We combine the evanescent field (EF) sensing mechanism with the fiber loop ringdown (FLRD) sensing scheme to create FLRD-EF sensors. The EF sensor heads are fabricated by etching the cladding of a single-mode fiber (SMF), while monitoring the etching process by the FLRD technique in real-time, on-line with high control precision. The effect of the sensor head dimensions on the sensors' detection sensitivity and response time are investigated. The EF scattering (EFS) sensing mechanism is combined with the FLRD detection scheme to create a new type of fiber optic index sensor. The detection limit for an optical index change is 3.2×10-5. This is the highest sensitivity for a fiber optic index sensor so far, without using any chemical-coating or optical components at the sensor head. A new type of index-based biosensor using high sensitivity FLRDEFS technique to sense deoxyribonucleic acid (DNA) and bacteria (Escherichia coli) is created.

Optical fibers have been mostly used in fiber optic communications, imaging optics, sensing technology, etc. Fiber optic sensors have gained increasing attention for scientific and structural health monitoring (SHM) applications. In this study, fiber loop ringdown (FLRD) sensors were fabricated for scientific, SHM, and sensor networking applications. FLRD biosensors were fabricated for both bulk refractive index (RI)- and surface RI-based DNA sensing and one type of bacteria sensing. Furthermore, the effect of glucose oxidase (GOD) immobilization at the sensor head on sensor performance was evaluated for both glucose and synthetic urine solutions with glucose concentration between 0.1% and 10%. Detection sensitivities of the glucose sensors were achieved as low as 0.05%. For chemical sensing, heavy water, ranging from 97% to 10%, and several elemental solutions were monitored by using the FLRD chemical sensors. Bulk indexbased FLRD sensing showed that trace elements can be detected in deionized water. For physical sensing, water and cracking sensors were fabricated and embedded into concrete. A partially-etched single-mode fiber (SMF) was embedded into a concrete bar for water monitoring while a bare SMF without any treatment was directly embedded into another concrete bar for monitoring cracks. Furthermore, detection sensitivities of water and crack sensors were investigated as 10 ml water and 0.5 mm surface crack width, respectively Additionally fiber loop ringdowniber Bragg grating temperature sensors were developed in the laboratory; two sensor units for water, crack, and temperature sensing were deployed into a concrete cube in a US Department of Energy test bed (Miami, FL). Multi-sensor applications in a real concrete structure were accomplished by testing the six FLRD sensors. As a final stage, a sensor network was assembled by multiplexing two or three FLRD sensors in series and parallel. Additionally, two FLRD sensors were combined in series and parallel by using a 2×1 micro-electromechanical system optical switch to control sensors individually. For both configurations, contributions of each sensor to two or three coupled signals were simulated theoretically. Results show that numerous FLRD sensors can be connected in different configurations, and a sensor network can be built up for multiunction sensing applications.

Optical fibers are getting significant considerations in the field of the sensors and sensing beyond its applications in optical communications. Because of several advantages, e.g., low profile of the sensors, immunity to electromagnetic noises, the ability of multiplexing, etc., the use of the fiber optic sensor is increasing in the field of physical, chemical, and biomedical sensing. In this study, we have developed two new fiber optic sensors based on fiber loop ringdown technique (FLRD) and have demonstrated their applications in the field of sensing. In the first part of this study, we report on the development of a high-sensitivity FLRD strain sensor. For the design of the strain sensor, the fiber loop was cut at the middle, and then the two fiber ends from broken fiber loop were cleaved and aligned carefully to couple the light from one end to another end. Any strain during the measurement changes the alignment of the fiber ends, consequently, the ringdown time changes. With this scheme, the FLRD strain sensor has shown the strain detection limit of 65 nanostrain, which is five times better than any FLRD strain sensors reported in the literature. Furthermore, The FLRD strain sensors were successfully embedded into prestressed concrete-beams.The FLRD strain sensor was able to monitor stress on a post-tensioned rod, as well as the load applied on the concrete-beam during the three-point loading test, thus exhibiting immense potential in structural health monitoring. For the chemical sensor, a new scheme of interrogation for a fiber optic surface plasmon sensor was developed with the use of the FLRD technique. A gold nanolayer was deposited on an uncladded fiber section, and the fiber section was integrated into the FLRD system as a sensor head. The gold layer facilitates for increased interaction of sample of interest, with the light pulse confined in the fiber waveguide. Moreover, with the affinity of the gold with specific biomolecules, the sensor has the potential for applications in biochemical sensing. In the experiment, the SP-FLRD sensor was used for refractive index sensing, and index detection limit of 4.6×10-5 RIU was achieved.

