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Composite materials have a wide range of applications in civil and structural engineering due to their advantages in mechanical properties and higher strengths over the base materials alone. Polymer-concrete composites are particularly attractive for use in industrial and infrastructure applications from combining the higher mechanical properties of the concrete in tension and the high tensile strength and ductile properties of the polymeric materials. However, these materials tend to be more expensive that typical concrete composites. This thesis explores the mechanical properties of two different polymer-concrete composites and their effectiveness in civil and structural applications: polymer concrete for rapid repair and 3D printed plastic-concrete composite members for energy absorption. The North Atlantic Treaty Organization (NATO) requires that emergency repair of military runways should be completed within 4 hours. In coordination with Luna Innovations Incorporated, a polymer concrete was developed by Luna for use as a rapid repair material for military runways to meet this requirement through its rapid heat curing. Its mechanical properties including its compressive and flexural strength, bond strength in various orientations, workability, modulus of elasticity, and coefficient of thermal expansion were tested and compared against another rapid repair material. The Tri-Service Pavements Working Group Manual recommendations for rigid repair materials were used as the requirements in determining whether the polymer concrete was an adequate rapid repair material. The polymer concrete formulation that was down-selected for further testing met these requirements for all tests except for the coefficient of thermal expansion. This was due to the resin itself having a high volumetric expansion when exposed to greater temperatures. As the polymer concrete is still under development, future tests are to be performed to determine the impact of the higher expansion on the surrounding runways. Additionally, inspired from naturally forming nacre found in some seashells, a 3D printed plastic-concrete beam structure was developed and tested in flexure to determine its energy absorption capabilities. The nacreous structure allows the material to experience a strain-hardening behavior, thus allowing for energy dissipation in the beam as it deflects from further applied load. It is theorized that the energy absorption capabilities would be suitable for withstanding the effects of dynamic loadings in structures, such as earthquake and blast loads. Multiple beam structures were developed and tested to determine the impact of percent-polymeric material and layout had on the energy dissipation. Overall, the specimens with more polymer in the cross-section demonstrated larger load vs. crack mouth displacement curves and fracture energy. These specimens demonstrated a higher toughness as well, making them more suitable for use in structural applications. As the project is still in development, future tests and analysis must be performed to determine their strength properties and feasibility as a structural material. The results of this thesis highlight the benefits of novel polymer composites in industrial and infrastructure applications, such as improved rapid setting characteristics and significantly enhanced mechanical and energy absorbing performance. Future work is needed to optimize these performance metrics, such as freeze thaw cycling, fatigue, and durability tests for the polymer concrete and analysis of moment capacity for the bioinspired nacreous composites. / Master of Science / Composite materials have a wide range of applications in civil and structural engineering due to their advantages in mechanical properties and higher strengths over the base materials alone. Polymer concrete composites are not as widely used due to their greater initial costs. However, they are very attractive in industrial and infrastructure applications because of the improved behavior in tension. This thesis explores the mechanical properties of two different polymer-concrete composites and their effectiveness in civil and structural applications: polymer concrete for rapid repair and 3D printed plastic-concrete composite members for energy absorption. The North Atlantic Treaty Organization (NATO) requires that emergency repair of military runways should be completed within 4 hours. In coordination with Luna Innovations Incorporated, a polymer concrete was developed by Luna for use as a rapid repair material for military runways to meet this requirement through its rapid heat curing. Its mechanical properties were tested and compared against another rapid repair material. The polymer concrete formulation that was down-selected for further testing met the requirements of the military for all tests performed except for the coefficient of thermal expansion. As the polymer concrete is still under development, future tests are to be performed to determine the impact of the higher expansion on the surrounding runways. Additionally, inspired from naturally forming nacre found in some seashells, a 3D printed plastic-concrete beam structure was developed and tested in bending to determine its energy absorption capabilities. The nacreous structure allows the material to experience a strain-hardening behavior, thus allowing for energy dissipation in the beam as it deflects from further applied load. It is theorized that the energy absorption capabilities would be suitable for withstanding the effects of earthquake and blast loads in structures. Multiple beam structures were developed and tested to determine the impact of percent-polymeric material and layout had on the energy dissipation. Overall, the specimens with more polymer in the cross-section demonstrated greater energy absorption capabilities. As the project is still in development, future tests and analysis must be performed to determine their strength properties and feasibility as a structural material. The results of this thesis highlight the benefits of novel polymer composites in industrial and infrastructure applications, such as improved rapid setting characteristics and significantly enhanced mechanical and energy absorbing performance. Future work is needed to optimize these performance metrics, such as freeze thaw cycling, fatigue, and durability tests for the polymer concrete and analysis of moment capacity for the bioinspired nacreous composites.

