Optical image processing systems using an acousto-optic cell have been studied previously. However, these previous studies have been limited to two diffracted order in the Bragg regime and two spatial dimensions. Some comparisons between experimental data and theoretical predictions have been made. This dissertation studies image processing by acousto-optic Bragg diffraction to perform image enhanment. Theoretical results involving two diffracted orders in three spatial dimensions is presented. Experimental data is presented that confirms the validity of the theoretical results. Detailed analysis of several optical image processing system using acousto-optic modulators is presented. Also, the methodology use to derive an analytically expression in three spatial dimension for the interaction of an arbitrary light profile and a rectangular sound column in an acousto-optic cell is presented. Lastly, the ability to change the characteristics of the derived transfer function that mathematically represents the interaction of light and sound inside the acousto-optic cell is discussed and future research topics is given. / Ph. D.

A modelagem numérica de cristais fotônicos tridimensionais é o objeto de estudo deste trabalho. Especificamente, o método das diferenças finitas no domínio do tempo (FDTD) é utilizado para a modelagem de um cristal FCC (face-centered-cubic) formado por opalas de látex imersas em ar. Por meio de uma análise comparativa com o cristal formado por opalas inversas (opalas de ar incrustadas em uma matriz dielétrica com alto índice de refração), é mostrado que o baixo contraste de índice de refração do cristal de látex é característica preponderante para a inexistência de uma banda proibida completa. No entanto, podem ser observadas bandas fotônicas proibidas ao longo de algumas direções de propagação, como é evidenciado através da investigação da difração de Bragg relativa à família de planos cristalinos (111). Sempre que possível os resultados numéricos são comparados com os dados experimentais disponíveis. / The numerical modeling of tridimensional photonic crystals is the object of study in this work. Especifically, the finite difference time domain method (FDTD) is used for the modeling of a FCC (face-centered-cubic) crystal composed by latex opals immersed in air. Through a comparative analysis to a crystal composed by inverse opals (close-packed air opals in a dielectric matrix with high refractive index), it is shown that the low contrast of the latex crystal is the crucial characteristic to prevent the rising of a complete photonic band gap. However, photonic band gaps can be observed for certain directions of propagation, as it is demonstrated by the investigation of Bragg diffraction related to the (111) crystalline planes. Wherever possible, the numerical results are compared to available experimental data.

A modelagem numérica de cristais fotônicos tridimensionais é o objeto de estudo deste trabalho. Especificamente, o método das diferenças finitas no domínio do tempo (FDTD) é utilizado para a modelagem de um cristal FCC (face-centered-cubic) formado por opalas de látex imersas em ar. Por meio de uma análise comparativa com o cristal formado por opalas inversas (opalas de ar incrustadas em uma matriz dielétrica com alto índice de refração), é mostrado que o baixo contraste de índice de refração do cristal de látex é característica preponderante para a inexistência de uma banda proibida completa. No entanto, podem ser observadas bandas fotônicas proibidas ao longo de algumas direções de propagação, como é evidenciado através da investigação da difração de Bragg relativa à família de planos cristalinos (111). Sempre que possível os resultados numéricos são comparados com os dados experimentais disponíveis. / The numerical modeling of tridimensional photonic crystals is the object of study in this work. Especifically, the finite difference time domain method (FDTD) is used for the modeling of a FCC (face-centered-cubic) crystal composed by latex opals immersed in air. Through a comparative analysis to a crystal composed by inverse opals (close-packed air opals in a dielectric matrix with high refractive index), it is shown that the low contrast of the latex crystal is the crucial characteristic to prevent the rising of a complete photonic band gap. However, photonic band gaps can be observed for certain directions of propagation, as it is demonstrated by the investigation of Bragg diffraction related to the (111) crystalline planes. Wherever possible, the numerical results are compared to available experimental data.

