Kenaf fiber is increasingly getting the attention of the industries due to its excellent mechanical properties, feasibility, growth rate, and ease of cultivation. On the other hand, cellulose nanofibril is one of the important building blocks of all the bast fibers which significantly contributes to their mechanical properties. However, most of the studies in the literature have estimated the value of axial elastic modulus for fiber-bundles which has some unavoidable issues resulting in incorrect modulus. Moreover, the transverse elastic modulus is another important parameter that also needs to be studied. Hence, to compensate for the gap in the literature, a single unit of both kenaf microfiber and cellulose nanofibril have been subjected to nanomechanical characterization to analyze their surface morphology and determine their elastic modulus in the axial and transverse direction. The experiments also pave to a protocol to characterize micro and nanofibrils nanomechanically and determine their elastic moduli.

Geogrid reinforcement can improve the performance of pavements by stiffening the aggregate base material and decreasing pavement deformations. Understanding the effects of cyclic loading on the modulus of geogrid-reinforced base materials would help engineers better anticipate actual increases in the modulus of aggregate base materials under given traffic loads. The objective of this laboratory research was to investigate the effects of cyclic loading on the resilient modulus, the modulus to peak axial stress, the elastic modulus, and the modulus at 2 percent strain of geogrid-reinforced aggregate base materials. The scope of the research included two aggregate base materials (Wells Draw and Springville) having different particle-size distributions and particle angularity. Geogrid-reinforced and unreinforced specimens were subjected to conditioning periods consisting of cyclic loading ranging from 10 to 10,000 cycles. Immediately following cyclic loading, all specimens were tested using the quick shear portion of the American Association of State Highway and Transportation Officials T 307 (Determining the Resilient Modulus of Soils and Aggregate Materials). Specimen preparation involved material weigh-outs, compaction, and membrane applications. Specimen testing in the loading machine consisted of two testing portions, including cyclic loading and quick shear testing. The cyclic loading data were used to calculate the resilient modulus on 200-cycle intervals throughout the duration of the conditioning period. The quick shear data were used to calculate the peak axial stress, the modulus to peak axial stress, the elastic modulus and the modulus at 2 percent strain. For the Wells Draw material, the resilient modulus increases by 11 percent for the specimens with geogrid and increases by 8 percent for the specimens without geogrid as the number of load cycles increases from 1,000 to 10,000. For the Springville material, the resilient modulus increases by 2 percent for the specimens with geogrid and increases by 3 percent for the specimens without geogrid as the number of load cycles increases from 1,000 to 10,000. As with other studies, the results do not show a consistent or significant effect of geogrid reinforcement on the resilient modulus of the tested materials. The modulus at 2 percent strain has the most potential for consistently showing improvements to aggregate base materials due to both cyclic loading and geogrid reinforcement. For the Wells Draw and Springville materials, the modulus at 2 percent strain increases by 31 and 9 percent, respectively, as the number of load cycles increases from 10 to 10,000. Additionally, for the Wells Draw and Springville materials, the modulus at 2 percent strain of the specimens with geogrid is 23 and 46 percent, respectively, greater than that of the specimens without geogrid. The results show a consistent and significant positive effect of geogrid reinforcement on modulus at 2 percent strain of the tested materials. According to the modulus at 2 percent strain results, a sufficient conditioning period appears to occur at 5,000 cycles for the Wells Draw material and 10,000 cycles for the Springville material.

Compacted soils are frequently used as subgrade for pavements as well as commercial and residential buildings. The stiffness and shear strength properties of compacted soils, which are collectively denoted as Ω in this thesis, fluctuate with moisture content changes that result from the influence of environmental factors such as the evaporation and infiltration. For example, mechanistic pavement design methods require the information of resilient modulus (MR), which is the soil stiffness behavior under cyclic traffic loading, and its variation with respect to the soil moisture content determined from laboratory tests or estimation methods. Significant advances have been made during the last five decades to understand and model the variation of the Ω with respect to soil moisture content and soil suction (s) based on the principles of mechanics of unsaturated soils. There are a variety of models presently available in the literature relating the Ω to the s using different approaches. There are however uncertainties extending these models for predicting Ω - s relationships when they are used for a larger soil suction range. In addition, the good performance of these models are only valid for certain soil types for which they were developed and calibrated. Studies presented in this thesis are directed towards developing a unified methodology for modelling the relationship between the Ω and the s using limited while easy-to-obtain information. However, more emphasis has been focused on the MR - s relationships of pavement subgrade soils considering the need for the application of the mechanistic pavement design methods in Canada. The following studies have been conducted: (i) State-of-the-art review on existing equations in the literature for the MR - s relationships is summarized. A comparison study is followed to discuss the strengths and limitations of these equations; (ii) A unified methodology for modelling the Ω - s relationships is proposed. Experimental data on 25 different soils are used to verify the proposed unified methodology. The investigations are applied on small strain shear modulus, elastic modulus, and peak and critical shear strength. Good predictions are achieved for all of the investigated soils; (iii) Performance of the proposed methodology is examined for the MR - s relationships using experimental data of 11 subgrade soils. Reasonably good predictions are achieved for all of the subgrade soils; (iv) Extensive experimental investigations are conducted on the MR - s relationships for several subgrade soils collected from various regions in Canada. Experimental results suggest non-linear variation in the MR with respect to s, moisture content and the external stress. The measured results are modelled using the proposed methodology with adequate success; (v) Additional experimental investigations are performed to determine the variation of the elastic modulus (E) and unconfined compression strength (qu) with the s and the gravimetric moisture content (w) for several Canadian subgrade soils. An approach, which is developed extending the proposed unified methodology, is used to normalize the measured MR - w, E - w and qu - w relationships. It is shown that the normalized MR - w, E - w and qu - w relationships exhibit remarkable similarity and can be well described using the proposed approach. Such similarity in the normalized Ω - moisture content relationships are also corroborated using the experimental data on several other soils reported in the literature. The proposed unified methodology alleviates the need for the determination of the Ω - s relationships which requires elaborate testing equipment that needs the supervision of trained personnel and is also time-consuming and expensive. In addition, experimental programs in this thesis provide detailed experimental data on the MR, E, qu, and soil-water characteristic curves of Canadian subgrade soils. These data will be helpful for the better understanding of the hydro-mechanical behavior of the Canadian subgrade soils and for the implementation of the mechanistic pavement design method in Canada. The simple tools presented in this thesis are promising and encouraging for implementing the mechanics of unsaturated soils into conventional geotechnical engineering practice.