Cuttlebone, the endoskeleton of cuttlefish, offers an intriguing biological structural model for designing low-density cellular ceramics with high stiffness and damage tolerance. Cuttlebone is highly porous (porosity ~93%) and lightweight (density less than 20% of seawater), constructed mainly by brittle aragonite (95 wt%), but capable of sustaining hydrostatic water pressures over 20 atmospheres and exhibits energy dissipation capability under compression comparable to many metallic foams (~4.4 kJ/kg). Here we computationally investigate how such a remarkable mechanical efficiency is enabled by the multiscale structure of cuttlebone. Using the common cuttlefish, Sepia Officinalis, as a model system, we first conducted high-resolution synchrotron micro-computed tomography (µ-CT) and quantified the cuttlebone's multiscale geometry, including the 3D asymmetric shape of individual walls, the wall assembly patterns, and the long-range structural gradient of walls across the entire cuttlebone (ca. 40 chambers). The acquired 3D structural information enables systematic finite-element simulations, which further reveal the multiscale mechanical design of cuttlebone: at the wall level, wall asymmetry provides optimized energy dissipation while maintaining high structural stiffness; at the chamber level, variation of walls (number, pattern, and waviness amplitude) contributes to progressive damage; at the entire skeletal level, the gradient of chamber heights tailors the local mechanical anisotropy of the cuttlebone for reduced stress concentration. Our results provide integrated insights into understanding the cuttlebone's multiscale mechanical design and provide useful knowledge for the designs of lightweight cellular ceramics. Upon the prior curvature analysis of the cuttlebone walls, we discovered that the walls were primarily "saddle-shaped". Thus, the characterization of different curvatures, varying between flat, domed, saddled, or cylindrical surfaces, were explored. A mathematical model was utilized to generate multiple walls with different curvature characteristics. We observed the mechanical performance of these walls via finite-element analysis and formulated different techniques for designing effective ceramic structures through incorporation of curvature. / Master of Science / The cuttlefish is a marine species that instead of having an inflatable swim bladder like fish, is a mollusk capable of swimming by utilizing their skeleton, called the cuttlebone. The cuttlefish can freely traverse the waters by controlling the flow of water in and out of their brittle skeletons, changing their buoyancy. For this reason, the cuttlebone must be very porous yet strong to withstand the deep-water pressures, enticing an interest for closer observation of the structure which may be useful in engineering applications involving ceramic structures. In this study, we examined an actual cuttlebone structure to better visualize its features with high-resolution synchrotron micro-computed tomography (µ-CT) and tabulated its mechanical performance through a variety of tests using computational software. The skeletal design of the cuttlebone consists of multiple layered chambers supported by wavy, pillar-like walls. It was revealed that the cuttlebone is remarkable due to its multiscale design: the asymmetric geometry of the walls are designed to tolerate considerable amounts of energy while a stiff construction; at the chamber level, variation of walls (number, pattern, and waviness amplitude) helps avoid complete destruction of the structure in the event of an excessive force; at the entire skeletal level, various of chamber heights reduces inflicted stress in concentrated regions of the cuttlebone. The wavy walls were also observed to retain a saddle-shaped curviness, versus simple flat, domed, or cylindrical shaped walls. This created an incentive to explore the effects of curvature on the structural integrity of brittle ceramic structures. We developed an effective way for generating walls with different curvatures and observed the mechanical performance of each wall by crushing them in computer simulations. It was identified that adding curvature to brittle walls prolonged the failure period significantly. While the cylindrical walls were found to be rather stiff, saddle-shaped walls, although not capable of withstanding as much force as flat or cylindrical walls, has a more progressive failure behavior meanwhile maintaining high energy absorption, hence the saddled walls of the cuttlebone to allow maintenance and self-repair in damaged regions.