Fiber loop ring down (FLRD) spectroscopy is a sensitive spectroscopic technique that is based on absorption and it is convenient for trace chemical detection. Different FLRD systems are being improved in order to increase their sensitivity. In FLRD spectroscopy, detection of a sample is done by measuring of a leaking light at each trip within an optical cavity. Intensity of leaking light has an exponential decay where it is reduced by absorption of sample and scattering of light. In this project, two FLRD set-ups at 1535 nm and 808 nm were designed. In both set-ups, optical fiber and optical fiber couplers are used to form a cavity. At 1535 nm, a FLRD set-up is constructed by utilizing a pulsed laser and used for characterization of thin films, various pure liquids and fluorescein solutions. Two different sensor regions are designed with free space collimators and ferrules for the measurement of thin films and liquids, respectively. The future endeavor of the set-up is improvement for reliability and reproducibility of the system. For visible and NIR regions, a fiber coupled laser with four colors as 642 nm, 785 nm, 808 nm and 852 nm laser is used to design of a FLRD set-up. 808 nm laser is selected to build a prototype of the FLRD system. The construction of a closed loop FLRD set-up is completed and the system is characterized. Ultimate aim in our project is to be able to do trace detection at visible and NIR regions where the chemical sensitivity is higher.

Optical fiber sensors have already been developed from the experimental stage to practical applications in the past 20 years. There is no doubt that this technology can bring a wealth of applications, ranging from sensors in medical industry, aerospace and wind-energy industries, through to distributed sensors in oil and gas industry. Among a large amount of physical and chemical parameters which optical fiber sensors could measure, temperature and strain are the most widely studied. This thesis presents several low-cost optical fiber sensor configurations primarily for temperature and strain measurement. Several basic optical fiber components which are good candidates as optical fiber sensors are used in our experiments, such as fiber Bragg gratings (FBGs), multimode fibers (MMFs), small-core dispersion compensation fibers (SCDCFs), high-birefringence fiber loop mirrors (HBFLMs), and polarization-maintaining photonic crystal fibers (PMPCFs). Temperature and strain cross sensitivity is a crucial issue when designing high performance optical fiber sensors, since most of the sensing components are both sensitive to temperature and strain. This would introduce an error when measuring each of them independently. We developed several schemes to overcome this problem by cascading an FBG and a section of MMF, inserting an FBG into an HBFLM, and space division multiplexing two HBFLMs. By measuring the wavelength shifts of the two independent components' spectra in each scheme, simultaneous measurement of temperature and strain could be achieved. However, all the above schemes need optical spectrum analyzers to monitor the spectral information, which increases the cost of the system and limits the operation speed. In order to avoid using optical spectrum analyzers, we use an intensity-based interrogation method with MMFs and HBFLMs as edge filters. By measuring power ratio changes, instead of monitoring spectra shifts, simultaneous measurement of temperature and strain could be realized with a low cost and high speed. The resolutions of the above five configurations are between 0.26 - 1.2 ^oC in temperature and 9.21 - 29.5 με in strain, which are sufficient for certain applications. We also investigate the sensing applications with the SCDCF. Since the cutoff wavelength of this kind of fiber is around 1663 nm, which makes it naturally an MMF in the wavelength range of 1550 nm. By slightly offsetting the core of the SCDCF with respect to that of the standard single-mode fiber (SMF), a high extinction ratio could be achieved with almost 9 dB. When a lateral force (lateral strain) applied on the SCDCF, extinction ratio will decrease. The change of the extinction ratio is almost independent of temperature variation. The measured extinction ratio change has a good quadratic relationship with respect to applied lateral force. This feature could be used to measure lateral force (lateral strain). In addition, we also use this feature to realize simultaneous measurement of both the longitudinal strain and lateral strain, since the applied longitudinal strain results in the whole spectrum shift. Moreover, a miniature high temperature sensor could also be made using the SCDCF. One end of a 4-mm long SCDCF is spliced directly to SMF with the other end cleaved. By monitoring the reflection spectrum of the SCDCF, temperature information could be obtained. This sensing head is very compact and could realize high temperature measurement up to 600 ^oC. Recently, a kind of PMPCF has been found to have very small responses to temperature change. This offers an opportunity to measure other parameters without considering temperature influence. We construct a compact 7-mm long transmission-type sensor with this kind of PMPCF. The interference spectrum generated by the coupling of cladding modes and core mode is obtained by slightly offsetting the PMPCF core to SMF core. The experiment shows that the interference spectrum is almost unchanged within the temperature range of 25-60 ^oC. The presented sensor has the potential to be used to measure strain and refractive index in the normal environment without temperature discrimination for practical applications.

