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Heat treatment processes are used to develop the desired mechanical properties for steels. Unfortunately, heat treatment, especially quenching, can cause distortion. Failure to meet geometry specifications can result in extensive rework or rejection of the parts. A series of quenching simulations, using DANTE, have been conducted on an AISI 4140 steel Navy C-ring distortion coupon and a WPI designed plate with a hole to determine the effects of quenching process parameters including part geometry, agitation during quenching, and quench start temperatures on distortion. The heat transfer coefficients (HTC) of the quenchant with selected pump speeds were measured by CHTE quench probe system, which is the key input for heat treatment simulation. The maximum HTC of the quenching oil was increased from 2350 W/m2K to 2666 W/m2K with higher pump speed. Quenching experiments were also conducted. It was found that the experimental measured gap opening of the standard Navy C-rings increased from 0.307mm without agitation to 0.536mm at a high agitation. Quench start temperature does not have a significant effect on the gap opening. The experimental results showed good agreement with simulation results. The important processing parameter identification was conducted using design of experiments (DoE) coupled with analysis of variance (ANOVA). The effect of processing parameters in decreasing order of importance were determined to be: quenchant type, part geometry, agitation speed, quenching orientation, quenchant temperature, immersion rates, and quench starts temperature. Based on the simulation and experimental results, it was found that the two most import parameters are: 1. The part geometry and size (product design) 2. The temperature dependent heat transfer coefficients between the part and the quenchant (process design) The coupling of these product and process parameters is necessary to apply the systems analysis that must be accomplished to understand the interaction between the part design and process design parameters. This coupling can be accomplished by locally applying the well-known Biot number. Bi (T) = h(T) * L / k(T) Where h(T) = film coefficient or convective heat transfer coefficient [W/m2*K]. LC = characteristic length, which is generally described as the volume of the body divided by the surface area of the body [m]. k(T) = thermal conductivity of the body [W/m*k] The concept of a local Biot number is introduced to quantify the local variations of part size, geometry and heat transfer coefficient. First, a large Bi indicates large temperature gradients within the part. Second, large local (geometry dependent) variations in Bi number will lead to large lateral temperature gradients. Therefore, variations in local Bi can lead to large temperature gradients and therefore high stress during quenching and finally distortion. This local Bi concept can be used in a systems approach to designing a part and the quenching system. This systems approach can be designated as design for heat treating.

Heat treatment processes are used to develop the desired mechanical properties for steels. Unfortunately, heat treatment, especially quenching, can cause distortion. Failure to meet geometry specifications can result in extensive rework or rejection of the parts. A series of quenching simulations, using DANTE, have been conducted on an AISI 4140 steel Navy C-ring distortion coupon and a WPI designed plate with a hole to determine the effects of quenching process parameters including part geometry, agitation during quenching, and quench start temperatures on distortion. The heat transfer coefficients (HTC) of the quenchant with selected pump speeds were measured by CHTE quench probe system, which is the key input for heat treatment simulation. The maximum HTC of the quenching oil was increased from 2350 W/m2K to 2666 W/m2K with higher pump speed. Quenching experiments were also conducted. It was found that the experimental measured gap opening of the standard Navy C-rings increased from 0.307mm without agitation to 0.536mm at a high agitation. Quench start temperature does not have a significant effect on the gap opening. The experimental results showed good agreement with simulation results. The important processing parameter identification was conducted using design of experiments (DoE) coupled with analysis of variance (ANOVA). The effect of processing parameters in decreasing order of importance were determined to be: quenchant type, part geometry, agitation speed, quenching orientation, quenchant temperature, immersion rates, and quench starts temperature. Based on the simulation and experimental results, it was found that the two most import parameters are: 1. The part geometry and size (product design) 2. The temperature dependent heat transfer coefficients between the part and the quenchant (process design) The coupling of these product and process parameters is necessary to apply the systems analysis that must be accomplished to understand the interaction between the part design and process design parameters. This coupling can be accomplished by locally applying the well-known Biot number. Bi (T) = h(T) * L / k(T) Where h(T) = film coefficient or convective heat transfer coefficient [W/m2*K]. LC = characteristic length, which is generally described as the volume of the body divided by the surface area of the body [m]. k(T) = thermal conductivity of the body [W/m*k] The concept of a local Biot number is introduced to quantify the local variations of part size, geometry and heat transfer coefficient. First, a large Bi indicates large temperature gradients within the part. Second, large local (geometry dependent) variations in Bi number will lead to large lateral temperature gradients. Therefore, variations in local Bi can lead to large temperature gradients and therefore high stress during quenching and finally distortion. This local Bi concept can be used in a systems approach to designing a part and the quenching system. This systems approach can be designated as design for heat treating.