This dissertation is concerned with a type of energy absorption device made of thin-walled tubes. The tubes will undergo plastic deformation when subjected to an impact loading, and therefore absorb kinetic energy. It has been found that, if the surface of a tube is pre-folded according to an origami pattern, the failure mode of the tube can be altered, leading to a noticeable increase in energy absorption while at the same time, reducing the force needed to initiate plastic deformation within the tube. The main work is presented in four parts. First of all, an experimental study of a type of previously reported thin-walled square tube with pre-manufactured pyramid patterns on the surface has been conducted. Quasi-static axial crushing tests show that the octagonal mode, although numerically proven to be efficient in terms of energy absorption, cannot be consistently triggered. Secondly, a new type of thin-walled tubular energy absorption device, known as the origami tube, which has origami pattern pre-fabricated on the surface, has been studied. A family of origami patterns has been designed for tubes with different profiles. The performances of a series of origami tubes with various configurations subjected to quasi-static axial crushing have been investigated numerically. It is found that a new failure mode, referred to as the complete diamond mode, can be triggered, and both over 50% increase in the mean crushing force and about 30% reduction in the peak force can be achieved in a single tube design in comparison with those of a conventional square tube with identical surface area and wall thickness. A theoretical study of the axial crushing of square origami tubes has been conducted and a mathematical formula has been derived to calculate the mean crushing force. Comparison between theoretical prediction and numerical results shows a good agreement. Quasi-static axial crushing experiments on several square origami tube samples have been carried out. The results show that the complete diamond mode is formed in the samples and both peak force reduction and mean crushing force increase are attained. Thirdly, a new type of curved thin-walled beam with pre-manufactured origami pattern on the surface, known as the origami beam, has been designed and analyzed. A numerical study of a series of origami beams with a variety of configurations subjected to quasi-static lateral bending has been conducted. The results show that two new failure modes, namely, the longitudinal folding mode and the mixed mode, can be induced, and both reduced peak force and increased energy absorption are achieved. Finally, a number of automobile frontal bumpers, which have the origami tube and the origami beam as key components, have been designed and analyzed. Three impact tests have been conducted on each bumper. The numerical results show that both types of origami structures can perform well in realistic loading scenarios, leading to improved energy absorption of the bumpers.

On March 13th, 2006, the Division of Electricity at Uppsala University deployed its first wave energy converter, L1, in the ocean southwest of Lysekil. L1 consisted of a buoy at the surface, connected through a line to a linear generator on the seabed. Since the deployment, continuous investigations of how L1 works in the waves have been conducted, and several additional wave energy converters have been deployed. This thesis is based on ten publications, which focus on different aspects of the interaction between wave, buoy, and generator. In order to evaluate different measurement systems, the motion of the buoy was measured optically and using accelerometers, and compared to measurements of the motion of the movable part of the generator - the translator. These measurements were found to correlate well. Simulations of buoy and translator motion were found to match the measured values. The variation of performance of L1 with changing water levels, wave heights, and spectral shapes was also investigated. Performance is here defined as the ratio of absorbed power to incoming power. It was found that the performance decreases for large wave heights. This is in accordance with the theoretical predictions, since the area for which the stator and the translator overlap decreases for large translator motions. Shifting water levels were predicted to have the same effect, but this could not be seen as clearly. The width of the wave energy spectrum has been proposed by some as a factor that also affects the performance of a wave energy converter, for a set wave height and period. Therefore the relation between performance and several different parameters for spectral width was investigated. It was found that some of the parameters were in fact correlated to performance, but that the correlation was not very strong. As a background on ocean measurements in wave energy, a thorough literature review was conducted. It turns out that the Lysekil project is one of quite few projects that have published descriptions of on-site wave energy measurements.

Accurate dosimetry is a fundamental requirement for the safe and efficient use of radiation in medical applications. International Codes of Practice, such as IAEA TRS-398 (2000) for radiotherapy beams and IAEA TRS-457 (2007) for diagnostic radiology beams, provide the necessary formulation for reference and relative dosimetry and the data required for their implementation. Research in recent years has highlighted the shortage of such data for radiotherapy small photon beams and for surface dose estimations in diagnostic and interventional radiology, leading to significant dosimetric errors that in some instances have jeopardized patient’s safety and treatment efficiency. The aim of this thesis is to investigate and determine key data for the reference and relative dosimetry of radiotherapy and radiodiagnostics beams. For that purpose the Monte Carlo system PENELOPE has been used to simulate the transport of radiation in different media and a number of experimental determinations have also been made. A review of the key data for radiotherapy beams published after the release of IAEA TRS-398 was conducted, and in some cases