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In this thesis, my main focus was to establish a novel composite-cavity fibre laser (CCFL) and to apply it in sensing, particularly in the hydrophone application. The CCFL that I have proposed is formed by writing three wavelength matched fibre Bragg gratings directly into a continuous length of doped fibre. I have also examined the relative advantages and disadvantages of interferometric and intensity-based hydrophone systems, and have established a hydrophone system that can be switched between the two modes of operation, by making use of digital signal processing. I have established a theoretical model to study the lasing and spectral characteristics of the CCFL. My analysis showed that whilst the CCFL have significantly different phase and threshold conditions from the common semiconductor diode lasers with external cavity, the CCFL also have mode-limiting properties that are often sought after. Through simulations, I was able to identify that a non-uniform straining scheme, that is, when one of the sub-cavities of the CCFL is restrained from strain, can improve the sensitivity with respect to existing single cavity fibre lasers, in both the frequency and intensity domains. My simulations also showed that the sensitivity of such a straining scheme can be optimised by tuning the reflectivity of the gratings, sub-cavity lengths, doping concentration and pump power. I have fabricated multiple CCFLs using the in-house grating writing facilities, and have experimentally assessed their power and spectral related lasing characteristics. Whilst having a significantly longer total cavity length compared to typical fibre lasers, the CCFLs demonstrated stable single longitudinal mode operation and narrow linewidth in the order for a few tens of kHz. Asymmetric output power and frequency as a result of unequal sub-cavity lengths were also examined. Finally, I conducted sensing experiments by applying the CCFLs in strain monitoring and intensity-based hydrophone. My results showed that the non-uniform straining scheme had significantly improved the intensity response of the CCFL, and that the acoustic pressure and frequency can be determined by directly sampling and applying Fourier transform to the output intensity of the fibre laser.

In this thesis, my main focus was to establish a novel composite-cavity fibre laser (CCFL) and to apply it in sensing, particularly in the hydrophone application. The CCFL that I have proposed is formed by writing three wavelength matched fibre Bragg gratings directly into a continuous length of doped fibre. I have also examined the relative advantages and disadvantages of interferometric and intensity-based hydrophone systems, and have established a hydrophone system that can be switched between the two modes of operation, by making use of digital signal processing. I have established a theoretical model to study the lasing and spectral characteristics of the CCFL. My analysis showed that whilst the CCFL have significantly different phase and threshold conditions from the common semiconductor diode lasers with external cavity, the CCFL also have mode-limiting properties that are often sought after. Through simulations, I was able to identify that a non-uniform straining scheme, that is, when one of the sub-cavities of the CCFL is restrained from strain, can improve the sensitivity with respect to existing single cavity fibre lasers, in both the frequency and intensity domains. My simulations also showed that the sensitivity of such a straining scheme can be optimised by tuning the reflectivity of the gratings, sub-cavity lengths, doping concentration and pump power. I have fabricated multiple CCFLs using the in-house grating writing facilities, and have experimentally assessed their power and spectral related lasing characteristics. Whilst having a significantly longer total cavity length compared to typical fibre lasers, the CCFLs demonstrated stable single longitudinal mode operation and narrow linewidth in the order for a few tens of kHz. Asymmetric output power and frequency as a result of unequal sub-cavity lengths were also examined. Finally, I conducted sensing experiments by applying the CCFLs in strain monitoring and intensity-based hydrophone. My results showed that the non-uniform straining scheme had significantly improved the intensity response of the CCFL, and that the acoustic pressure and frequency can be determined by directly sampling and applying Fourier transform to the output intensity of the fibre laser.

