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The mechanical properties of PET (widely used in bottles and synthetic fibres) and Nylon 11 (also used in the fabrication of synthetic fibres) were studied over several decades of strain rate at different temperatures in an effort to provide a more complete description of these materials behaviour. Processing techniques can be improved if such information is available. Tests were carried out using a conventional Hounsfield machine and two in-house-developed dropweight and a cross bow systems from 10°C to 200°C. The three systems enable true stress vs. true strain curves to be calculated.

Thesis (PhD)--Stellenbosch University, 2015. / ENGLISH ABSTRACT: Macro synthetic fibres are known to significantly improve the toughness and energy absorption capacity of conventional concrete in the short term. However, since macro synthetic fibre are flexible and have relatively low modulus of elastic compared to steel fibres, it is uncertain if the improved toughness and energy absorption could be sustained over a long time, particularly under sustained tensile loadings. The main goal of this study is to investigate the time-dependent crack mouth opening response of macro synthetic fibre reinforced concrete (FRC) under sustained uniaxial tensile loadings, and to simulate the flexural creep behaviour. For the purpose of simulating the in-service time-dependent condition, all specimens were pre-cracked. Experimental investigations were carried out at three levels (macro, single fibre and structural) to investigate the time-dependent behaviour and the mechanisms causing it. At the macro level, compressive strength, uniaxial tensile strength and uniaxial tensile creep test at 30 % to 70 % stress levels of the average residual tensile strength were performed. To understand the mechanism causing the time-dependent response, fibre tensile test, single fibre pullout rate test, time-dependent fibre pullout test and fibre creep test were done. Flexural test and flexural creep test were done to simulate the structural level performance. The results of this investigation have shown significant drop in stress and increase in crack width of uniaxial tensile specimens after the first crack. The post cracking response has shown significant toughness and energy absorption capacity. Under sustained load at different stress levels, significant crack opening has been recorded for a period of 8 month even at a low stress level of 30 %. Creep fracture of specimens occurred at 60 % and 70 % indicating that these stress levels are not sustainable for cracked macro synthetic FRC. The single fibre level investigations have revealed two mechanisms responsible for the time-dependent crack widening of cracked macro synthetic FRC under sustained loading: time-dependent fibre pullout and fibre creep. In all cases of investigation, fibre failure was by complete pullout without rupture. Flexural creep results have shown that the crack opening increases over time. After 8 months of investigation, the total crack opening was 0.2 mm and 0.5 mm at 30 % and 50 % stress levels respectively. Since the crack opening of tensile creep and flexural creep specimens cannot be compared due to differences in geometry, specimen size, load transfer mechanisms and stress distribution in the cracked plane, a finite element analysis (FEA) was conducted. Material model parameters obtained from the uniaxial tensile test and viscoelastic parameters from curve fitting to experimental uniaxial creep results have been implemented to successfully predict the time-dependent crack opening of specimens subjected to sustained flexural loading. Analyses results correspond well with experimental result at both 30 % and 50 % stress levels. / AFRIKAANSE OPSOMMING: Makro sintetiese vesels is bekend daarvoor dat dit die taaiheid en energie absorpsie van konvensionele beton beduidend verbeter in die kort termyn. Aangesien makro sintetiese vesels buigsaam is met 'n relatiewe lae styfheidsmodulus in vergeleke met staalvesels, is dit onseker of die verhoogde kapasiteit vir energie absorpsie en taaiheid volgehou kan word oor die langer termyn, veral in gevalle waar dit aan volgehoue trekkragte blootgestel is. Die