Steam exploded fibers from Yellow Poplar (Liriodendron tulipifera) wood were assessed in terms of (a) their impact on torque during melt processing of a thermoplastic cellulose ester (plasticized CAB); (b) their fiber incorporation and dispersion characteristics in a CAB-based composite by SEM and image analysis, respectively; and (c) their impact on the mechanical properties (under tension) of CAB-based composites having fiber contents of between 10 and 40% by weight. The fibers included water-washed steam exploded fibers (WEF), alkali-extracted fibers (AEF), acetylated fibers (AAEF), all from Yellow poplar (log Ro = 4.23), and oat fillers (COF) as control. The stepwise increase in cellulose content by extraction, and especially the (surface) modification by acetylation, contributed to increased torque during melt processing, and to improved interfacial adhesion as well as fiber dispersion. As compared to pure CAB, AAEF generated the highest increase in torque (+ 421%) followed by AEF (+ 260%) and WEF (+ 190%) at 40% fiber content by weight. AAEF was also found to enhance the tensile properties of the resulting composites. SEM studies of the tensile fracture surfaces indicated significant interfacial delamination and also pull - out of fibers when WEF, AEF, and COF were used to reinforce the CAB matrix. Composites with AAEF, by contrast, revealed fracture surfaces with reduced interfacial delamination and with significant fiber fracturing during failure. Image analysis was used to determine fiber dispersion within the resulting composites quantitatively. Significant improvement in fiber dispersion was achieved when the matrix was reinforced with acetylated fibers (AAEF). Fiber addition to the matrix resulted in loss of strain at break (- 80 to - 93%) and slight or significant increases in modulus (+ 47 to + 103%) depending on fiber type at 40% fiber content. Maximum stress declined for all fibers except AAEF at all fiber contents. AAEF-based composites revealed a decline in maximum stress when fiber content rose to 10%, and this reversed when fiber content increased beyond 10%. This increase in strength is consistent with the rule of mixtures that stipulates reinforcement of the matrix by fibers that are capable of transferring stresses across the fiber-matrix interface. All fibers suffered length decreases during melt processing. / Master of Science

Invention of silica based optical fiber not only led to revolution in communication but also provided fundamental basis for many research areas. One example area is distributed optical fiber sensing, which has been attracting research interests for decades. Optical fiber sensors are immune to electromagnetic interference, and resistant to corrosion and can endure harsh environment so they have found applications such as structural health monitoring, intrusion detection and oil downhole measurement. Significant research efforts have been paid to fiber sensing area, many techniques have been developed and some of them have been successfully demonstrated, however achieving both high-speed and long-range is still under intensive research. This dissertation proposes and demonstrates a technique with the capability of simultaneous long-range and high-speed sensing by employing serial ultra-weak fiber Bragg gratings (UW-FBGs) and dispersive components. Various factors which have influence on the system performance, including wavelength resolution, spatial resolution and sensing rate, are analyzed. Different types of light sources and dispersive units were designed and a sensing system was built. With this system, both static and dynamic response were measured, and a sensing link consisting of more than 2000 UW-FBGs was successfully measured at the speed of 20kHz. The noise sources of the system were also theoretically analyzed and experimentally measured. This demonstrated sensing technique can be applied to long range temperature and strain sensing. / Ph. D. / Optical fiber is a thin glass rod with normally two layers of slightly different silica. Because of its low loss, optical fiber can guide light for a long distance without causing significant signal fading. Modifications can be made to a small section of an optical fiber to form a fiber Bragg grating, whose optical characteristics are dependent on its temperature or the strain applied to it. This dissertation proposes a technique with the ability of measuring the temperature or strain of a long length of optical fiber which has large quantity of fiber Bragg gratings fabricated in it. Along with the capability of long range sensing, this technique also has high sensing speed. It has been demonstrated that the sensing system could perform measurement in every 50µs when the optical fiber has about 2000 fiber Bragg gratings in it. The resolution, if converted to temperature, is about 1.5°C and the accuracy is 2°C. With the ability of monitoring temperature or strain of a large span at high speed, this technique could be used in areas such as civil structure and air craft health monitoring, instruction detection and high speed temperature monitoring.