Evaporated thin film sandwich structures of Au-SiOX-Au have been studied. These normally show electroforming effects and subsequently electron emission, electroluminescence, negative resistance and thermal-voltage memory effects. Previous work in the field is critically reviewed. It was shown that the time dependence of the device current and emission current can be explained by making certain modifications to the filamentary conduction theory of Dearnaley. Detailed direct current-voltage measurements have revealed the existence of two different types of breakdown behaviour. At voltages less than 20 V single-hole breakdowns were observed, while in the voltage range 20-30 V large scale irreversible breakdown behaviour took place. The dependence of the voltage at which this occurs (Vß) on insulator thickness and temperature, together with measurements of the device temperature at breakdown and visual evidence of damage after breakdown, has led to the conclusion that this type of breakdown is a thermal effect. Such measurements also pointed to the existence of a high field region within the insulator, and potential distribution measurements confirmed this hypothesis. The high field region was also in evidence at low temperatures where the device current (Ic) showed a log Ic α Vb1/2 dependence on applied voltage (Vb). Measurements of electron attenuation lengths in SiOx gave values of 400-1000 Å irrespective of temperature. The temperature independence was consistent with the emitted electron energy distributions at 77 and 300 K. It was shown that electrons underwent Bragg diffraction through the top Au electrode. The angular distribution of emitted electrons became more isotropic with increasing voltage. Measurements on other systems showed that Al-SiOx/B2O3-Al devices could withstand very high voltages and give improved emission efficiency, while Au-CaBr2-Au and Au-Si3N4-Au devices showed very high initial currents and current-voltage characteristics which were irreversible.

Ce travail de thèse vise à développer de nouvelles techniques de caractérisation pour l'intégration 3D en micro-électronique. Plus précisément, ce travail porte sur l'imagerie 3D de tels objets et la mesure des contraintes par diffraction de Bragg, réalisées sur de récentes lignes de lumière de l'ESRF (European Synchrotron Radiation Facility).L'intégration 3D a pour but de répondre aux besoins de performances de la micro-électronique, en empilant les différents éléments constituant les puces au lieu de les placer les uns à côté des autres; ceci permet de limiter la place qu'ils occupent et la longueur des connections. Pour ce faire, de nouvelles connections entre puces ont du être développées, telles que les piliers de cuivre et les pads de cuivre, utilisés dans le cas du collage hybride. Afin de maîtriser leurs procédé de fabrication, il est important de pouvoir caractériser ces objets, à la fois par des moyens d'imagerie et de mesure de la déformation dans les puces. Ces mesures doivent permettre un large champ de vue (100 µm), ainsi qu'une haute résolution (50 nm). De plus, afin de satisfaire les besoins en temps de l'industrie micro-électronique, les techniques choisies doivent être aussi rapides et automatiques que possible.Pour satisfaire ces besoins, plusieurs techniques ont été étudiés durant ces travaux de thèse.Une technique d'imagerie 3D par Slice and View, inspirée de la technique classique du FIB/SEM et implémentée dans un PFIB (Plasma Focused Ion Beam), a été développée durant ces travaux de thèse. Elle permet aujourd'hui l'acquisition de larges volumes de manière automatique. De même, le procédé d'analyse des mesures de tomographies réalisées sur la ligne de lumière ID16A de l'ESRF a été adapté, afin de limiter au maximum l'intervention humain et le temps global d'analyse.Des mesures de déformations ont également été menées à l'ESRF, sur une ligne de nano-diffraction, ID01. Ces expériences ont été réalisées sur des empilements dédiés au collage, hybride ou direct. Il a été possible de mesurer en une seule expérience les déformations présentes dans deux couches de silicium, et de réaliser des mesures textit{in situ} dans le cuivre.Dans les travaux de thèse présentés ici, nous montrons les possibilités de techniques synchrotron (imagerie et mesure de déformations) pour la caractérisation d'objets issus de l'intégration 3D. Nous montrons que certaines adaptations des techniques existante peuvent permettre des analyses routinières à haute résolution pour le milieu de la micro-électronique. / This PhD thesis aims at developing new characterization techniques for 3D integration in microelectronics. More specifically, the focus is set on recent ESRF (European Synchrotron Radiation Facility) beamlines, both for 3D imaging by tomography and for strain measurements by Bragg diffraction.3D integration aims at reducing the global microelectronics devices footprint and connections length, by stacking the dies on top of one another instead of setting them one to another. This new geometry however requires new connections, such as copper pillars (CuP) and copper pads, used in hybrid bonding. The monitoring of their fabrication process requires their imaging in three dimensions, and the measure of the strain inside them. Those measurements must be conducted on large areas (100 µm2), with high resolution (500 nm for strain and 100 nm for imaging). Moreover, given the industrial context of this study, the characterization methods must be as routine and automatic as possible.To answer those needs, several techniques have been developed in this work.Two 3D imaging techniques have been made compatible with the requirements of 3D integration characterization. A Slice and View procedure has been implemented inside a single beam PFIB, leading to large volumes 3D automated imaging. The tomography workflow accessible on the ID6A beamline of the ESRF has been adapted, in order to limit the human intervention and beam times. This leads to possible statistical measurements on this beamline.Strain measurements have been conducted on the ID01 beamline of the ESRF, on silicon and copper stacks meant for direct and hybrid bonding. They allowed for simultenous local strain measurements in two independent layers of silicon, and textit{in situ} measurements in copper.In this work, we show the possibilities of synchrotron based techniques (here, tomography and Bragg diffraction) for the chacracterization of 3D integration devices. We show that, provided some adjustments, these techniques can be used routinely for the microelectronics field.

