to occur when the ΔP over the sample bed increases by more than 200 mm H2O. For the specific tests evaluated, this occurred at 1200°C. At this temperature, the liquid with a fayalite composition as well as the alkali rich liquid are present. The formation of the low melting fayalite phase with a high viscosity appears to cause the sudden rise in ΔP. A temperature arrest occurs at the same time supporting the suggestion that liquid formation is responsible for the pressure increase. The results indicate that the mechanisms responsible for the observed pressure drop (decreased gas permeability) and dripping may well be different from those given in the literature. The literature mechanisms emphasise the importance of the amount of FeO available to act as flux for the silica which is present as gangue; hence a greater degree of (indirect) reduction below the melting point of fayalite gives poorer fluxing of silica since less FeO is available. However, the charge materials considered in this study appear to be of substantially higher grade than those used in the previous work. For this reason, there does not appear to be any shortage of FeO to act as flux. This abundance of FeO, and the observation that the peak in pressure drop is not associated with any great change in the amount of liquid, together imply that the literature mechanism regarding changes in the amount and composition of the liquid (i.e. becoming more Si02-rich and viscous as the FeO is reduced) cannot explain the pressure fluctuations observed here. Rather, the increase in pressure appears to be a joint effect of liquid being present (giving the first increase in pressure) and compaction of the sample. Loss of voidage in the sample by this substantial amount of compaction appears the likely cause of the pressure increase. The subsequent decrease in the pressure drop is probably associated with lower viscosity as the sample temperature increases. The importance of compaction means that the amount of indirect reduction does playa role in the development of the pressure drop, but not for the reasons cited in the literature. Pure iron is more malleable than the oxides, and reduction gives a porous iron structure which is more easily compacted. F or both these reasons, the metallic product of indirect reduction favours compaction (and hence the pressure increase). The sharp increase in reduction rate close to the peak pressure presumably results from better contact between the remaining iron oxide (in the fayalite-based liquid, and wustite) with the coke reductant, so favouring direct reduction; this increased reduction (endothermic because of the Boudouard reaction) results in one of the noticeable temperature arrests on the sample temperature curve. The correspondence between the temperature arrests and the changes within the sample do imply that these arrests can be used to gain some information on the reduction mechanisms. However, the reliability of the temperature arrests as indicators of the state of the sample and the reaction conditions within the sample must be tested by further work. / Dissertation (MSc (Metallurgy))--University of Pretoria, 1998. / Materials Science and Metallurgical Engineering / unrestricted

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The single-degree-of-freedom (SDOF) transformation factors as tabulated in John Biggs’ textbook (Biggs 1964) are accepted as the equivalent factors for simplifying and analyzing a component's response to blast. The study validates the stiffness and mass transformation factors through multi-degree-of-freedom (MDOF) numerical methods. After validating the transformation factors, the MDOF numerical method is used to create new stiffness and mass transformation factors for loading cases not already included in Biggs’ textbook. The validated factors, as well as the newly developed factors are used in SDOF analyses. The deflections from the SDOF responses accurately predict the MDOF responses as long as the component behaves elastically; however, the deflections diverge when inelastic behavior is involved. The diverged deflections indicate that the SDOF inelastic response analysis method can be improved.

<p> An experimental investigation has been conducted into the reduction of iron oxides under blast furnace conditions. The necessary equipment has been designed, constructed and tested, and a program of study on two types of prereduced ore materials has been completed.</p> / Thesis / Master of Science (MSc)

This study focused on isolating important wood decay fungi from two field sites located in Harrison County, MS, and Oktibbeha County, MS. Southern Yellow Pine samples of various types and treatments including: Cu8, CuOm, ACQ, PCP, proprietary organic biocide, and un-treated were collected, and fungal isolates were cultured. DNA was extracted from isolated fungal cultures and amplified by polymerase chain reaction (PCR). The internal transcribe spacer (ITS) region was sequenced, and fungal cultures were identified by comparison to sequences on GenBank using BLAST. A total of 68 fungal isolates were recovered and successfully identified from 196 samples. Thirteen basidiomycete isolates were identified, with Veluticeps fimbriata occurring most frequently. The white-rot ascomycete, Daldinia fissa was also common. Two sequence-specific oligonucleotide probes (SSOP) were designed using Lasergene® PrimerSelect software. Unsuccessful attempts were made to attach poly (dT) tails to the probes in order to cross link the probes to nylon membranes.

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