<P> This thesis is concerned with the investigation of the diffusion controlled reaction between MgO and β-quartz in the temperature range 1200 - 1450 °C in wet and dry atmospheres. The reactions were studied by placing known faces of quartz crystals in direct contact with Mg0 powder, heat treating them, and then investigating the cross sections. The product layer was investigated by both reflected light and thin section metallography, electron - microprobe and X- ray diffraction. Using Wagner's and Schmalzried's ideas on solid state reactions, a theoretical model for the diffusion controlled formation of silicates was developed. With this model, a mechanism for the diffusion controlled formation of forsterite from MgO and β-quartz was advanced. </P> / Thesis / Master of Science (MSc)

<p> In North America, heat treating adds about $15 billion per year in value to metal goods by imparting specific properties that are required if parts are to function successfully. Heat treating is an energy-intensive industry, requiring about 500 trillion BTUs (~ 0.5 trillion ft3 of natural gas) per year, which accounts for about 20% of the total cost ofthe business. Considering this huge demand on energy resources and its significant impact on the environment, in the year 1996, members of the heat treating industry represented by the ASM Heat Treating Society and the Metal Treating Institute (MTI) met and discussed the future of the heat treating industry in North America. A vision was developed known as "Heat Treating Industry Vision-2020". In that vision, the industry identified key research areas among which was the development of integrated process models. The industry recognized that most current heat-treating procedures are based on the experience of the heat treater. Trial-and-error often results in operations or components that are functional but not optimized. </p> <p> The present study is concerned with the development of process models of gas nitriding operations using Artificial Neural Networks (ANNs). Data required for the development of ANN s have been acquired from experiments carried out at the industrial partner site, V AC AERO International, Oakville, Ontario. Two types of ANNs have been developed and tested using the experimental data. The two models were able to predict various case depths produced by the nitriding process with reasonable accuracy in the ± 20% range. Predictions of the white layer thickness were in the ± 40% range. The sensitivity of predictions due to measurement errors has been investigated. The range of measurement error of the current study did not have a significant effect on the ANNs predictions. The effect of rate of cooling after the nitriding operation on the developed case depths has also been investigated. Cooling rates in the range of3° F/min to about 20 °F/min were tested. Results indicated that this range of cooling rates do not have a significant effect on the developed case depths. </p> <p> The present study has confirmed that ANNs models have the ability to be trained and applied to multivariable systems which renders ANNs the most suitable tool to develop integrated models for heat treating processes. </p> / Thesis / Master of Applied Science (MASc)

A simulação no tratamento térmico tem-se tornado de vital importância, principalmente na fase de projeto de produto e planejamento e controle produção, reduzindo significativamente o tempo e o custo antes dedicados a estas tarefas. Esta tecnologia quando combinada à medição das curvas de resfriamento, torna-se uma poderosa e confiável ferramenta para a predição das propriedades mecânicas e metalúrgicas em peças tratadas termicamente. A modelagem do processo de têmpera traz como resultados, a exeqüibilidade do processo, a constituição microestrutural final e a distribuição das distorções e tensões residuais da peça. O presente trabalho visa simular a transferência de calor, através do cálculo dos coeficientes de transferência de calor, e das tensões residuais térmicas e distorções em corpos de prova de aço AISI 5160 e de uma sonda de Inconel 600, com a análise posterior dos parâmetros obtidos. / The simulation of heat treating is becoming of vital importance, specially during design of product and production planning and control, reducing significantly costs and time that used to be wasted on these tasks. This technology when combined to measured cooling curves, become a powerful and trustful tool for predicting mechanical and metallurgical properties of heat treated components. Modeling the quenching process shows the feasibility of the process, the final microstructure and the distribution of residual stresses and distortions on workpiece. The present work aims at simulate the heat transfer, the thermal residual stresses and distortions in a workpiece of AISI 5160 steel and of a probe of Inconel 600, with posterior analysis of the obtained parameters.