Un phénomène d'intrication entre des photons a été observé dans les années 80 par l'équipe dirigée par Alain Aspect. Cette observation a permis de rendre compte du caractère non local de ce phénomène. Nous verrons comment transposer les expériences d'optique au domaine des atomes froids. Une étude nouvelle d'une source d'atomes corrélée (intriquée ?) en impulsion sera présentée et des expériences d'interférences multiples seront analysées. L'objectif final de notre étude est de montrer qu'un test de violation des inégalités de Bell avec des atomes corrélés en impulsion est possible. C'est une expérience de physique fondamentale qui, si elle réussit, ouvre une porte sur la mesure d'effets de la gravité sur l'intrication, un des grands enjeux de la physique actuelle. / It has been experimentally demonstrated in the 1980s by Alain Aspect that the polarization entanglement between two photons can exist and consequently that the locality is no longer valid in this type of experiment. In our experiments, we seek to highlight this kind of phenomenon on atoms. Measurements will focus on external variables such as speed and we will see what tools we need to achieve them. It is a fundamental physics experiment that, if successful, opens the door to measures of possible effects between gravity and entanglement.

Gallium nitride (GaN) light emitting diodes (LED) embody a large field of research that aims to replace inefficient, conventional light sources with LEDs that have lower power, higher luminosity, and longer lifetime. This thesis presents an international collaboration effort between the State Key Laboratory for Mesoscopic Physics in Peking University (PKU) of Beijing, China and the Electrical Engineering Department of California Polytechnic State University, San Luis Obispo. Over the course of 2 years, Cal Poly’s side has simulated GaN LEDs within the pure blue wavelength spectrum (460nm), focusing specifically on the effects of reflection gratings, transmission gratings, top and bottom gratings, error gratings, 3-fold symmetric photonic crystal, and 2-fold symmetric nano-imprinted gratings. PKU used our simulation results to fabricate GaN high brightness LEDs from the results of our simulation models. We employed the use of the finite difference time domain (FDTD) method, a computational electromagnetic solution to Maxwell’s equations, to measure light extraction efficiency improvements of the various grating structures. Since the FDTD method was based on the differential form of Maxwell’s equations, it arbitrarily simulated complex grating structures of varying shapes and sizes, as well as the reflection, diffraction, and dispersion of propagating light throughout the device. We presented the optimized case, as well as the optimization trend for each of the single grating structures within a range of simulation parameters on the micron scale and find that single grating structures, on average, doubled the light extraction efficiency of GaN LEDs. Photonic crystal grating research in the micron scale suggested that transmission gratings benefit most when grating cells tightly pack together, while reflection gratings benefit when grating cells space further apart. The total number of grating cells fabricated on a reflection grating layer still affects light extraction efficiency. For the top and bottom grating structures, we performed a partial optimization of the grating sets formed from the optimized single grating cases and found that the direct pairing of optimized single grating structures decreases overall light extraction efficiency. However, through a partial optimization procedure, top and bottom grating designs could improve light extraction efficiency by 118% for that particular case, outperforming either of the single top or bottom grating cases alone. Our research then explored the effects of periodic, positional perturbation in grating designs and found that at a 10-15% randomization factor, light extraction efficiency could improve up to 230% from the original top and bottom grating case. Next, in an experiment with PKU, we mounted a 2-fold symmetric photonic crystal onto a PDMS hemi-cylinder by nano-imprinting to measure the transmission of light at angles from near tangential to normal. Overall transmission of light compared with the non-grating design increases overall light extraction efficiency when integrated over the range of angles. Finally, our research focused on the 3-fold symmetric photonic crystal grating structure and employed the use of 3-D FDTD methods and incoherent light sources to better study the effects of higher-ordered symmetry in grating design. Grating cells were discovered as the source of escaping light from the GaN LED model. The model revealed that light extraction efficiency and the far-field diffraction pattern could be estimated by the position of grating cells in the grating design.

