The growing effect of combustion pollutant emission on the environment and increasing petroleum prices are driving development of design methodologies for clean and efficient industrial combustion technologies. The design optimization methodology employs numerical algorithms to find the optimal solution of a design problem by converting it into a multivariate minimization problem. This is done by defining a vector of design parameters that specifies the design configuration, and an objective function that quantifies the performance of the design, usually so the optimal design outcome minimizes the objective function. A numerical algorithm is then employed to find the design parameters that minimize the objective function; these parameters thus specify the optimal design. However this technique is used in several other fields of research, its application to industrial combustion is fairly new. In the present study, a statistical optimization method called response surface methodology is connected to a CFD solver to find the highest combustion efficiency by changing the inlet air swirl number and burner quarl angle in a furnace. OpenFOAM is used to model the steady-state combustion of natural gas in the 300 KW BERL combustor. The main barrier to applying optimization in the design of industrial combustion equipment is the substantial computational effort needed to carry out the CFD simulation every time the objective function needs to be evaluated. This is intensified by the stiffness of the coupled governing partial differential equations, which can cause instability and divergent simulations. The present study addresses both of these issues by initializing the flow field for each objective function evaluation with the numerical results of the previously converged point. This modification dramatically reduced computation time. The combustion of diesel spray in the GenTex 50M process heater is investigated in the next part of this thesis. Experimental and numerical studies were carried out for both the cold spray and the diesel combustion where the numerical results satisfactorily predicted the observations. The simulation results show that, when carrying out a parametric design of a liquid fuel-fired combustor it is necessary to consider the effect of design parameters on the spray aerodynamic characteristics and size distribution, the air/spray interactions, and the size of the recirculation zones.

The growing effect of combustion pollutant emission on the environment and increasing petroleum prices are driving development of design methodologies for clean and efficient industrial combustion technologies. The design optimization methodology employs numerical algorithms to find the optimal solution of a design problem by converting it into a multivariate minimization problem. This is done by defining a vector of design parameters that specifies the design configuration, and an objective function that quantifies the performance of the design, usually so the optimal design outcome minimizes the objective function. A numerical algorithm is then employed to find the design parameters that minimize the objective function; these parameters thus specify the optimal design. However this technique is used in several other fields of research, its application to industrial combustion is fairly new. In the present study, a statistical optimization method called response surface methodology is connected to a CFD solver to find the highest combustion efficiency by changing the inlet air swirl number and burner quarl angle in a furnace. OpenFOAM is used to model the steady-state combustion of natural gas in the 300 KW BERL combustor. The main barrier to applying optimization in the design of industrial combustion equipment is the substantial computational effort needed to carry out the CFD simulation every time the objective function needs to be evaluated. This is intensified by the stiffness of the coupled governing partial differential equations, which can cause instability and divergent simulations. The present study addresses both of these issues by initializing the flow field for each objective function evaluation with the numerical results of the previously converged point. This modification dramatically reduced computation time. The combustion of diesel spray in the GenTex 50M process heater is investigated in the next part of this thesis. Experimental and numerical studies were carried out for both the cold spray and the diesel combustion where the numerical results satisfactorily predicted the observations. The simulation results show that, when carrying out a parametric design of a liquid fuel-fired combustor it is necessary to consider the effect of design parameters on the spray aerodynamic characteristics and size distribution, the air/spray interactions, and the size of the recirculation zones.

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The need for low order models capable of performing damage identification has become apparent in many structural dynamics applications where structural health monitoring and damage prognosis programs are implemented. These programs require that damage identification routines have low computational requirements and be reliable with some quantifiable degree of accuracy. Response surface metamodels (RSMs) are proposed to fill this need. Popular in the fields of chemical and industrial engineering, RSMs have only recently been applied in the field of structural dynamics and to date there have been no studies which fully demonstrate the potential of these methods. In this thesis, several RSMs are developed in order to demonstrate the potential of the methodology. They are shown to be robust to noise (experimental variability) and have success in solving the damage identification problem, both locating and quantifying damage with some degree of accuracy, for both linear and nonlinear systems. A very important characteristic of the RSMs developed in this thesis is that they require very little information about the system in order to generate relationships between damage indicators and measureable system responses for both linear and nonlinear structures. As such, the potential of these methods for damage identification has been demonstrated and it is recommended that these methods be developed further. / Master of Science