"The effects of heat treating process parameters on the microstructure, residual stress, and distortion of a vacuum carburized, quenched and cold treated ring gear made of Pyrowear 53 has been determined using Abaqus and DANTE software. The data from these finite element method simulations was compared to measured values from physical testing. It was found that the heat treating process of the ring gear could be simulated and provide similar results to the measured and specified values for hardness, carbon content, and distortion. The simulations and distortion in this paper provide a detailed view of the mass transfer, heat transfer, and stress that occur during heat treating. These simulations suggest nonuniform cooling of a ring gear leads to greater distortion than uniform cooling. Simulations compared the retained austenite and hardness in ring gears that were oil quenched and high pressure gas quenched."

A simulação no tratamento térmico tem-se tornado de vital importância, principalmente na fase de projeto de produto e planejamento e controle produção, reduzindo significativamente o tempo e o custo antes dedicados a estas tarefas. Esta tecnologia quando combinada à medição das curvas de resfriamento, torna-se uma poderosa e confiável ferramenta para a predição das propriedades mecânicas e metalúrgicas em peças tratadas termicamente. A modelagem do processo de têmpera traz como resultados, a exeqüibilidade do processo, a constituição microestrutural final e a distribuição das distorções e tensões residuais da peça. O presente trabalho visa simular a transferência de calor, através do cálculo dos coeficientes de transferência de calor, e das tensões residuais térmicas e distorções em corpos de prova de aço AISI 5160 e de uma sonda de Inconel 600, com a análise posterior dos parâmetros obtidos. / The simulation of heat treating is becoming of vital importance, specially during design of product and production planning and control, reducing significantly costs and time that used to be wasted on these tasks. This technology when combined to measured cooling curves, become a powerful and trustful tool for predicting mechanical and metallurgical properties of heat treated components. Modeling the quenching process shows the feasibility of the process, the final microstructure and the distribution of residual stresses and distortions on workpiece. The present work aims at simulate the heat transfer, the thermal residual stresses and distortions in a workpiece of AISI 5160 steel and of a probe of Inconel 600, with posterior analysis of the obtained parameters.

Este trabalho teve por objetivo estudar o efeito dos parâmetros de corte e dos tratamentos térmicos na usinagem de três aços inoxidáveis austeníticos (ABNT 303, 304 e 310). Estes aços apresentam mesma estrutura cristalina e microestrutura semelhante. O aço ABNT 303 tem composição próxima ao ABNT 304, exceto pelo elevado teor de enxofre. Já o aço ABNT 310 apresenta maiores teores de elementos de ligas. Esses materiais foram tratados termicamente (solubilização ou envelhecimento). Os aços estudados foram caracterizados microestruturalmente e foram realizadas medidas de dureza Vickers. Os aços foram então torneados em várias condições de usinagem, variando principalmente a relação avanço por profundidade de corte. Foram medidas as forças de corte e de avanço em algumas das condições e coletados os cavacos resultantes para análise morfológica, que foram realizadas utilizando-se principalmente microscopia óptica e eletrônica de varredura. Foram também medidas as rugosidades e determinados os perfis das superfícies usinadas para a avaliação do acabamento superficial. Os resultados obtidos neste trabalho permitiram determinar algumas diferenças no comportamento dos três aços inoxidáveis estudados. As maiores diferenças foram verificadas quando as superfícies foram observadas utilizando microscopia. O aço ABNT 303 apresentou as piores superfícies e os menores esforços de corte em relação aos aços ABNT 304 e 310. A utilização de diferentes ferramentas neste trabalho mostrou influência principalmente na formação do cavaco, não tendo muita influencia nos esforços de corte e tão pouco no acabamento superficial. Os tratamentos térmicos realizados propiciaram a formação de outras fases, as quais causaram alterações na microestrutura. No entanto, esses tratamentos térmicos não alteraram de forma significativa o processo de torneamento. Finalmente, a formação de martensitas induzidas por deformação foi identificada no cavaco, mas não pode ser quantificada. / The main objective of this work is to study and evaluate the effect of cutting parameters, the cutting tool and the heat treatments in the turning process of three different types of austenitic stainless steels (ABNT 303, 304 e 310). The steels studied are structurally and microstructurally comparable. The chemical composition of the ABNT 303 and the ABNT 304 is similar except for the presence of sulfur in the ABNT 303 steel which alloeds the manganese sulfide formation. On the other hand, the ABNT 310 steel is richer in alloying elements and has lower tendency to strain induced martensite formation than the other steels studied. The steels studied were also heat treated in different conditions (annealed and aged). The materials were microstructurally characterized and Vickers hardness was also measured. The turning tests were carried out by using different cutting parameters, mainly the feedcutting depth relations. These relations lead to a plane state of tension or a plane state of deformation. The cutting and feed forces were measured during turning tests. During the tests the chips were also collected for morphological analysis through optical and scanning electron microscopies. The roughness and the surfaces characteristics were also determined to evaluate the surface finishing. The major difference in the steels turned was related to surface finishing observed by using optical and scanning electron microscopies. On the whole, the ABNT 303 steel presented the worst surface and the lowest cutting forces. However, the differences among all results were not significant. The tests carried out also showed there was not considerable difference between the tools used except for the chip morphology. The heat treatments led to precipitation in the steels studied and changes in their microstructure. However, the microstructural changes hardly affected the results of the turning tests. Finally, the martensite formation was detected although this phase could be not quantified.