the considerable differences found were questioned under the criterion of data consistency throughout the dosimetry chain (from standards laboratories to the user). A modified concept of output factor, defined in a new international formalism for the dosimetry of small photon beams, requires corrections to dosimeter readings for the dose determination in small beams used clinically. In this work, output correction factors were determined, for Varian Clinac 6 MV photon beams and Leksell Gamma Knife Perfexion 60Co gamma-ray beams, for a large number of small field detectors, including air and liquid ionization chambers, shielded and unshielded silicon diodes and diamond detectors, all of which were simulated by Monte Carlo with great detail. Backscatter factors and ratios of mass energy-absorption coefficients required for surface (skin) determinations in diagnostic and interventional radiology applications were also determined, as well as their extension to account for non-standard phantom thicknesses and materials. A database of these quantities was created for a broad range of monoenergetic photon beams and computer codes developed to convolve the data with clinical spectra, thus enabling the determination of key data for arbitrary beam qualities. Data presented in this thesis has been contributed to the IAEA international dosimetry recommendations for small radiotherapy beams and for diagnostic radiology in paediatric patients. / <p>At the time of the doctoral defense, the following paper was unpublished and had a status as follows: Paper 6: Manuscript.</p>

Selective laser melting (SLM) is an additive manufacturing process which enables the creation of intricate components from high performance alloys. This facilitates the design and fabrication of new cellular materials for blast and impact mitigation, where the performance is heavily influenced by geometric and material sensitivities. Design of such materials requires an understanding of the relationship between the additive manufacturing process and material properties at different length scales: from the microstructure, to geometric feature rendition, to overall dynamic performance. To date, there remain significant uncertainties about both the potential benefits and pitfalls of using additive manufacturing processes to design and optimise cellular materials for dynamic energy absorbing applications. This investigation focuses on the out-of-plane compression of stainless steel cellular materials fabricated using SLM, and makes two specific contributions. First, it demonstrates how the SLM process itself influences the characteristics of these cellular materials across a range of length scales, and in turn, how this influences the dynamic deformation. Secondly, it demonstrates how an additive manufacturing route can be used to add geometric complexity to the cell architecture, creating a versatile basis for geometry optimisation. Two design spaces are explored in this work: a conventional square honeycomb hybridised with lattice walls, and an auxetic stacked-origami geometry, manufactured and tested experimentally here for the first time. It is shown that the hybrid lattice-honeycomb geometry outperformed the benchmark metallic square honeycomb in terms of energy absorption efficiency in the intermediate impact velocity regime (approximately 100 m/s). In this regime, the collapse is dominated by dynamic buckling effects, but wave propagation effects have yet to become pronounced. By tailoring the fold angles of the stacked origami material, numerical simulations illustrated how it can be optimised for specific impact velocity regimes between 10-150 m/s. Practical design tools were then developed based on these results.

This thesis presents the work of an experimental investigation into the impact damage resistance and damage tolerance for symmetrical and unsymmetrical composite honeycomb sandwich panels through in-plane compression. The primary aim of this research is to examine the impact damage resistance of various types of primarily carbon/epoxy skinned sandwich panels with varying skin thickness, skin lay-up, skin material, sandwich asymmetry and core density and investigate the residual in-plane compressive strengths of these panels with a specific focus on how the core of the sandwich contributes to the in-plane compressive behaviour. This aim is supported by four specifically constructed preconditions introduced into panels to provide an additional physical insight into the loading-bearing compression mechanisms. Impact damage was introduced into the panels over a range of IKEs via an instrumented drop-weight impact test rig with a hemi-spherical nosed impactor. The damage resistance in terms of the onset and propagation of various dominant damage mechanisms was characterised using damage extent in both impacted skin and core, absorbed energy and dent depth. Primary damage mechanisms were found to be impacted skin delamination and core crushing, regardless of skin and core combinations and at high energies, the impacted skin was fractured. In rare cases, interfacial skin/core debonding was found to occur. Significant increases in damage resistance were observed when skin thickness and core density were increased. The reduction trends of the residual in-plane compressive strengths of all the panels were evaluated using IKE, delamination and crushed core extents and dent depth. The majority of impact damaged panels were found to fail in the mid-section and suffered an initial decline in their residual compressive strengths. Thicker skinned and higher density core panels maintained their residual strength over a larger impact energy range. Final CAI strength reductions were observed in all panels when fibre fracture in the impacted skin was present after impact. Thinner skinned panels had a greater compressive strength over the thicker skinned panels, and panel asymmetry in thin symmetrical panels appeared to result in an improving damage tolerance trend as IKE was increased due to that the impact damage balanced the in-plane compressive resistance in the skins with respect to the pre-existing neutral plane shift due to the uneven skin thickness.

