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Thesis: Sc. D., Massachusetts Institute of Technology, Department of Materials Science and Engineering, 1978 / Vita. / Includes bibliographical references. / Sc. D. / Sc. D. Massachusetts Institute of Technology, Department of Materials Science and Engineering

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Thesis (PhD)--University of Stellenbosch, 2004. / ENGLISH ABSTRACT: Analog-to-digital converters (ADCs) are an integral part of the interface between the analog and digital realms. This dissertation presents the design and simulation of a Complementary Output Switching-Logic (COSL) compatible, voltage state, switching logic comparator and a flash ADC for high speed applications with multi-GHz input bandwidth. Josephson technology and the COSL family of gates were utilized for this purpose. A detailed design for the switching logic comparator is first provided. The design is verified with simulations to obtain a functional comparator. The comparator is then optimized utilizing an optimization tool developed using the scripting facilities of WRSpice. Incorporated in this tool is a Monte Carlo capability to randomly vary the component values according to Gaussian distributions, and trimming facilities to be able to trim a non-functional comparator to restore functionality. The design component values are then optimized by maximizing the yield of a comparator. The optimized comparator is incorporated into the construction of a4-bit quantizer of an ADC. The output from the quantizer section yields a switching-logic Gray-code output. A Gray-to- Binary converter is designed with COSL gates to convert the Gray output from the quantizer into Binary code for further processing. The functionality, linearity, maximum input bandwidth and dynamic range of the 4-bit ADC is verified by simulation. A number of special input waveforms are used for this purpose. The performance of the comparator and the 4-bit ADC is also evaluated with thermal noise incorporated into simulation. Beat frequency simulations and Fourier spectra were also used in the evaluation of the ADC performance. A fully functional 4-bit ADC, with a maximum input bandwidth of 10 GHz for a clock speed of 20 GHz was achieved through simulations. Beat frequency simulations revealed that the comparators have an input bandwidth greater than 19 GHz with sufficient dynamic range for an ADC of greater than 6 bits of resolution. Due to the fact that the aperture time for the ADC is dependant on the rise time of the sampling pulse and not the width of the pulse, a much smaller aperture time is obtained which directly translates to higher input bandwidth. Finally, a layout of a 4-bit sampler circuit was done according to the Hypres manufacturing process to enable the high-speed testing of the comparator circuits. / AFRIKAANSE OPSOMMING: Analoog-na-Digitale Omsetters (ADOs) vorm 'n integrale deel van die koppelvlak tussen die analoog en digitale wêrelde. Hiedie proefskrif stel die ontwerp en simulasie van 'n Komplementêre Uittree Geskakelde Logika (COSL) aanpasbare, spanningstoestand, geskakelde logika vergelyker en ADO bekend. Hierdie ADO kan vir hoë spoed toepassings waar multi-GHz intree-bandwydte benodig word, aangewend word. Josephson tegnologie en die Komplementêre Uittree Geskakelde Logika (COSL) familie van hekke word vir hierdie doel gebruik. Die volledige ontwerp vir die geskakelde logika vergelyker word eerstens gegee. Die ontwerp word met behulp van simulasies bevestig om sodoende 'n ten volle funksionele vergelyker te verkry. Die vergelyker word verder geëptimeer deur middel van 'n proses wat met behulp van programmering in WRSpice ontwikkel is. Hierdie optimeringsproses sluit 'n Monte Carlo proses in wat die komponentwaardes van die vergelyker onwillekeurig volgens 'n Gaussiese verspreiding verander, sowel as 'n verstellingsmeganisme waarmee 'n nie-funksionerende vergelyker verstel kan word totdat dit weer ten volle funksioneer. Die komponentwaardes word dan geëptimeer vir maksimale opbrengs van 'n vergelyker. Die geëptimeerde vergelyker word gebruik in die konstruksie van 'n 4-bis kwantifiseerder vir 'n ADO. Die uittree van die 4-bis kwantifiseerder is in Gray kode. 'n Gray-na-Binêre kode omsetter word vir hierdie doelontwerp deur van COSL hekke gebruik te maak. Die volle ADO word voorts gesimuleer om die funksionalitet, lineariteit, maksimum intreebandwydte en dinamiese bereik te verifieer. 'n Verskeidenheid van intreeseine is vir hierdie doel gebruik. Die vergelyker en die 4-bis ADO is ook gesimuleer met termiese ruis om die effek daarvan te bepaal. Fourier spektra en ''verskilfrekwensie'' (Beat Frequency) simulasies word ook gebruik in die evaluering van die vergelyker en die ADO. Die korrekte werking van 'n 4-bis ADO met intreebandwydte van 10 GHz met 'n klokspoed van 20 GHz is deur simulasie bevestig. Verskilfrekwensie simulasies dui aan dat die vergelykers 'n intreebandwydte van groter as 19 GHz het, met voldoende dinamiese bereik vir 6 bis resolusie. Aangesien die vergelykers se venstertydperk bepaal word deur die stygende helling van die monsterpuls en nie deur die pulswydte nie, maak dit voorsiening vir 'n baie klein venstertydperk. 'n Klein venstertydperk is essensieel vir 'n hoë intreebandwydte. 'n Uitleg van 'n 4-bis vergelyker stadium is gedoen vir die Hypres vervaardigingsproses om die vergelyker teen hoë spoed te kan toets.