Este trabalho teve por objetivo estudar o efeito dos parâmetros de corte e dos tratamentos térmicos na usinagem de três aços inoxidáveis austeníticos (ABNT 303, 304 e 310). Estes aços apresentam mesma estrutura cristalina e microestrutura semelhante. O aço ABNT 303 tem composição próxima ao ABNT 304, exceto pelo elevado teor de enxofre. Já o aço ABNT 310 apresenta maiores teores de elementos de ligas. Esses materiais foram tratados termicamente (solubilização ou envelhecimento). Os aços estudados foram caracterizados microestruturalmente e foram realizadas medidas de dureza Vickers. Os aços foram então torneados em várias condições de usinagem, variando principalmente a relação avanço por profundidade de corte. Foram medidas as forças de corte e de avanço em algumas das condições e coletados os cavacos resultantes para análise morfológica, que foram realizadas utilizando-se principalmente microscopia óptica e eletrônica de varredura. Foram também medidas as rugosidades e determinados os perfis das superfícies usinadas para a avaliação do acabamento superficial. Os resultados obtidos neste trabalho permitiram determinar algumas diferenças no comportamento dos três aços inoxidáveis estudados. As maiores diferenças foram verificadas quando as superfícies foram observadas utilizando microscopia. O aço ABNT 303 apresentou as piores superfícies e os menores esforços de corte em relação aos aços ABNT 304 e 310. A utilização de diferentes ferramentas neste trabalho mostrou influência principalmente na formação do cavaco, não tendo muita influencia nos esforços de corte e tão pouco no acabamento superficial. Os tratamentos térmicos realizados propiciaram a formação de outras fases, as quais causaram alterações na microestrutura. No entanto, esses tratamentos térmicos não alteraram de forma significativa o processo de torneamento. Finalmente, a formação de martensitas induzidas por deformação foi identificada no cavaco, mas não pode ser quantificada. / The main objective of this work is to study and evaluate the effect of cutting parameters, the cutting tool and the heat treatments in the turning process of three different types of austenitic stainless steels (ABNT 303, 304 e 310). The steels studied are structurally and microstructurally comparable. The chemical composition of the ABNT 303 and the ABNT 304 is similar except for the presence of sulfur in the ABNT 303 steel which alloeds the manganese sulfide formation. On the other hand, the ABNT 310 steel is richer in alloying elements and has lower tendency to strain induced martensite formation than the other steels studied. The steels studied were also heat treated in different conditions (annealed and aged). The materials were microstructurally characterized and Vickers hardness was also measured. The turning tests were carried out by using different cutting parameters, mainly the feedcutting depth relations. These relations lead to a plane state of tension or a plane state of deformation. The cutting and feed forces were measured during turning tests. During the tests the chips were also collected for morphological analysis through optical and scanning electron microscopies. The roughness and the surfaces characteristics were also determined to evaluate the surface finishing. The major difference in the steels turned was related to surface finishing observed by using optical and scanning electron microscopies. On the whole, the ABNT 303 steel presented the worst surface and the lowest cutting forces. However, the differences among all results were not significant. The tests carried out also showed there was not considerable difference between the tools used except for the chip morphology. The heat treatments led to precipitation in the steels studied and changes in their microstructure. However, the microstructural changes hardly affected the results of the turning tests. Finally, the martensite formation was detected although this phase could be not quantified.