[EN] The aim of this work is to demonstrate theoretically and experimentally how acoustic wave propagation can be controlled by temperature gradients. Starting with the simplest case of two hot wires in air the study extends over periodic structures known as Sonic Crystals (SCs). The Finite Elements Method (FEM) has been employed to perform numerical simulations in order to demonstrate collimation and focusing effect of acoustic waves in two-dimensional (2D) SC whose filling fraction is adjusted by temperature gradients. As a part of the research, Bragg reflection and Fabry-Perot type of acoustic effects are investigated for the proposed type of SC. As example, a SC with desired transmittance can be tailored. Also, gradient index (GRIN) 2D sonic lenses are studied. Using parallel rows of heated wires whose temperatures vary according to a prefixed gradient index law a GRIN lens can be designed with a given performance. Moreover, by changing the temperature of the wires a change in the filling fraction inside the GRIN SC can be achieved. Thus, the local refraction index, which is directly related to the filling fraction, is changed too and an index gradient variation inside the GRIN SC is obtained. This GRIN SC is a direct analogy of gradient media observed in nature. Like their optical counterparts, the investigated 2D GRIN SC lenses have flat surfaces and are easier for fabrication than curved SC lenses. The bending of sound waves obtained by GRIN acoustics structures can be used to focusing and collimating acoustic waves. Another aspect of this work is about tuning some SC properties as effective refractive index, effective mass density, etc. in order to obtain a SC with prefixed properties. Since active tuning of the phononic band gaps is certainly desirable for future applications with enhanced functionalities, few attempts have been made to develop tunable SCs thus far. By controlling the incident angle or operating frequency, a GRIN SC can dynamically adjust the curved trajectory of acoustic wave propagation inside the SC structure. Among the last studies of tunable SCs, the filling fractions were tuned either by direct physical deformation of the structure or external stimuli. The former is impractical for most applications and the latter often requires very strong stimuli to produce only modest adjustment. In this work another way to tune the SC properties is proposed. Hot and cold media have different density, speed of sound, refractive index, etc. in comparison with the same properties at normal conditions, so inserting temperature gradients inside the medium can be used to tune the SC properties in certain limits. The proposed way to obtain temperature gradients inside SC is by wires made of Nicrom which are heated by electrical currents. There are some important advantages of this method. First, changing the electrical current intensity through the wires the SC properties can be changed dynamically. Second, it is relatively easier to change the filling fraction simply by adjusting the current intensity than physically changing the structure or applying strong electric or magnetic fields. In conclusion, the method proposed in this thesis allows us, in principle, to get materials and structures with dynamically adjustable acoustic properties using the temperature control through electric current in the wires, within certain limits. Thus, it is easy to carry out experiments of wave propagation phenomena in a macroscopic scale similar to those that occur in microscopic structures for the propagation of electromagnetic waves of high frequency (microwaves and light). / [ES] El objetivo de este trabajo es demostrar teoréticamente y experimentalmente como la propagación de ondas acústicas puede ser controlada por gradientes de temperatura. Empezando con el caso más simple de dos hilos calientes en aire, el estudio se extiende sobre estructuras periódicas conocidas como cristales sónicos (CS). Se ha utilizado el Método de Elementos Finitos (FEM) para realizar simulaciones numéricas con el objetivo de demonstrar la colimación y focalización de ondas acústicas en CS bidimensionales (2D) cuya fracción de llenado es ajustable mediante gradientes de temperatura. Como parte de la investigación se ha analizado la reflexión de Bragg y el efecto de tipo Fabry-Perot asociados con los CSs estudiados. Entre los ejemplos tratados figuran un CS con una transmitancia ajustable a voluntad, dentro de ciertos límites. También se han estudiado lentes acústicas bidimensionales de gradiente de índice, basadas en gradiente de temperatura. Utilizando cortinas paralelas de hilos calientes cuya temperatura varía según una ley dada se puede diseñar una lente GRIN con propiedades determinadas. Por