Transition metal fluorides represent an important family of complex solids displaying a variety of different properties and interesting phenomena. Despite their remarkable behaviour, these classes of materials have not received much attention and the rationalization of their behaviour is still lacking a systematic approach. This thesis aims to contribute to the field by examining previously unknown or understudied complex fluorides. The compounds were selected for their intriguing physical properties that range from superconductivity to multiferroism. The discovery of superconductivity in the iron pnictides sparked new interest in materials with layered ZrCuSiAs-type structure. Herein the properties of one of these systems, namely SrFeAsF, will be discussed. We have found that it behaves as a poor metal and undergoes a tetragonal (P4/nmm) to orthorhombic (Cmma) structural transition at T = 180 K, accompanied by a spin density wave in magnetic susceptibility and electrical resistivity. Below T < 150 K, the Fe moments order in antiferromagnetic spin-stripes. Electron doping with La3+ is a successful route to obtain superconducting phases, with maximum Tc = 27 K (x = 0.2). The isostructural AeMnPnF series (Ae = Sr, Ba; Pn = P, As, Sb) was also investigated to elucidate the influence of transition metal d-electrons and size effects of Ae and Pn on the physical properties. The isoelectronic replacement of Ae and Pn leads to a significant distortion in the tetragonal building blocks. All d5 Mn fluorides investigated here are insulating antiferromagnets with TN ~ 350 K. Due to the coexistence of electronic and magnetic ordering, the tetragonal tungsten bronze (TTB) materials KxM2+ xM3+ 1-xF3 (x = 0.4 – 0.6; M = transition metal) are potential multiferroics. The type of structural distortion adopted by these systems is strongly dependant on the M2+/M3+ ratio. For instance, our high-resolution diffraction study on K0.5Mn0.5Cr0.5F3 has revealed a small orthorhombic distortion, which indicates full chemical order of Mn2+ and Cr3+ on all crystallographic sites. K0.5Mn0.5Cr0.5F3 remains orthorhombic Ccc2 on cooling through the ferromagnetic transition at TN = 23 K. On heating, the structure is acentric up to T = 373 K, where a change to tetragonal P42/mbc symmetry marks the transition from ferroelectric (polar) to paraelectric (apolar) states. High-pressure diffraction experiments have shown that the Ccc2 structure is robust upon pressurization with anisotropic axial compressibility up to the maximum pressure applied p = 18 GPa. The crystal structure of related mixed-valence TTB fluoride K0.6Cr2+ 0.6Cr3+ 0.4F3 is influenced by the presence of Jahn-Teller active Cr2+. The structural analysis described here revealed the presence of a small polar monoclinic distortion (P112) providing a clear signature of full charge order (CO). On heating, the gradual loss of CO leads to two consecutive structural phase transitions to orthorhombic (Pba2, T = 423 K) and then tetragonal (P42/mbc, T = 823 K) lattices, the latter is the signature of the ferro- to paraelectric transition. Below T = 150 K, increased X-ray exposure time leads to CO-melting and the stabilization of a new, charge-disordered orthorhombic phase (Cmm2), with a phenomenology similar to the CO manganites. In highpressure diffraction experiments, a further transition to tetragonal P4bm symmetry is found at p = 6 GPa. The magnetic susceptibility points towards a complex spin arrangement, with two transitions at TN = 33 K and 6 K. The results presented herein show the richness of the structural, electronic and magnetic phase diagrams of transition metal fluorides and clearly demonstrate that systematic studies on these systems will greatly enhance our current understanding of the underlying mechanisms of important phenomena such as superconductivity and ferroelectricity.

