As advances in solid rocket technology push rocket motors to more extreme operating speeds and temperatures, it becomes increasingly important to have well-designed material systems capable of surviving these harsh conditions. One common component in these systems is the use of a fiber- and particle-reinforced EPDM insulation layer between the motor casing and the solid fuel to shield the casing from the temperatures of the burning fuel and from the high velocity of gas particles traveling within the motor. This work studies several insulation materials to determine which exhibits the highest shear strength after being charred. Double-notch shear test specimens of three materials, ARI-2718, ARI-2719, and ARI-2750, were charred and tested to measure the failure strength of each charred material. The ARI-2750 showed the highest shear strength when loaded along the material orientation, but the ARI-2719 was strongest when transversely loaded. The strength measurements for ARI-2750 were highly sensitive to loading direction, unlike ARI-2718 and ARI-2719. Extensive scanning electron microscopy to identify correlations between shear strength and microstructure revealed that the amount of fiber orientation and amount of residual matrix material may have significant impacts on charred shear strength in these materials. / Master of Science

A small shear sensor utilizing an array of carbon nanotubes to support a sensor head was developed for use in steady, high speed, 2D flow. The sensor is a non-intrusive, direct measurement device with a 2 x 2 mm square sensor head surrounded by a small gap on each side (~0.004 inches). The translation of the sensing element is due to the nanotubes bending when a shear force is applied to the sensor head. Displacements are measured by an interferometric technique using fiber-optics to measure the distance the sensor head travels by viewing a polished side of the head. The fiber-optical displacement sensor is bonded to a stationary substrate so that all measurements are relative to a fixed position. Arrays of carbon nanotubes were grown on bare 2 x 2 mm square silicon chips. The nanotubes were grown to heights of 75 microns with a thin layer of amorphous carbon on top. The silicon chips were then flipped, and the amorphous layer of carbon was bonded to bare 1 x 1 cm silicon substrates, making the bottom of 2 x 2 mm silicon chip the sensor head. The sensors were calibrated at Luna Innovations using a point-load technique. Four of the six sensors could not be successfully calibrated because they were fatally damaged during the last step of the calibration process. Wind tunnel tests were conducted on the one sensor that survived the calibration. An arrangement was designed and built from aluminum to test the performance of the sensor in the Virginia Tech Supersonic Wind Tunnel. Seven test runs were conducted in this cold-flow facility at a nominal Mach number of 2.4 and stagnation pressures ranging from 50 - 90 psia. Two test runs gave skin friction values 3 - 20% lower than those values predicted by indirect measurement techniques before the sensor was damaged. While these first results are encouraging, further studies are clearly needed. Due to distinct anomalies in the displacement data during test run 3, it was concluded that the sensor was damaged during this run. Possible explanations of the failure of this sensor are offered along with suggestions for future work. / Master of Science

UHPC (ultra-high performance concrete) is a relatively new type of concrete that exhibits mechanical properties that are far superior to those of conventional concrete and in some cases rival those of steel. The main characteristics that distinguish UHPC from conventional reinforced concrete are the improved compressive strength, the tensile strength, the addition of steel fibers, and the resistance to corrosion and degradation. The mechanical properties of UHPC allow for smaller, thinner, lighter sections to be designed while strength is maintained or improved. The use of UHPC has been limited to a few structural applications due to the high cost of the materials and the lack of established design guidelines. A proposed material model based on material and finite element models has served as the foundation of this research effort. The model was used to minimize the dimension of an optimum section in order to limit the material usage and maximize the performance. In the model, the top flange served as the riding surface and contained no reinforcing steel to resist shear. The lack of steel reinforcement allowed for the possibility of a punching shear failure to occur from the application of a point load such as a wheel tire patch load. The model and optimized section served as the foundation for this research, the characterization of punching shear capacity of thin UHPC plates. A total of 12 UHPC slabs were tested to failure to determine the boundary between a flexural failure and a punching shear failure. The variables considered were the slab thickness and loading plate dimensions. The results of the testing were compared to existing models for punching shears and other failure modes, with varying success. The test results aided in the development of a design equation for the prediction of punching shear in UHPC slabs. After evaluation of the test results, recommendations are made as to which model predicts the punching shear capacity of UHPC slabs and the minimum slab thickness required to prevent a punching shear failure. / Master of Science

