no / The complexity of powertrain calibration has increased significantly with the development and introduction of new technologies to improve fuel economy and performance while meeting increasingly stringent emissions legislation with given time and cost constraints. This paper presents research to improve the model-based engine calibration optimization using an integrated sequential Design of Experiments (DoE) strategy for engine mapping experiments. This DoE strategy is based on a coherent framework for a model building - model validation sequence underpinned by Optimal Latin Hypercube (OLH) space filling DoEs. The paper describes the algorithm development and implementation for generating the OLH space filling DoEs based on a Permutation Genetic Algorithm (PermGA), subsequently modified to support optimal infill strategies for the model building - model validation sequence and to deal with constrained non-orthogonal variables space. The development, implementation and validation of the proposed strategy is discussed in conjunction with a case study of a GDI engine steady state mapping, focused on the development of an optimal calibration for CO₂ and particulate number (Pn) emissions. The proposed DoE framework applied to the GDI engine mapping task combines a screening space filling DoE with a flexible sequence of model building - model validation mapping DoEs, all based on optimal DoE test plan augmentation using space filling criteria. The case study results show that the sequential DoE strategy offers a flexible way of carrying out the engine mapping experiments, maximizing the information gained and ensuring that a satisfactory quality model is achieved.

Fine-grained sediment accumulation in the interstices of gravel beds is a key factor in degrading riverine habitats. However, interstitial deposits are highly dynamic and are not sufficiently understood. This work enhances the understanding of interstitial fine sediment deposition by investigating interstitial storage and ingress, flow, suspended sediment and gravel bed character. Furthermore, this work introduces a numerical suspended sediment deposition model with the power to predict patterns of interstitial ingress. The investigation of interstitial deposition were carried out on two levels. Both data orginating from flume experiments and from three locations of the River Culm, Devon, UK was collected. The experimental data showed the significant influence of small scale variations in flow and bed character and their influence on interstitial ingress. The field investigation showed clear differences in interstitial fine-grained sediment for the different river reaches and an overall higher interstitial ingress compared to recent published data. The numerical model development was realised in a two-step approach. First, the model was coded and calibrated for the flume scale processes and, second, an upscaled reach scale model was devolped for the field data. This reach scale suspended sediment deposition model included flow information, for which depthaveraged two dimensional hydrodynamic models were developed with the software Delft3D. The overall explanatory power of the model at this state is not satisfactory with regards to local deposition distribution. A separate chapter discusses the possible causes and implications of this short coming for further research from a data aquisition and modelling perspective.

Les procédés conventionnels de transformation thermique de la biomasse sont conçus pour la production d’huiles ou de gaz riches en CO, CO2, H2 et hydrocarbures légers à des fins énergétiques ou chimiques. Le pilote de pyrolyse rapide utilisé dans cette étude comporte un réacteur cyclone, chauffé à ses parois, et capable de mettre en oeuvre la pyroliquéfaction ou la pyrogazéification par le simple jeu des conditions opératoires. Les produits de réaction (charbon, huiles et gaz) sont récupérés et analysés. Les bilans de matière massiques et élémentaires (C, H, O) bouclent de façon très satisfaisante. Les basses températures de paroi et faibles débits de gaz vecteur favorisent la pyroliquéfaction. La production d’huiles augmente avec le débit de biomasse. La taille des particules a une faible influence sur les sélectivités en gaz, liquides et charbon. Un modèle de fonctionnement du cyclone est établi en tenant compte de l’hydrodynamique des phases gaz et solide ainsi que des lois de transferts de chaleur paroi-gaz et paroi-solides dans le cyclone. Ce modèle inclut également un schéma cinétique de pyrolyse rapide intégré dans un modèle de décomposition de la particule, ainsi qu’un modèle de craquage des vapeurs. Validé successivement sur la cellulose puis sur le bois, il permet de prédire les variations des sélectivités en fonction des conditions opératoires. Le modèle montre que les réactions de craquage se déroulent majoritairement dans une mince couche limite proche des parois chaudes. On propose deux lois générales (pyrogazéification et pyroliquéfaction) regroupant les différents paramètres opératoires contrôlant les performances du réacteur / The usual processes of biomass thermal upgrading are designed for the production of bio-oils or of gases rich in CO, CO2, H2 and light hydrocarbons for energy or chemical productions. The laboratory-scaled set-up used in this study includes a cyclone reactor, heated at its walls and able to carry out the fast pyroliquefaction or pyrogazeification by simply changing the operating conditions. The reaction products (charcoal, liquids and gases) are recovered and analyzed. The masses and elementary (C, H, O) balances closures are very accurate. Pyroliquefaction conditions are favoured by low walls temperatures and small carrier gas flowrates. The bio-oils fractions increase with the biomass flowrate. The particles size has only a weak influence on gas, liquids and charcoal selectivities. A model representing the cyclone behaviour is established by taking into account the hydrodynamics of the gases and solids, and the wall-gas and wall-solids heat transfer laws inside the cyclone. This general model includes also a model of particle decomposition (scheme of fast pyrolysis in competition with heat transfers) and a model of vapours cracking. Validated successively with cellulose and then with wood, it allows to predict the variations of the selectivities according to the operating conditions. The model shows that the cracking reactions occur mainly inside a thin boundary layer close to the hot walls. Two laws (pyrogazeification and pyroliquefaction) gathering the various operational parameters that control the performances of the reactor are finally proposed