Thesis (MScEng (Electrical and Electronic Engineering))--Stellenbosch University, 2008. / This thesis is aimed at testing commercially available CMOS amplifier ICs at 4 K. Super Conducting Electronics (SCE) will also be used to amplify RSFQ signals for easier detection by CMOS technology and better signal-to-noise ratios. The SCE comprises of a Suzuki stack amplifier, a 250 μA JTL and a DC-to-SFQ converter. The Suzuki stack amplifier is simulated in WRSPICE. It is able to amplify an SFQ signal synchronised with an external clock signal. The amplified signal can then be detected by a normal commercially available CMOS amplifier IC. To keep the noise in the signal to a minimum, the commercial amplifier must be be situated as close as possible to the SCE. The amplifier must therefore be able to operate at 4 K. Ten different amplifier ICs were tested and three was found that worked down to 4 K.

Thesis (MScEng (Electrical and Electronic Engineering))--University of Stellenbosch, 2007. / This thesis is concerned with the fabrication of high temperature bi-epitaxial grain boundary Josephson junctions for use in superconducting microelectronic circuits. It aims to provide a proof-of-concept manufacturing process which can serve as a basis for future research at the University of Stellenbosch. The work in this thesis integrates ...

Thesis (MScEng (Electrical and Electronic Engineering))--Stellenbosch University, 2008. / This thesis relates to the analysis and design of a SQUID microscope. Superconductor theory is discussed in depth to provide a thorough understanding of Josephson junctions and of dc SQUID magnetometers. The behaviour and suitability of different types of single-layer dc SQUIDs are looked at. The quality of the superconducting material patterned onto a substrate and the Josephson junction design used affect the behaviour of a practical dc SQUID. Noise and cooling play an integral part in the design and operation of a dc SQUID. The source of noise is looked at in an effort to minimize its effect. Cryocooling is essential to real world operation so different cooling strategies and their consequences are analyzed. This thesis focuses on modeling the behaviour of the dc SQUID to creating a practical system for use inside a SQUID microscope. Operating the dc SQUID with the appropriate electronics will linearize the device, reduce the effect of noise, and create a device with wide bandwidth. Each step in creating a practical system is discussed in detail. Simulations are used to create models predicting the behaviour of the dc SQUID and the electronics. They are then used to design and create practical electronic systems. Measurements are performed on Josephson junctions and dc SQUID magnetometers using the designed electronics. The Josephson junctions behave as predicted and were successfully tested. The dc SQUIDs did not behave as predicted and were not successfully tested. The SQUIDs were damaged, either by a malfunction in the cryocooler or through age related deterioration. A full test of the flux-locked loop was not possible and the dc SQUID was not linearized.

Thesis (MScEng (Electical and Electronic Engineering))--University of Stellenbosch, 2008. / A Cryogenic CMOS-based Control System for Testing Superconductor Electronics P.C. van Niekerk Department of Electrical and Electronic Engineering University of Stellenbosch Private Bag X1, 7602 Matieland, South Africa Thesis: M.Sc.Eng. (E&E) March 2008 A complete control system, with accompanying software, is designed to interface superconductive digital and sensory circuits for use in cryogenic vacuumed environments. It acts as an inter-mediator between superconductor electronics and room temperature electronics for research purposes. In order to facilitate low bit-error rate communications with superconductive electronics, the system is designed to have ultra low-noise current and voltage sources for transmitting data to superconductor electronics. Very high sensitivity voltage inputs are also implemented for data extraction from superconductor electronics. It implements both digital as well as analog design components, including ADC and DAC devices. The data is transmitted via a USB cable connection at 1Mbaud to a computer where the data is processed by specially designed software and graphically displayed for user interfaced research. Extensive research is done on the electronic components, such as CMOS devices, for functioning in an average temperature of 70 Kelvin inside cryogenic environments. This is done to reduce the thermal noise and heat transfer to superconductor electronics. An integrated temperature control system also ensures a stable environment for the electronics to operate at 70 K.