Thesis (MSc (Physics))--University of Stellenbosch, 2009. / The role fulfilled by theoretical models is rapidly increasing due to lasers becoming appli- cation driven to satisfy certain criteria and demands. Construction of high precision lasers requires good theoretical models and consequently good approximations of the parameters that such models are based upon. Despite the di erent model formalisms, most share a com- mon set of input parameters, including fibre waveguiding properties, input powers, transition cross-sections and overlaps between guided modes and the dopand distribution. Experimental and numerical work which was aimed at obtaining the wide-band emission and absorption cross-sections of fibre indirectly by means of the Giles parameters was done. The Giles parameters were used rather than the well known ionic cross-sections primarily because of the convenient encapsulation of the cumbersome overlap factors and the ionic cross-sections within the Giles parameters. The wide band spectral characteristics of the Giles parameters are indispensable in the design of fibre lasers and amplifiers, as they form the key parameters for laser models. These parameters are normally obtained utilizing absorption spectroscopy to obtain the absorption cross-sections and models such as the Fuchtbauer Ladenberg relation, the Mc- Cumber relation or uorescence spectroscopy to obtain the emission cross-sections. Recent research however indicates that these methods are inaccurate in certain spectral regions. An investigation was launched to extract the Giles parameters from measurements of the ampli- fied spontaneous emission (ASE) and pump absorption in ytterbium-doped fibre for several lengths of fibre and subsequent computer simulations, utilizing an ampli fier model. The Giles parameters are extracted with a fitting algorithm that adjusts the relevant numerical values to minimize the least square difference between the numerical data obtained from the amplifier model and the measured data. Using the model devised in this project on literature data, the Giles parameters were extracted and compared to the Giles parameters extracted in literature on the same data. This comparison conforms the extraction of the Giles parameters, utilizing the model devised in this project, as successful. Subsequently the model devised in this project was applied to extract the Giles parameters from experimental data measured at Stellenbosch, using a double cladding ytterbium-doped fibre. Finally a fibre laser was built utilizing the double cladding ytterbium-doped fibre and the output was measured. The Giles parameters extracted were then used in a fibre laser model to calculate the output and compare it to the measurements taken. This served as suffcient verification that the Giles parameters extracted can be used to model a fibre laser effciently.

The commissioning and development of a laser-wire transverse electron beam profile monitor at the Accelerator Test Facility 2 in Japan is presented. The experimental setup used including a gigawatt laser system is detailed and characterised. Results from data taking in December 2010 are presented detailing the use of the laser-wire to tune the electron beam. In conjunction with this, the use of a fibre-based laser system as a suitable laser source for a laser-wire is discussed. A test bed fibre laser system was constructed to investigate the suitability of fibre lasers and the results are presented demonstrating high efficiency and excellent spatial quality. From this, a laser system capable of high resolution and high repetition intra-train scanning for demonstration at the Accelerator Test Facility 2 was designed, constructed and characterised. A commercial fibre laser system was extended using a photonic crystal fibre where periodic amplification designed to match the duty cycle of an accelerator was used advantageously to achieve higher than normal pulse energies. The results and techniques developed to measure them are presented.

Processing of Si in the semiconductor and solar cell industry has been dominated by the Diode Pumped Solid State (DPSS) Ultraviolet (UV) laser. Recent advances in laser source technology have produced fibre lasers with Master Oscillator Power Amplifier (MOPA) architectures that offer high repetition rates, high operational efficiencies, and pulse modulation controls exceeding those of typical Q-switched DPSS lasers. The aim of this research is to investigate 1 μm fibre laser machining of Si with a view to identifying the influential laser parameters for optimum processing of high quality, high efficiency micro drilling and surface texturing applications. A secondary aim is to develop a greater understanding of the laser material interactions and material removal mechanism when using fast rise-time nanosecond laser pulse envelopes. The IR fibre laser was able to perform percussion drilling and single pulse machining on the polished Si over a range of intensities up to 1.22 GW/cm2. With the optimum parameters, the micro-sized holes generated by the IR laser have a well defined edge, no heavy recast and no cracks. With a pulse shape of fast rise time (<7.5 ns for a 10-90% rise in signal), a high front