Due to dramatic growth of capacity in optical fiber communication, the fiber dispersion has become one of major factors affecting the quality of optical signal transmission with different modulation scheme, leading to the importance in controlling optical chirp. Among the elements used for optical fiber communications, electroabsorption modulator (EAM) and semiconductor optical amplifier (SOA) are served as optical amplitude and phase modulation. In this work, EAM-integrated SOA is used to realize the pre-chirp technique through their inherently reversed phase modulation as well as amplitude modulation. In the experiment, tunable optical filter and a 10Gb/s data pattern are used for extracting the frequency chirp of the timely signal. With the positive chirp operation in EAM, it is found that the overall chirp of EAM-integrated SOA can be varied from 3GHz to -9GHz by adjusting current injection through SOA. Also, as inspecting the 10Gb/s pattern, the pattern effect can also be controlled by the reversed carrier dynamics between EAM and SOA. Finally, a 10Gb/s data transmission with 43km transmission is demonstrated by using such pre-chirp technique, showing that such technique can be applied to other type signal processing.

Carbon ber composites have become popular in aerospace structures and applications due to their light weight, high strength, and high performance. Recently, scientists have begun investigating hybrid composites that include fibers and particulate fillers, since they allow for advanced tailoring of mechanical properties, such as improved fatigue life. This project investigated a hybrid carbon ber reinforced polymer (HCFRP) that includes carbon fiber and additional alumina nanoparticle fillers, which act as embedded nano stress-sensors. Utilizing the piezospectroscopic e ect, the photo-luminescent spectral signal of the embedded nanoparticles has been monitored as it changes with stress, enabling non-contact stress detection of the material. The HCRFPs stress-sensitive properties have been investigated in-situ using a laser source and a tensile mechanical testing system. Hybrid composites with varying mass contents of alumina nanoparticles have been studied in order to determine the e ect of particle content on the overall stress sensing properties of the material. Additionally, high resolution photo-luminescent maps were conducted of the surfaces of each sample in order to determine the particulate dispersion of samples with varying alumina content. The dispersion maps also served as a method of quantifying particulate sedimentation, and can aid in the improvement of the manufacturing process. The results showed that the emitted photo-luminescent spectrum can indeed be captured from the embedded alumina nanoparticles, and exhibits a systematic trend in photo-luminescent peak shift with respect to stress. The stress maps showed a linear increase in peak shift up to a certain critical stress, and matched closely with the DIC strain results. Therefore, the non-contact stress sensing results shown in this work have strong implications for the future of structural health monitoring and nondestructive evaluation (NDE) of aerospace structures.

The master theses deals with a detailed analysis of optical fiber sensors. Specifically, there are discussed optical fibers, various types of sensors and realization optical fiber senzor and senzor system that has been optimized and processed data in real time. In master theses also describes the LabView programming enviroment and uses components, including the entire sensor systém of a sensors system that sends measured data