The majority of residential construction and a significant portion of light commercial and industrial construction has been, and will continue to be light-framed timber construction. In recent years, innovations have surfaced to improve upon light-framed construction. Structurally insulated panels (SIPS) are gaining popularity due to their superior energy efficiency and ease of construction. Light-framed timber construction has proven to be trustworthy in high-wind and seismic regions due to its lightweight construction and numerous redundancies. Shear walls, along with floor and roof diaphragms, resist lateral loads in a timber structure. In the past, research has focused on the static racking performance of light-framed shear walls. More recently, research has been focused on the cyclic and dynamic performance of shear walls. To the author's knowledge, no other research is reported in the literature on the cyclic performance of SIPS shear walls. It is important to understand and quantify the monotonic and cyclic response of shear walls. In this study, twenty-three full-scale shear walls were tested under monotonic loading and sequential phased displacement cyclic loading. Four different wall configurations were examined. Monotonic and cyclic performance of the shear walls and monotonic and cyclic testing procedures are compared. Response of SIPS shear walls is also compared to the response of light-framed shear walls based on capacity, stiffness, ductility, energy dissipation, damping characteristics, and overall behavior. Results of this study will provide useful information regarding the performance of SIPS shear walls and similar systems subjected to static, cyclic, and dynamic lateral loads. / Master of Science

The Blue Plains Wastewater Treatment Plant in Washington, D.C. is in the process of updating its anaerobic digesters, with a completion date set for 2008. This research was undertaken to aid designers at Blue Plains by evaluating alternative digestion approaches. The technologies applicable to the plant included thermophilic anaerobic digestion, acid/gas phased digestion, and temperature phased anaerobic digestion. To obtain design data, a year long study was conducted using bench scale digestion systems operating at different solids retention times (SRT) and organic loading rates (OLR). The digesters were fed with mixed primary and secondary waste (50/50 by weight) from the Blue Plains wastewater treatment facility. The digesters were operated until they reached steady state as observed by volatile solids reduction (VSR), methane production, and volatile fatty acid (VFA) levels. At this point, samples of digested waste sludge were analyzed for residual biological activity, dewatering properties and headspace organo-sulfur production. Results from the study demonstrated that the TPAD digestion process had the lowest residual biological activity (RBA) after digestion, and that the single stage thermophilic digesters had the highest RBA. Sludge from single stage mesophilic digestion had the highest odor potential, with headspace gas tests generating over 1400 mg organo-sulfur per m3 of headspace gas, while both single stage thermophilic and TPAD systems generated less than 400 mg/m3 at all SRTs studied. / Master of Science

An in vitro arterial flow bioreactor system for the generation of physiological flows in a biological environment was designed, constructed, and characterized. The design was based on models previously used to investigate the response of endothelial cells to shear. The model interfaces a bioreactor with flow elements to compose a flow loop that reproduces arterial flow conditions within the bioreactor. High-resolution (8.6 microns) time-resolved (4 ms) velocity field measurements within the bioreactor were obtained using Particle Image Velocimetry (PIV). Two physiological flows were considered, corresponding to medium human arteries at rest and exercise conditions: first, with an average Reynolds number of 150 and a Womersley parameter of 6.4, and second, with an average Reynolds number of 300 and a Womersley parameter of 9.0. Two cases were considered: first, using a smooth artery section, and second, with a confluent layer of human microvascular endothelial cells grown on the inner surface of the artery section. The instantaneous wall shear stress, time-averaged wall shear stress, and oscillatory shear index were computed from the velocity field measurements and compared for the cases with and without cells. These measurements were used to assess the value of the system for measurement of correlations between fluid dynamics and the response of biological tissue. It was determined that the flow present in such a system is not an accurate reproduction of physiological flow, and that direct measurement of the flow is necessary for accurate quantification of cellular response to fluid parameters. / Master of Science

The most common fastening technique that is used to connect the components of wooden pallets together are helically or annularly threaded pallet nails. Pallet nails create a strong durable connection and increase manufacturing efficiency for a low cost. However, nails can also cause iron staining, wood splitting, and when exposed can cause product damage or personnel injury. Using adhesives could be a solution to these problems, but only if the adhesives' strength and durability is comparable or higher than nails. The objective of the study was to investigate the tensile and shear strength of pallet connections secured using commercially available wood adhesives and compare their performance to pallet connections secured using common pallet nails. The lowest pre-compression pressure resulted in the best tension and shear performance for a solvent based construction adhesive (SBCA). The pre-compression pressure did not have any practical effect on the performance of the two-part emulsion polymer isocyanate (EPI) adhesive. Samples made with the solvent based construction adhesive (SBCA) had greater strength and energy at failure than nailed samples. Meanwhile, the samples made with the two-part emulsion polymer isocyanate (EPI) adhesive had equal or greater strength than nailed samples, except for during the tension parallel to the grain tests in which they had equal or lower strength. / MS / The most common technique used to connect the components of wooden pallets together is nails. Pallet nails create a strong connection with high manufacturing efficiency for a low cost. However, nails can cause iron staining, wood splitting, and when exposed can cause product damage or personnel injury. Using adhesives could be a solution to these problems, but only if the adhesives’ strength and durability is comparable or higher than nails. The objective of this study was to investigate the tensile and shear strength of pallet connections when secured using commercially available wood adhesives and compare its performance to pallet connections secured by using common pallet nails. The lowest pre-compression pressure tested resulted in the best overall performance for a solvent based construction adhesive (SBCA); meanwhile, pre-compression pressure did not have any practical effect on the performance of the two-part emulsion polymer isocyanate (EPI) adhesive tested. Therefore, using a lower pre-compression pressure would provide adequate performance and could also improve the ease of manufacturing and potentially reduce overall costs. Based on the tests conducted it was found that the solvent based construction adhesive (SBCA) demonstrated the best performance of all connection methods and could be a potential replacement for nails. More tests, such as weathering and impact, should be conducted to determine the full limitations of the adhesive in use.