京都大学 / 0048 / 新制・課程博士 / 博士(医学) / 甲第18164号 / 医博第3884号 / 新制||医||1003(附属図書館) / 31022 / 京都大学大学院医学研究科医学専攻 / (主査)教授 戸口田 淳也, 教授 妻木 範行, 教授 開 祐司 / 学位規則第4条第1項該当 / Doctor of Medical Science / Kyoto University / DFAM

Soil cement has been used as a means of stabilizing highway pavement layers, airport pavement layers, embankments, and foundations for decades. The technology uses a compacted mixture of soil, cement, and water to form a hardened material layer that has specific strength and durability properties. Even after decades of utilization, however, design of soil cement pavement layers has room for enhancement. This thesis investigates factors that influence the design and performance of cement stabilized pavement layers in Mississippi. A survey was conducted to collect information about soil cement design procedures from across the U.S. The factors examined in the laboratory investigation are strength gain with time, unconfined compressive strength variability, elastic modulus, and wheel tracking. More than 1,100 specimens were tested to determine the influence of these factors on the design and performance of soil cement pavement layers.

We construct a covering system whose minimum modulus is 42. This improves the previous record of 40 by P. Nielsen.

This paper presents results on experimental research for concrete produced using recycled coarse aggregates (RCA). Five types of coarse aggregates were used in this study, four of which were RCA. The main purpose of this research was to examine how different types and properties of coarse aggregate affected compressive strength, modulus of elasticity, and shrinkage in concrete when natural coarse aggregates were replaced with RCA. Concrete batches were made with water-cement (w/c) ratios of 0.30, 0.45, and 0.60, and substitution percentages ranged from 0% to 100% of natural aggregate with RCA. Test results clearly show that compressive strength, modulus of elasticity, and shrinkage greatly depend on the quality and type of coarse aggregate used. In addition to testing of hardened concrete, predictive models for elasticity and ultimate shrinkage were developed to formulate and reinforce proposed conclusions about the properties and performance for the different RCA.

The relationship between cells and their environment is one of dynamic reciprocity, whereby cells can influence their surrounding and the surroundings can influence the cells. One example of this relationship arises from the effect of the mechanical properties of an environment on a cell and of a cell on its environment. Inspired by this relationship, we investigate 1) the local environment of biological materials, both native and synthetic, and 2) the forces that cell sheets exert on surfaces. We do this by developing techniques that focus on local mechanical properties and experimental strategies that provide insight into intercellular mechanics. We first focus on determining local mechanical properties of hydrogel materials by developing the Cavitation Rheology technique. This process involves inducing a cavitation event at the tip of a syringe needle. We develop theory to show that the critical pressure to cavitate can be directly related to the modulus of the material (Chapter 2). This allows us to experimentally determine the mechanical properties at arbitrary locations throughout a material scaffold over a range of length scales defined by the needle radius (Chapter 3). We then demonstrate that we can viturally elminate the energy contribution from the creation of new surface area to the critical pressure by cavitating with a media of lower surface energy (Chapter 4). In chapter 5, we show that Cavitation Rheology can be used on native biological tissues and we go on to demonstrate the importance of measuring the mechanical properties in vivo. We then focus on understanding the force development of cells as they grow to confluency on a dynamic substrate (Chapter 6). We demonstrate the method of living microlenses to measure the collective strains cell sheets attain by growing cells on a thin polystyrene film supported by a surface of microwells. The cells cause the film to buckle and the resultant buckling can be directly related to the strain. We use this technique to study the strains exerted by various cell types and to determine the importance of the cell-cell junctions on the strain development.

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