peak power zone (approaching 14 kW) and an energetic long tail (40-180 ns), the absorption coefficient of Si at IR wavelength increased dramatically with time and temperature due to the fact that the liquid Si has a metal like absorption behavior. As a result, Si was quickly melted and the rest of pulse energy was able to remove the liquid Si effectively. The machining process left a limited amount of resolidified melt droplets and vapor condensates, which could be washed off ultrasonically. The drilling process was energy efficient when melt expulsion dominated the machining mechanism (0.08-0.2 mJ pulse energy depending on the pulse durations). The low energy pulse (~0.2 mJ) can achieve similar depth as the high energy pulse (~0.7 mJ), so high repetition rates of 100 kHz can be used to instead of 25 kHz, resulted in high processing speed. In addition, by comparing the single pulse machining with the state of the art UV laser, the IR fibre laser machined deeper features and better surface finish in the pulse energy region of >0.07 mJ. With the pulse shaping capability, the material properties can be varied and the wavelength factor can be minimized. The results suggest that applications like microvia drilling can now be carried out with the more flexible and low cost IR fibre laser. The increased repetition rates of fibre laser can increase production speed to satisfy the needs of drilling ~10 thousands holes per second, required by the modern semiconductor and solar cell production. The shortened optical penetration length of 1 μm wavelength laser on Si with increasing temperature and sufficient thermal diffusion length resulted from the asymmetrical fibre laser pulse and the dynamic properties of Si produced a thick liquid layer. A one-dimensional heat conduction model based on the surface heating source predicted that this superheated liquid layer was able to stay above 4706 K (0.905 times the thermal critical temperature 5200 K of Si) for longer than 70 ns to induce explosive boiling. This proposed material removal mechanism was also confirmed by the shadowgraph images, showing particulates ejection lasting up to ten microseconds after the laser pulse. The estimated hole depth based on the explosive boiling alone were different from the measured ones at varying peak power densities (<1.22 GW/cm2) but fixed pulse duration (200 ns), since Si was removed by a mixture of mechanisms. With varying pulse durations (40-200 ns) but fixed peak power density (~0.63 GW/cm2), the estimated depth based on the explosive boiling was in close agreement with the measured ones (6% difference on average). The SEM images at this power density showed a micron- /submicron-sized debris field, which was also observed with the explosive boiling in the past. Although the improved quality of Si machining was demonstrated with the 1 μm MOPA based fibre laser, the setup of this system was only applicable to surface texturing, blind holes and through holes of less than 100 μm in depth. Further research is required to demonstrate the capability of more energetic pulse with higher peak power and large pulse duration range to explore more machining options.

Laser technologies have made distinguished contributions to modern industry. These have typically been realised through the important role played by lasers in the advancement of manufacturing technology in many areas such as welding, which has become an important joining technique and thus promoted the use of lasers in a wide variety of applications in the oil, gas, aerospace, aircraft, automotive, electronics and medical industries. A detailed review of previous work in the use of lasers for advanced manufacturing, and in particular, laser beam welding is given. The work reported in this thesis aims to develop a new method of laser welding. This is connected with investigations relating to the production of net shape welds for bead-on-plate welding and butt welding of mild steel plates. Based on the nature of its operation, use of a fibre laser was considered most suitable compared to other solid state lasers. Net-shape welds were demonstrated on mild steel plates using an IPG 1 kW single mode fibre laser with a maximum power output of 1000 W.The thesis shows results from experimental and modelling (based on finite element and computational fluid dynamic modelling) to validate the idea and the understanding of underlying scientific principles. The thesis is presented in the form of a collection of published work generated by the author during the course of this project. In addition, some results that are not yet published are also included. Design of experiments and statistical modelling has been used in the experimental work to understand the process parameter interactions. Microstructural and mechanical testing have been carried out to evaluate the performance of the welds. Net shaped (the weld bead is flat to the parent material surface) welds have been achieved and compared with standard welds. The understanding of net-shape weld formation and the effect of the laser welding parameters was enhanced by the theoretical modelling. The thesis concludes with a summary of scientific findings and an overview of future work.

