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  • About
  • The Global ETD Search service is a free service for researchers to find electronic theses and dissertations. This service is provided by the Networked Digital Library of Theses and Dissertations.
    Our metadata is collected from universities around the world. If you manage a university/consortium/country archive and want to be added, details can be found on the NDLTD website.
1

Efeito da adi??o de feldspato e/ou res?duo de caulin em formula??es ? base de argila il?tica

Castro, Raimundo Jos? de Sousa 16 November 2010 (has links)
Made available in DSpace on 2014-12-17T14:07:06Z (GMT). No. of bitstreams: 1 RaimundoJSC_TESE.pdf: 1754370 bytes, checksum: 88d2811dd20d4c281cc4bc5a58cfc6fa (MD5) Previous issue date: 2010-11-16 / The red pottery industry in Piau? state is well developed and stands out at the national context for the technical quality of its products. The floor and wall tile industry, however, is little developed since the state has only one company that produces red clay-based ceramic tiles. This thesis aims at using the predominantly illitic basic mass of the above mentioned industry, with the addition of feldspar and/or kaolin residue in order to obtain products of higher technical quality. Kaolin residue consists basically of kaolinite, muscovite mica and quartz; the feldspar used was potassic. In this experiment, basic mass (MB) was used for experimental control and fifteen formulations codified as follows: F2, F4, F8, F16, F32, FR2, FR4, FR8, FR16, FR32, R2, R4, R8, R16 and R32. All raw materials were dry-milled, classified, formulated and then humidified to 10% water. Thereafter, test samples were produced by unixial pressing process in a rectangular steel matrix (60.0 x 20.0 x 5.0) mm3 at (25 MPa). They were fired at four temperatures: 1080?C, 1120?C, 1160?C, with a heating rate of 10?C/min during up to 10 min in an electric oven, and the last one in an industrial oven with a peak of 1140?C, aim ing to confirm the results found in laboratory and, finally, technological tests were performed: MEA, RL, AA, PA, TRF and PF. The results revealed that the residue under study can be considered a raw material with large potential in the industry of red clay-based ceramic tiles, since the results found both in laboratory and in the industry have shown that the test samples produced from the formulations with up to 4% feldspar and those produced with up to 8% feldspar and residue permitted a reduction in the water absorption rate and an increase in the mechanical resistance while those samples produced with up to 4% residue had an increase in the mechanical resistance when compared to those produced from the basic mass and that the formulation with 2% feldspar and residue presented the best technological properties, lowering the sintering temperature down to 1120?C / A ind?stria de cer?mica vermelha do Piau? ? bem desenvolvida e se destaca no contexto nacional pela qualidade t?cnica de seus produtos. J? a ind?stria de revestimento pouco se desenvolveu, visto que o estado possui uma ?nica empresa que produz revestimento de base argilosa vermelha. Esta tese tem por objetivo utilizar a massa b?sica predominantemente il?tica da ind?stria citada, adicionando ? mesma feldspato e/ou res?duo de caulim com o prop?sito de obter produtos de melhores qualidades t?cnicas. O res?duo caulim ? constitu?do basicamente de caulinita, mica moscovita e quartzo; o feldspato utilizado foi o pot?ssico. Para este experimento, utilizou-se a massa b?sica (MB) para controle experimental e quinze formula??es assim codificadas: F2, F4, F8, F16, F32, FR2, FR4, FR8, FR16, FR32, R2, R4, R8, R16 e R32. Todas as mat?rias-primas foram mo?das a seco, caracterizadas, formuladas, depois umidificadas a 10% com ?gua. Em seguida, foram confeccionados corpos-de-prova por prensagem uniaxial em matriz retangular de a?o (60,0 x 20,0 x 5,0) mm? a (24 MPa), os quais foram queimados em quatro temperaturas: 1080?C, 1120?C, 1160?C, com taxa de aqu ecimento de 10?C/min e patamar de 10 min em forno el?trico, e a ?ltima em forno a rolo industrial e pico de 1140?C com o objetivo de validar os resultados encontra dos em laborat?rio; por ?ltimo, foram realizados ensaios tecnol?gicos: MEA, RL, AA, PA, TRF e PF. Os mesmos mostraram que o res?duo estudado pode ser considerado como mat?riaprima de grande potencial para a ind?stria de pisos e revestimentos cer?micos de base argilosa vermelha, j? que tanto os resultados encontrados em laborat?rio como na ind?stria mostram que os corpos-de-prova produzidos a partir das formula??es com feldspato at? 4% e os produzidos com feldspato e res?duo at? 8% permitiram uma redu??o da absor??o de ?gua e aumento da resist?ncia mec?nica, sendo que os corpos-de-prova produzidos com at? 4% de res?duo tiveram aumento da resist?ncia mec?nica, quando comparados aos corpos-de-prova produzidos a partir da massa b?sica e que a formula??o com 2% de feldspato e res?duo apresentou melhores propriedades tecnol?gicas, reduzindo a temperatura de sinteriza??o para 1120?C

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