Optical fiber sensors have already been developed from the experimental stage to practical applications in the past 20 years. There is no doubt that this technology can bring a wealth of applications, ranging from sensors in medical industry, aerospace and wind-energy industries, through to distributed sensors in oil and gas industry. Among a large amount of physical and chemical parameters which optical fiber sensors could measure, temperature and strain are the most widely studied. This thesis presents several low-cost optical fiber sensor configurations primarily for temperature and strain measurement. Several basic optical fiber components which are good candidates as optical fiber sensors are used in our experiments, such as fiber Bragg gratings (FBGs), multimode fibers (MMFs), small-core dispersion compensation fibers (SCDCFs), high-birefringence fiber loop mirrors (HBFLMs), and polarization-maintaining photonic crystal fibers (PMPCFs). Temperature and strain cross sensitivity is a crucial issue when designing high performance optical fiber sensors, since most of the sensing components are both sensitive to temperature and strain. This would introduce an error when measuring each of them independently. We developed several schemes to overcome this problem by cascading an FBG and a section of MMF, inserting an FBG into an HBFLM, and space division multiplexing two HBFLMs. By measuring the wavelength shifts of the two independent components' spectra in each scheme, simultaneous measurement of temperature and strain could be achieved. However, all the above schemes need optical spectrum analyzers to monitor the spectral information, which increases the cost of the system and limits the operation speed. In order to avoid using optical spectrum analyzers, we use an intensity-based interrogation method with MMFs and HBFLMs as edge filters. By measuring power ratio changes, instead of monitoring spectra shifts, simultaneous measurement of temperature and strain could be realized with a low cost and high speed. The resolutions of the above five configurations are between 0.26 - 1.2 ^oC in temperature and 9.21 - 29.5 με in strain, which are sufficient for certain applications. We also investigate the sensing applications with the SCDCF. Since the cutoff wavelength of this kind of fiber is around 1663 nm, which makes it naturally an MMF in the wavelength range of 1550 nm. By slightly offsetting the core of the SCDCF with respect to that of the standard single-mode fiber (SMF), a high extinction ratio could be achieved with almost 9 dB. When a lateral force (lateral strain) applied on the SCDCF, extinction ratio will decrease. The change of the extinction ratio is almost independent of temperature variation. The measured extinction ratio change has a good quadratic relationship with respect to applied lateral force. This feature could be used to measure lateral force (lateral strain). In addition, we also use this feature to realize simultaneous measurement of both the longitudinal strain and lateral strain, since the applied longitudinal strain results in the whole spectrum shift. Moreover, a miniature high temperature sensor could also be made using the SCDCF. One end of a 4-mm long SCDCF is spliced directly to SMF with the other end cleaved. By monitoring the reflection spectrum of the SCDCF, temperature information could be obtained. This sensing head is very compact and could realize high temperature measurement up to 600 ^oC. Recently, a kind of PMPCF has been found to have very small responses to temperature change. This offers an opportunity to measure other parameters without considering temperature influence. We construct a compact 7-mm long transmission-type sensor with this kind of PMPCF. The interference spectrum generated by the coupling of cladding modes and core mode is obtained by slightly offsetting the PMPCF core to SMF core. The experiment shows that the interference spectrum is almost unchanged within the temperature range of 25-60 ^oC. The presented sensor has the potential to be used to measure strain and refractive index in the normal environment without temperature discrimination for practical applications.

Cavity ring-down spectroscopy has been used over the last twenty years as a highly sensitive absorption spectroscopic technique to measure light attenuation in gases, liquids, and solid samples. An optical cavity is used as a multi-pass cell, and the decay time of the light intensity in the cavity is measured, thereby rendering the techniques insensitive to light intensity fluctuations. Optical waveguides are used to build the optical cavities presented in this work. The geometries of such waveguides permit the use of very small liquid sample volumes while retaining the advantages of cavity ring-down spectroscopy. In this thesis cavity ring-down measurements are conducted, both, in the time domain and by measuring phase-shifts of sinusoidally modulated light, and the two methods are theoretically connected using a simple mathematical model, which is then experimentally confirmed. A new laser driver, that is compatible with high powered diode lasers, has to be designed to be able to switch from time domain to frequency domain measurements. A sample path length enhancement within the optical cavity is explored with the use of liquid core waveguides. The setup was optimised with respect to the matrix liquid, the geometrical matching of waveguide geometries, and the shape of liquid core waveguide ends. Additionally, a new technique of producing concave lenses at fibre ends has been developed and the output of a general fibre lens is simulated. Finally, liquid core waveguides are incorporated into a fibre-loop ring-down spectroscopy setup to measure the attenuation of two model dyes in a sample volume of <1 µL. The setup is characterized by measuring concentrations of Allura Red AC and Congo Red from 1 µM to a limit of detection of 5 nM. The performance of the setup is compared to other absorption techniques measuring liquid samples. / Thesis (Ph.D, Chemistry) -- Queen's University, 2013-04-23 14:08:16.33