otra parte, cambiando la temperatura de los hilos se puede lograr un cambio en la fracción de llenado dentro del GRIN CS. Así, el índice de refracción local, que está directamente relacionado con la fracción de llenado, se cambia también y se obtiene una variación de gradiente de índice dentro del GRIN CS. Este GRIN CS es una analogía directa de medios con gradiente, observados en la naturaleza. Otro aspecto de este trabajo trata sobre el ajuste de algunas propiedades de un SC como el índice de refracción efectivo o la densidad efectiva con el objetivo de obtener unas propiedades deseadas del cristal. Como el ajuste activo de los bandgaps fonónicos es ciertamente deseado para futuras aplicaciones con funcionalidades mejoradas, hasta ahora se han hecho varios intentos de desarrollar CSs de características ajustables. Controlando el ángulo de incidencia o la frecuencia de funcionamiento, un GRIN CS puede ajustar dinámicamente la curvatura de la trayectoria de propagación dentro de la estructura CS. Entre los últimos estudios de CSs las fracciones de llenado se ajustaron mediante una deformación física directa de la estructura o mediante estímulos externos (por ejemplo campos eléctricos o magnéticos). El primero es poco práctico para una gran parte de las aplicaciones y el segundo a menudo requiere estímulos muy fuertes para ajustes modestos. En este trabajo se propone otra forma de ajustar las propiedades de un CS. Las propiedades acústicas del medio de propagación (densidad, índice de refracción) dependen de la temperatura, por tanto, introduciendo gradientes de temperatura dentro de dicho medio pueden ajustarse a voluntad las propiedades del CS dentro de ciertos límites. La manera de obtener gradientes de temperatura dentro del CS, propuesta en este estudio, es mediante hilos de nicrom calentados con corrientes eléctricas. Hay algunas ventajas importantes de este método. En primer lugar, cambiando la intensidad de corriente eléctrica que circula por los hilos se puede conseguir cambiar dinámicamente las propiedades del CS. En segundo lugar, es relativamente más fácil de cambiar la fracción de llenado simplemente ajustando la intensidad de la corriente eléctrica que modificar físicamente la estructura o aplicar fuertes campos eléctricos o magnéticos. En conclusión, el método propuesto en esta tesis permite, en principio, conseguir materiales y estructuras con propiedades acústicas ajustables dinámicamente mediante el control de la temperatura a través de la corriente eléctrica en los hilos, dentro de ciertos límites. De esta forma se puede experimentar fácilmente a escala macroscópica fenómenos de propagación de ondas análogos a los que ocurren en estructuras microscópicas para la propagación de ondas electromagnéticas de alta frecuencia (microondas y l / [CAT] L'objectiu d'este treball és demostrar teorèticament i experimentalment com la propagació d'ones acústiques pot ser controlada per gradients de temperatura. Començant amb el cas més simple de dos fils calents en aire, l'estudi s'estén sobre estructures periòdiques conegudes com a cristalls sónics (CS) . S'ha utilitzat el Mètode d'Elements Finits (FEM) per a realitzar simulacions numèriques amb l'objectiu de demonstrar la col¿limació i focalització d'ones acústiques en CS bidimensionals (2D) la fracció de omplit de la qual és ajustable per mitjà de gradients de temperatura. Com a part de la investigació s'ha analitzat la reflexió de Bragg i l'efecte de tipus Fabry-Perot associats amb els CSs estudiats. Entre els exemples tractats figuren un CS amb una transmitancia ajustable a voluntat, dins de certs límits. També s'han estudiat lents acústiques bidimensionals de gradient d'índex, basades en gradient de temperatura. Utilitzant cortines paral¿leles de fils calents la temperatura de la qual varia segons una llei donada es pot dissenyar una lent GRIN amb propietats determinades. D'altra banda, canviant la temperatura dels fils es pot aconseguir un canvi en la fracció d'ompliment dins del GRIN CS. Així, l'índex de refracció local, que està directament relacionat amb la fracció d'ompliment, es canvia també i s'obté una variació de gradient d'índex dins del GRIN CS. Este GRIN CS és una analogia directa de mitjans amb gradient, observats en la naturalesa. Com les seues analogies òptiques, les lents, estudiades en este treball, tenen les superfícies planes i són més fàcils de fabricar que les lents corbades. La deflexión de les ones acústiques obtinguda per mitjà d'una lent de gradient GRIN es pot utilitzar per a focalitzar o colimar feixos de so. Un altre aspecte d'este treball tracta sobre l'ajust d'algunes propietats d'un SC com l'índex de refracció efectiu o la densitat efectiva amb l'objectiu d'obtindre unes