In den letzten Jahrzehnten ist das globale Kommunikationssystem in einem immer größerem Maße ein integraler Bestandteil des täglichen Lebens geworden. Optische Kommunikationssysteme sind die technologische Basis für diese Entwicklung. Nur Fasern können die riesige benötigte Bandbreite bereitstellen. Während für die ersten optischen Übertragungssysteme die Faser als "flacher" Kanal betrachtet werden konnte, machen Wellenlängenmultiplex und steigende Übertragungsraten die Einbeziehung von immer mehr physikalischen Effekten notwendig. Bei einer Erhöhung der Kanaldatenrate auf 40 Gbit/s und mehr ist die statische Kompensation von chromatischer Dispersion nicht mehr ausreichend. Die intrinsische Toleranz der Modulationsformate gegenüber Dispersion nimmt quadratisch mit der Symbolrate ab. Daher können beispielsweise durch Umwelteinflüsse hervorgerufene Dispersionsschwankungen die Dispersionstoleranz der Modulationsformate überschreiten. Dies macht eine adaptive Dispersionskompensation notwendig, was gleichzeitig auch Dispersionsmonitoring erfordert, um den adaptiven Kompensator steuern zu können. Vorhandene Links können mit Restdispersionskompensatoren ausgestattet werden, um sie für Hochgeschwindigkeitsübertragungen zu ertüchtigen. Optische Kompensationstechniken sind unabhängig von der Kanaldatenrate. Daher wird eine Erhöhung der Datenrate problemlos unterstützt. Optische Kompensatoren können WDM-fähig gebaut werden, um mehrere Kanäle auf einmal zu entzerren. Das Buch beschäftigt sich mit optischen Delay-Line-Filtern als eine Klasse von optischen Kompensatoren. Die Filtersynthese von solchen Delay-Line-Filtern wird behandelt. Der Zusammenhang zwischen optischen Filtern und digitalen FIR-Filtern mit komplexen Koeffizienten im Zusammenhang mit kohärenter Detektion wird aufgezeigt. Iterative und analytische Methoden, die die Koeffizienten für dispersions- und dispersions-slope-kompensierende Filter produzieren, werden untersucht. Genauso wichtig wie die Kompensation von Dispersion ist die Schätzung der Dispersion eines Signals. Mit Delay-Line-Filtern können die Restseitenbänder eines Signals genutzt werden, um die Dispersion zu messen. Alternativ kann nichtlineare Detektion angewandt werden, um die Pulsverbreiterung, die hauptsächlich von der Dispersion herrührt, zu schätzen. Mit gemeinsamer Dispersionskompensation und Dispersionsmonitoring können Dispersionskompensatoren auf die Signalverzerrungen eingestellt werden. Spezielle Eigenschaften der Filter zusammen mit der analytischen Beschreibung können genutzt werden, um schnelle und zuverlässige Steueralgorithmen zur Filtereinstellung bereitzustellen. Schließlich wurden Prototypen derartiger faseroptischen Kompensatoren von chromatischer Dispersion und Dispersions-Slope hergestellt und charakterisiert. Die Einheiten und ihr Systemverhalten wird gezeigt und diskutiert. / Over the course of the past decades, the global communication system has become a central part of people's everyday lives. Optical communication systems are the technological basis for this development. Only fibers can provide the huge bandwidth that is required. Where the fiber could be regarded as a flat channel for the first optical transmission systems wavelength multiplexing and increasing line rates made it necessary to take more and more physical effects into account. When the line rates are increased to 40 Gbit/s and higher static chromatic dispersion compensation is not enough. The modulation format's intrinsic tolerance for dispersion decreases quadratically with the symbol rate. Thus, environmentally induced chromatic dispersion fluctuations may exceed the dispersion tolerance of the modulation formats. This makes an adaptive dispersion compensation necessary implying also the need for a monitoring scheme to steer the adaptive compensator. Legacy links that are CD-compensated by DCFs can be upgraded with residual dispersion compensators to make them ready for high speed transmission. Optical compensation is independent from the line rate. Hence, increasing the data rates is inherently supported. Optical compensators can be built WDM ready compensating multiple channels at once. The book deals with optical delay line filters as one class of optical compensators. The filter synthesis of such delay line filters is addressed. The connection between optical filters and digital FIR filters with complex coefficients that are used in conjunction with coherent detection could be shown. Iterative and analytical methods that produce the coefficients for dispersion (and also dispersion slope) compensating filters are researched. As important as the compensation of dispersion is the estimation of the dispersion of a signal. Using delay line filters, the vestigial sidebands of a signal can be used to measure the dispersion. Alternatively, nonlinear detection can be used to estimate the pulse broadening which is caused mainly by dispersion. With dispersion compensation and dispersion monitoring, dispersion compensators can be adapted to the signal's impairment. Special properties of the filter in conjunction with an analytical description can be used to provide a fast and reliable control algorithm for setting the filter to a given dispersion and centering it on a signal. Finally, prototypes of such fiber optic chromatic dispersion and dispersion slope compensation filters were manufactured and characterized. The device and system characterization of the prototypes is presented and discussed.