Coherent Raman microscopy (CRM) is a powerful nonlinear optical imaging technique based on contrast via Raman active molecular vibrations. CRM has been used in domains ranging from biology to medicine to geology in order to provide quick, sensitive, chemical-specific, and label-free 3D sectioning of samples. The Raman contrast is usually obtained by combining two ultrashort pulse input beams, known as Pump and Stokes, whose frequency difference is adjusted to the Raman vibrational frequency of interest. CRM can be used in conjunction with other imaging modalities such as second harmonic generation, fluorescence, and third harmonic generation microscopy, resulting in a multimodal imaging technique that can capture a massive amount of data. Two fundamental elements are crucial in CRM. First, a laser source which is broadband, stable, rapidly tunable, and low in noise. Second, a strategy for image analysis that can handle denoising and material classification issues in the relatively large datasets obtained by CRM techniques. Stimulated Raman Scattering (SRS) microscopy is a subset of CRM techniques, and this thesis is devoted entirely to it. Although Raman imaging based on a single vibrational resonance can be useful, non-resonant background signals and overlapping bands in SRS can impair contrast and chemical specificity. Tuning over the Raman spectrum is therefore crucial for target identification, which necessitates the use of a broadband and easily tunable laser source. Although supercontinuum generation in a nonlinear fibre could provide extended tunability, it is typically not viable for some CRM techniques, specifically in SRS microscopy. Signal acquisition schemes in SRS microscopy are focused primarily on detecting a tiny modulation transfer between the Pump and Stokes input laser beams. As a result, very low noise source is required. The primary and most important component in hyperspectral SRS microscopy is a low-noise broadband laser source. The second problem in SRS microscopy is poor signal-to-noise (SNR) ratios in some situations, which can be caused by low target-molecule concentrations in the sample and/or scattering losses in deep-tissue imaging, as examples. Furthermore, in some SRS imaging applications (e.g., in vivo), fast imaging, low input laser power or short integration time is required to prevent sample photodamage, typically resulting in low contrast (low SNR) images. Low SNR images also typically suffer from poorly resolved spectral features. Various de-noising techniques have been used to date in image improvement. However, to enable averaging, these often require either previous knowledge of the noise source or numerous images of the same field of view (under better observing conditions), which may result in the image having lower spatial-spectral resolution. Sample segmentation or converting a 2D hyperspectral image to a chemical concentration map, is also a critical issue in SRS microscopy. Raman vibrational bands in heterogeneous samples are likely to overlap, necessitating the use of chemometrics to separate and segment them. We will address the aforementioned issues in SRS microscopy in this thesis. To begin, we demonstrate that a supercontinuum light source based on all normal dispersion (ANDi) fibres generates a stable broadband output with very low incremental source noise. The ANDi fibre output's noise power spectral density was evaluated, and its applicability in hyperspectral SRS microscopy applications was shown. This demonstrates the potential of ANDi fibre sources for broadband SRS imaging as well as their ease of implementation. Second, we demonstrate a deep learning neural net model and unsupervised machine-learning algorithm for rapid and automated de-noising and segmentation of SRS images based on a ten-layer convolutional autoencoder: UHRED (Unsupervised Hyperspectral Resolution Enhancement and De-noising). UHRED is trained in an unsupervised manner using only a single (“one-shot”) hyperspectral image, with no requirements for training on high quality (ground truth) labelled data sets or images.

This thesis concerns experimental investigations of laser cutting and piercing, with theoretical and practical discussions of the results. The thesis is made up of an introduction to laser cutting and six scientific Papers. These Papers are linked in such a way that each of them studies a different aspect of laser cutting: process efficiency in Paper I, morphology and melt flow on the laser cut front in Papers II, III and IV and laser piercing in Papers V and VI. Paper I investigates the effect of material type, material thickness, laser wavelength, and laser power on the efficiency of the cutting process for industrial state-of-the-art CO2 and fibre laser cutting machines. Here the cutting efficiency is defined in its most fundamental terms: as the area of cut edge created per Joule of laser energy. In Paper II a new experimental technique is presented which has been developed to enable high speed imaging of laser cut fronts produced using standard, commercial parameters. The results presented here suggest that the cut front produced when cutting 10 mm thick medium section stainless steel with a fibre laser and a nitrogen assist gas is covered in humps which themselves are covered in a thin layer of liquid. Paper III presents numerical simulations of the melt flow on a fibre laser ablation-driven processing front during remote fusion cutting, RFC. The simulations were validated with high speed imaging observations