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Dans l’optique de la conception et du développement d’un siège aéronautique et afin derespecter la règlementation sécuritaire en vigueur, la structure du siège développé doitpermettre une dissipation rapide de l’énergie perçue en cas de crash aérien (Fig. 1), ceci dansle but de protéger les passagers. La majorité des systèmes intégrés à la structure des sièges etpermettant cette absorption d’énergie (Fig. 2) est constituée de composants métalliques qui sedéforment plastiquement pour dissiper l’énergie due au crash. Actuellement, l’industrie et larecherche se tournent vers les matériaux composites pour substituer de tels systèmes.Cependant le comportement de ces matériaux lors de sollicitations mécaniques sévères estfortement différent des matériaux métalliques, notamment dû au fait que les mécanismesd’endommagement sont très distincts.Le but de cette étude portant sur des structures tubulaires composites est d’évaluer leurcapacité à dissiper l’énergie. A cette fin, différentes stratifications ont été testées encompression (Fig. 3 et 4) dans le but de déterminer leur comportement, comparer leurspropriétés et calculer leurs valeurs de SEA (absorption d'énergie spécifique, en kJ.kg-1)servant à évaluer leur aptitude à dissiper l’énergie engendrée en cas de crash. Ces dernièressont issues des courbes effort-déplacement obtenues lors des essais d’écrasement (Fig. 5). Lesdifférents essais de compression ont été instrumentés et suivis au moyen de caméras rapides etdes images post-essais ont été réalisées par tomographie pour comprendre les mécanismesd’endommagement mis en jeu (Fig. 4 et 6). Ces essais ont été réalisés à vitesse de chargementquasi-statique puis dynamique et selon diverses conditions limites. Les différents résultats decomportement en compression sont également utilisés dans le but de construire et enrichir unmodèle de calcul par éléments finis (Fig. 7 et 8) permettant de simuler la réponse de structurescomposites de différentes natures soumises au crash en intégrant la géométrie et lacomposition de la structure (Fig. 8).L’objectif de ce travail de recherche est ainsi d’évaluer l’énergie pouvant être dissipée par desstructures tubulaires composites, de comparer les absorptions induites par des structurescomposites de compositions différentes, et/ou bi-matériaux, et enfin de fournir un modèleéléments finis représentant le comportement de structures composites en compression jusqu’àl’endommagement et la ruine de la structure.Il a ainsi été établi qu’en chargement statique, un stratifié unidirectionnel orienté à 0° etstabilisé par des plis de tissus répond fortement aux attentes en terme de dissipation d’énergie,mais pas en sollicitation dynamique. Dans ce cas, une stratification à 90° semble plusadéquate. D’autre part, un confinement forcé vers l’intérieur est avantageux dans la plupartdes cas, réduisant le pic d’effort initial sans diminuer drastiquement la valeur de SEA. / With the perspective of the design and development of an aircraft seat and in order to respectthe safety regulations in effect, the structure of the developed seat must allow for a swiftdissipation of the energy received in the event of an aircraft crash (Fig. 1) so as to protect thepassengers. The majority of systems integrated into the seats structure and allowing energydissipation (Fig. 2) consists of metal components that sustain plastic deformation to dissipatethe energy induced by the crash. Currently, industry and research sectors are turning theirfocus towards composite materials to substitute such systems. However, the behavior of thesematerials during severe mechanical stress is strongly different from metallic materials, inparticular due to the fact that damage mechanisms are very distinct.The purpose of this study on composite tubular structures is to evaluate their ability todissipate the energy. To this end, different laminate structures were tested in compression(Fig. 3 and 4) in order to identify their behavior, compare their properties and calculate theirSEA value (Specific Energy Absorption, in kJ.kg-1) used to evaluate their capacity to dissipatethe energy generated during a crash. Those are resulting from the load-displacement curvesobtained during the crushing tests (Fig. 5). The various compression tests were instrumentedand monitored by means of rapid imaging cameras and post-crushing tomographic imaginghas been realized in order to understand the damage mechanisms involved (Fig. 4 and 6).Testing has been carried out under quasi-static and dynamic loading and using severalboundary conditions. The different results of compression and crushing behavior are also usedin order to build and improve a finite element calculation model (Fig. 7 and 8) allowing tosimulate the response of composite structures of different natures subjected to crash byintegrating the geometry and the composition of the structure (Fig. 8).The objective of this research work is thus to evaluate the energy that can be dissipated bycomposite tubular structures, to compare the absorption values induced by compositestructures of different compositions, and/or bi-materials, and, finally, to provide a finiteelement model representing the behavior of composite structure submitted to compressionuntil damage and fracture of the structure.It has consequently been established that in static loading, a unidirectional laminate orientedat 0° and stabilized by woven plies strongly meets the expectations in terms of energydissipation, but that is not the case in dynamic loading. In this case, a 90° stratification seemsmore adequate. Incidentally, an inner constrained containment is more effective in most cases,reducing the initial peak load without drastically reducing the SEA value.