The purpose of this study is to further evaluate the performance of the 5/16 in. diameter Elco Grade 8 standoff screw as a mechanical shear connector in composite joists. Standoff screws are being investigated as viable an alternative to welded shear studs in short span composite joists. The data and results obtained from 59 pushout tests performed on the 5/16 in. diameter Elco Grade 8 standoff screw are presented. The test parameters investigated in this study include: standoff screw height, quantity of standoff screws per deck rib, standoff screw position, slab depth, base angle thickness, deck type, and amount of transverse reinforcement. Test results gathered in this study are used in conjunction with selected test data from research performed by Alander (1998). This combined test data is used in determining the validity of existing predictive equations for the shear strength of the 5/16 in. diameter Elco Grade 8 standoff screw. The influence of various independent variables on shear strength is investigated for all screw densities tested. The performance of the 5/16 in. diameter Elco Grade 8 standoff screw in solid slab applications is also investigated. Proposed predictive equations for the shear strength of the 5/16 in. diameter Elco Grade 8 standoff screw based on screw-related failure modes, concrete cone failures and longitudinal splitting, are presented. / Master of Science

The White Mountain shear zone (WMSZ) is a zone of intense penetrative deformation that lies along the western front of the northern White-Inyo Range in eastern-most California and western-most Nevada. The northern half of the WMSZ is characterized by a NNE to NNW-striking steeply dipping foliation and associated shallowly plunging NNE to NW-trending stretching lineations. S-C fabrics observed in outcrop, microstructural shear sense indicators and kilometer-scale foliation geometry all indicate dextral movement. Localized discrete zones of coeval steeply plunging stretching lineations are present in the northern half of the WMSZ. Microstructural data from these domains indicate a high component of pure shear within a separate coeval kinematic framework and hence a transpressional history. The WMSZ appears to be tectonically related to both the Sierra Crest shear system to the west and the Santa Rita shear system to the south. Correlation between the WMSZ and the Santa Rita shear system indicates that Late Cretaceous dextral transpression may extend up to ~120 km along the western front of the White-Inyo Range. Cross-cutting relationships with Late Cretaceous plutons bracket the age of the WMSZ at between 72-92 Ma. A lack of annealing recrystallization in deformed quartz and the presence of high temperature crystallographic fabrics near the margins of the ca. 72 Ma Boundary Peak pluton indicate significant strain accumulation within the WMSZ subsequent to emplacement of the Boundary Peak pluton. These observations extend the duration of Late Cretaceous dextral transpression in eastern California to at least as recent as 72 Ma. / Master of Science

Tapered beams and columns are often used in single story gable framed steel buildings for reasons of economy. By varying the resistance to bending in similar proportion to the bending moments, more economical structures can be obtained. The beam and column connection, or knee area, is generally subject to the greatest bending moments. It is therefore comprised of the deepest sections of the tapered members, which also possess the least resistance to shear buckling. The web element's stress distribution in this region of relatively complicated geometry is unknown. For this reason, web stiffening plates are commonly used to brace the slender web elements against elastic shear buckling. The design and proper installation of these relatively small elements, while proven to be effective, is also costly. Because it is desirable to remove the stiffeners, the shear behavior of unstiffened tapered members near the moment connection was the primary focus of this study. Four knee area specimens were tested to failure under simulated gravity load conditions. The specimens were analyzed according to the AISC shear provisions for prismatic members. The appropriateness of a modified shear force, which accounts for the influence of inclined flanges, and the role of initial web imperfections were examined as well. Finally an analysis method which most consistently produces conservative results is proposed. / Master of Science