propietats desitjades del cristall. Com l'ajust actiu dels bandgaps fonónicos és certament desitjat per a futures aplicacions amb funcionalitats millorades, fins ara s'han fet diversos intents de desenrotllar CSs de característiques ajustables. Controlant l'angle d'incidència o la freqüència de funcionament, un GRIN CS pot ajustar dinàmicament la curvatura de la trajectòria de propagació dins de l'estructura CS. Entre els últims estudis de CSs les fraccions d'ompliment es van ajustar per mitjà d'una deformació física directa de l'estructura o per mitjà d'estímuls externs. El primer és poc pràctic per a una gran part de les aplicacions i el segon sovint requerix estímuls molt forts per a ajustos modestos. En este treball es proposa una altra forma d'ajustar les propietats d'un CS. Les propietats acústiques del mig de propagació (densitat, índex de refracció) depenen de la temperatura, per tant, introduint gradients de temperatura dins del dit mitjà poden ajustar-se a voluntat les propietats del CS dins de certs límits. La manera d'obtindre gradients de temperatura dins del CS, proposta en este estudi, és per mitjà de fils de Nicrom calfats amb corrents elèctrics. Hi ha alguns avantatges importants d'este mètode. En primer lloc, canviant la intensitat de corrent elèctric que circula pels fils es pot aconseguir canviar dinàmicament les propietats del CS. En segon lloc, és relativament més fàcil de canviar la fracció d'ompliment simplement ajustant la intensitat del corrent elèctric que modificar físicament l'estructura o aplicar forts camps elèctrics o magnètics. En conclusió, el mètode proposat en esta tesi permet, en principi, aconseguir materials i estructures amb propietats acústiques ajustables dinàmicament per mitjà del control de la temperatura a través del corrent elèctric en els fils, dins de certs límits. D'esta manera es pot experimentar fàcilment a escala macroscòpica fenòmens de propagació d'ones anàlegs a què ocorren e / Ivanov Angelov, M. (2016). Sound Scattering by Lattices of Heated Wires [Tesis doctoral no publicada]. Universitat Politècnica de València. https://doi.org/10.4995/Thesis/10251/63275 / TESIS

La qualité des interfaces dans les multicouches périodiques est essentielle au développement de miroirs réfléchissant efficacement dans les domaines des rayons X et extrême ultraviolet (X-EUV). De manière générale, la structure des interfaces dépend des possibles interdiffusion et processus chimiques aux interfaces entre couches. L'idée principale de cette thèse est d'appliquer la technique des ondes stationnaires dans le domaine X à la caractérisation de matériaux, principalement mais non exclusivement aux multicouches périodiques. Cette méthode est basée sur l'interférence de deux faisceaux de rayons X cohérents. L'interférence constructive sur un plan anti-nodal amplifie le champ électrique tandis que l'interférence destructive minimise ce dernier sur un plan nodal. Cette technique des ondes stationnaires dans le domaine X permet l'excitation (photoémission, fluorescence, ...) d'endroits spécifiques dans un empilement périodique de matériaux. De cette manière, les spectres expérimentaux ainsi obtenus sont principalement les spectres caractéristiques des atomes situés sur un plan anti-nodal. Combinée avec d'autres techniques expérimentales telles que la spectroscopie d'émission X (XES) ou la spectroscopie de photoélectrons dans le domaine X (XPS), une information sélective en profondeur, avec une sensibilité sub-nanométrique, peut être obtenue. / The interfacial information of periodic multilayers can be crucial for the development of reflecting mirrors which operate in the X-ray and extreme ultraviolet (X-EUV) ranges. Such information may contain the interdiffusion and chemical process at the interfaces of the layers. The idea of this thesis is to apply the X-ray standing wave technique to the characterization of materials, mainly but not limited to the periodic multilayers. X-ray standing wave technique enables to enhance the excitation (photoemission, fluorescence etc.) of specific locations within a periodic stack. The nature of such advantage is the interference of two coherent X-ray beams. One may compare the X-ray standing waves with the mechanical standing waves. The constructive interference at the anti-nodal plane amplifies the electric field; while the destructive interference at the nodal plane minimizes the electric field. In this way, the experimental spectra obtained under standing wave field will be mostly the material located on the anti-nodal plane. Combined with other techniques such as X-ray emission spectroscopy and X-ray photoelectron spectroscopy, a depth-selective information with a sub-nanoscale sensitivity can be obtained.