of the processing front. The simulation results provide explanations of the main liquid transport mechanisms on the processing front, based on information on the temperature, velocity and pressure fields involved. The results are of fundamental relevance for any process governed by a laser ablation induced front. In Paper IV cutting fronts created by CO2 and fibre lasers in stainless steel at thicknesses between 2 mm and 10 mm have been ‘frozen’ and their geometry has been measured. The resulting three-dimensional shapes have been curve fitted as ninth order polynomials. Various features of the cutting front geometry are discussed, including the lack of correlation of the cut front inclination with either the relevant Brewster angle or the inclination of the striations on the cut edge. In this paper, mathematical descriptions of the cutting fronts are obtained, which can be used as input parameters by any researcher in the field of laser cutting simulations. Paper V investigates the subject of laser piercing. Before any cut is started the laser needs to pierce the material. In this paper the laser piercing process is investigated using a wide range of laser pulse parameters, for stainless steel using a fibre laser. The results reveal the influence of pulse parameters on pierce time and pierced hole diameter. A high speed imaging camera was used to time the penetration event and to study the laser-material interactions involved in drilling the pierced holes. In Paper VI a ‘dynamic’ or ‘moving beam’, laser piercing technique is introduced for processing 15 mm thick stainless steel. One important aspect of laser piercing is the reliability of the process because industrial laser cutting machines are programmed for the minimum reliable pierce time. In this work a comparison was made between a stationary laser and a laser which moves along a circular trajectory with varying processing speeds. High speed imaging was employed during the piercing process to understand melt behavior inside the pierce hole. Throughout this work experimental techniques, including advanced high speed imaging, have been used in conjunction with simulations and theoretical analysis, to provide new knowledge for understanding and improving laser beam cutting and its associated piercing process.

Les lasers ultra-rapides fibrés sont aujourd’hui incontournables dans de nombreuses applications industrielles et scientifiques du fait de leur stabilité, de leur compacité et des hautes puissances disponibles. Les performances actuelles, rendues accessibles par le développement de fibres à larges aires modales et le concept d’amplification à dérive de fréquence, sont toutefois complexes à mettre oeuvre et limitées par l’utilisation de composants massifs pour les étapes de compression et d’étirement des impulsions. Ces travaux de thèse, à la fois expérimentaux et numériques, avaient pour objectif d’explorer des régimes dynamiques originaux basés sur l’utilisation de fibres actives spécifiques combinant large aire modale et propriétés dispersives adéquates pour la génération d’impulsions ultra-courtes de haute énergie. Les études numériques ont ainsi permis de montrer que des régimes impulsionnels à haute dispersion normale pouvaient être atteints en exploitant les phénomènes de résonnance et de couplage de modes dans des fibres de Bragg ou à profil en W. L’étude de l’influence des paramètres de la cavité laser sur le mécanisme de verrouillage de modes a permis d’identifier des configurations attractives pour la montée en puissance. La mise en oeuvre expérimentale de ces concepts a notamment permis le développement d’une source laser à soliton dissipatif produisant des impulsions énergétiques (38 nJ, 700 fs après compression) à des longueurs d’ondes autour de 1560 nm, record pour ce type d’oscillateur. La réalisation expérimentale de sources ultra-rapides basées sur des fibres actives spécifiques combinées au phénomène de couplage de mode ont permis d’identifier les potentialités et limitations de ces architectures originales à fortes dispersions totales pour la montée en énergie. / Ultrafast fiber lasers represent today a ubiquitous technology in various industrial and research applications thanks to their inherent advantages such as compactness, stability and high power. The best performances to date, mostly relying on large mode area fibers and chirped pulse amplification, however require complex experimental developments and are limited by the use of bulk components for pulse stretching and compression. The experimental and numerical work presented in this PhD thesis aimed at exploring original dynamical regimes based on specific active fibers combining large mode area and high dispersions for the generation of high-energy ultra-short pulses. The numerical studies then showed that pulsed regimes with high normal dispersions could be reached by exploiting resonance and mode-coupling phenomena in Bragg or W-type fibers. Studying the influence of the cavity parameters on mode-locking mechanisms allowed to target attractive configurations for energy scaling. The experimental implementation of this concept allowed the development of a dissipative soliton source delivering record high-energy chirped pulses (38 nJ, 700 fs after compression) at 1560 nm. The realization of ultrafast sources based on specific active fibers combined to mode-coupling phenomena then brought the possibility to identify the potentiality and limitations of these particular architectures with high dispersions for energy scaling.