Yes / The deodorization of the refined palm oil process is simulated here using ASPEN HYSYS. In the absence of a library molecular distillation (MD) process in ASPEN HYSYS, first, a single flash vessel is considered to represent a falling film MD process which is simulated for a binary system taken from the literature and the model predictions are compared with the published work based on ASPEN PLUS and DISMOL. Second, the developed MD process is extended to simulate the deodorization process. Parameter estimation technique is used to estimate the Antoine’s parameters based on literature data to calculate the pure component vapor pressure. The model predictions are then validated against the patented results of refining edible oil rich in natural carotenes and vitamin E and simulation results were found to be in good agreement, within a 2% error of the patented results. Third, Response Surface Methodology (RSM) is employed to develop non-linear second-order polynomial equations based model for the deodorization process and the effects of various operating parameters on the performance of the process are studied. Finally, an optimization framework is developed to maximize the concentration of beta-carotene, tocopherol and free fatty acid while optimizing the feed flow rate, temperature and pressure subject to process constrains. The optimum results of feed flow rate, temperature, and pressure were determined as 1291 kg/h, 147 C and 0.0007 kPa respectively, and the concentration responses of beta- carotene, tocopherol and free fatty acid were found to be 0.000575, 0.000937 and 0.999840 respectively. / Prince of Songkla University, Songkhla, Thailand for providing financial support (Grant code: PSU2554-022)

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In robust parameter design it is often possible to set the levels of the controllable factors to produce a zero gradient for the transmission of variability from the noise variables. If the number of control variables is greater than the number of noise variables, a continuum of zero-gradient solutions exists. This situation is useful as it provides the experimenter with multiple conditions under which to configure a zero gradient for noise variable transmission. However, this situation requires a confidence region for the multiple-solution factor levels that provides proper simultaneous coverage. This requirement has not been previously recognized in the literature. In the case where the number of control variables is greater than the number of noise variables, we show how to construct critical values needed to maintain the simultaneous coverage rate. Two examples are provided as a demonstration of the practical need to adjust the critical values for simultaneous coverage. The zero-gradient confidence region only focuses on the variance, and there are in fact many such situations in which focus is or could be placed entirely on the process variance. In the situation where both mean and variance need to be considered, a general confidence region in control variables is developed by minimizing weighted mean square error. This general method is applicable to many situations including mixture experiments which have an inherit constraint on the control factors. It also gives the user the flexibility to put different weights on the mean and variance parts for simultaneous optimization. It turns out that the same computational algorithm can be used to compute the dual confidence region in both control factors and the response variable. / Statistics

Yes / Reverse Osmosis (RO) process can be considered as one of the intensively used pioneering equipment for reusing wastewater of several applications. The recent study presented the development of an accurate model for predicting the dimethylphenol removal from wastewater via RO process. The Response Surface Methodology (RSM) was applied to carry out this challenge based on actual experimental data collected from the literature. The independent variables considered are the inlet pressure (5.83-13.58) atm, inlet temperature (29.5-32) ° C, inlet feed flow rate (2.166-2.583) × 10-4 m3/s, and inlet concentration (0.854-8.049) × 10-3 kmol/m3 and the dimethylphenol removal is considered as the response variable. The analysis of variance showed that the inlet temperature and feed flow rate have a negative influence on dimethylphenol removal from wastewater while the inlet pressure and concentration show a positive influence. In this regard, F-value of 240.38 indicates a considerable contribution of the predicted variables of pressure and concentration against the process dimethylphenol rejection. Also, the predicted R2 value of 0.9772 shows the high accuracy of the model. An overall assessment of simulating the performance of RO process against the operating parameters has been systematically demonstrated using the proposed RSM model.

Many industrial statisticians employ the techniques of Response Surface Methodology (RSM) to study and optimize products and processes. A second-order Taylor series approximation is commonly utilized to model the data; however, parametric models are not always adequate. In these situations, any degree of model misspecification may result in serious bias of the estimated response. Nonparametric methods have been suggested as an alternative as they can capture structure in the data that a misspecified parametric model cannot. Yet nonparametric fits may be highly variable especially in small sample settings which are common in RSM. Therefore, semiparametric regression techniques are proposed for use in the RSM setting. These methods will be applied to an elementary RSM problem as well as the robust parameter design problem. / Ph. D.