Quantensensoren auf Basis ultra-kalter Atome sind gegenwärtig auf dem Weg ihre klassischen Pendants als Messintrumente sowohl in Präzision als auch in Genauigkeit zu überholen, obwohl ihr Potential noch immer nicht vollständig ausgeschöpft ist. Die Anwendung von Quantensensortechnologie wie Materiewelleninterferometern im Weltraum wird ihre Sensitivität weiter steigen lassen, sodass sie potentiell die genauesten erdbasierten Systeme um mehrere Grössenordnungen übertreffen könnten. Mikrogravitationsplattformen wie Falltürme, Parabelflugzeuge und Höhenforschungsraketen stellen exzellente Testumgebungen für zukünftge atominterferometrische Experimente im Weltraum dar. Andererseits erfordert ihre Nutzung die Entwicklung von Schlüsseltechnologien, die hohe Standards in Bezug auf mechanische und thermische Robustheit, Autonomie, Miniaturisierung und Redundanz erfüllen müssen. In der vorliegenden Arbeit wurden erste Interferometrieexperimente mit degenerieten Quantengasen in Schwerelosigkeit im Rahmen des QUANTUS Projektes durchgeführt. In mehr als 250 Freifall-Experimenten am Bremer Fallturm konnte die Präparation, freie Entwicklung und Phasenkohärenz eines Rubidium Bose- Einstein Kondensates (BEC) auf makroskopischen Zeitskalen von bis zu 2 s untersucht werden. Dazu wurde ein BEC-Interferometer mittels Bragg-Strahlteilern in einen Atomchip-basierten Aufbau implementiert. In Kombination mit dem Verfahren der Delta-Kick Kühlung (DKC) konnte die Expansionsrate der Kondensate weiter reduziert werden, was zur Beobachtung von effektiven Temperaturen im Bereich von 1 nK führte. In einem Interferometer mit asymetrischer Mach-Zehnder Geometrie konnten Interferenzstreifen mit hohem Kontrast bis zu einer Verweildauer von 2T = 677 ms untersucht werden. / State-of-the-art cold atomic quantum sensors are currently about to outpace their classical counterparts in precision and accuracy, but are still not exploiting their full potential. Utilizing quantum-enhanced sensor technology such as matter wave interferometers in the unique environment of microgravity will tremendously increase their sensitivity, ultimately outperforming the most accurate groundbased systems by several orders of magnitude. Microgravity platforms such as drop towers, zero-g airplanes and sounding rockets are excellent testbeds for advanced interferometry experiments with quantum gases in space. In return, they impose demanding requirements on the payload key technologies in terms of mechanical and thermal robustness, remote control, miniaturization and redundancy. In this work, first interferometry experiments with degenerate quantum gases in zero-g environment have been performed within the QUANTUS project. In more than 250 free fall experiments operated at the drop tower in Bremen, preparation, free evolution and phase coherence of a rubidium Bose-Einstein condensate (BEC) on macroscopic timescales of up to 2 s have been explored. To this end, a BEC interferometer using first-order Bragg diffraction was implemented in an atomchip based setup. Combined with delta-kick cooling (DKC) techniques to further slow down the expansion of the atomic cloud, effective temperatures of about 1 nK have been reached. With an asymmetrical Mach-Zehnder geometry, high-contrast interferometric fringes were observed up to a total time in the interferometer of 2T = 677 ms.