hoofdoel van die studie is om die tydafhanklike-kraakvergrotingsgedrag van makro sintetiese veselversterkte beton (VVB) wat blootgestel is aan volgehoue trekkragte te ondersoek asook die simulasie van die kruipgedrag in buig. Ten einde die werklike toetstande te simuleer is al die proefstukke doelbewus gekraak in 'n beheerde manier voor die aanvang van die toetse. Die eksperimentele ondersoek is uitgevoer op drie vlakke (makro, enkelvesel en strukturele) om die tydafhanklike gedrag sowel as die meganismes verantwoordelik vir hierdie gedrag te ondersoek. Op die makro-vlak is druktoetse gedoen saam met eenassige trek- en eenassige kruiptoetse met belastings tussen 30 % en 70 % van die gemiddelde residuele treksterkte. Om die meganisme wat die tydafhanklike gedrag veroorsaak te verstaan is veseltoetse, enkel vesel uittrektoetse, enkel vesel uittrek kruiptoetse asook kruiptoetse op vesels gedoen. Buigtoetse en buig kruiptoetse is ook gedoen om die gedrag op die strukturele vlak te ondersoek. Die resultate van hierdie ondersoek wys dat daar 'n beduidende val in spanning is en dat daar gepaardgaande kraak opening in die eenassige trek proefstukke plaasgevind het na die vorming van 'n kraak. Die na-kraak gedrag wys beduidende taaiheid en energie absorpsie kapasiteit. Gedurende die volgehoue trekbelasting by verskillende spanningsvlakke is beduidende kraakvergroting opgemerk, selfs by 30 % belasting na 8 maande. Kruipfaling het plaasgevind by proefstukke met belastings van 60 % en 70 % wat daarop wys dat hierdie spanningsvlakke nie geskik is vir gekraakte makro sintetiese VVB nie. Op die enkel veselvlak is twee meganismes geïdentifiseer wat verantwoordelik is vir die kraakvergroting oor tyd vir gekraakte makro sintetiese VVB met volgehoue trekbelasting: tydafhanklike vesel uittrek en vesel-kruip. In alle gevalle in hierdie ondersoek was die falingsmeganisme vesels wat uittrek. Buig kruiptoets resultate wys dat die krake vergroot oor tyd. Na 8 maande van ondersoek was die kraakwydtes 0.2 mm en 0.5 mm by 30 % en 50 % spanningsvlakke onderskeidelik. Aangesien die kraak opening van eenassige trek kruiptoetse en die buig kruiptoetse nie direk met mekaar vergelyk kan word nie weens die verskille in geometrie, proefstuk grootte en spanningsverdeling in die kraakvlak, is 'n eindige element analises (EEA) gedoen. Materiaal eienskappe is bepaal deur gebruik te maak van die eenassige kruip trektoets se resultate en viskoelastiese parameters is bepaal deur middel van kurwepassing van die resultate. Dit was gebruik om suksesvol die buig kruip kraak opening gedrag te simuleer. Die analises se resultate vergelyk goed met die eksperimentele data by beide 30 % en 50 % spanningsvlakke.

The purpose of this research was to determine uni-axial response of synthetic fibres required for structural design. The stress versus crack opening curves, required by RILEM for structural design of fibre reinforced concrete, were determined for each fibre type investigate and were used to compare the per fibre post-crack response, the pullout curves, and the flexural response. A study of the fibre distribution was conducted in order to determine the orientation factor required to predict the number of fibres expect in the tensile specimen crack face. The orientation factor, dosage, fibre geometry, and per fibre post-crack response were determined in order to predict the resulting tensile strength of a concrete mix. The tensile strength was compared to that of steel fibre currently being used in structural applications. The synthetic fibres tested only achieve a small percentage of their ultimate tensile strength; in order to produce synthetic fibres for structural applications, the bond strengths must be improved.

The use of asbestos fibres in construction products has been banned in European countries for about two decades due to its effect on human health. At present, many developing countries use asbestos cement board as one of the most important construction products for roofing, cladding and partition walls. The Hatschek process is the most commonly used method to produce asbestos Fibre Cement Board (FCB). There are two major problems for the asbestos FCB manufacturers in replacing their products with non-asbestos FCB. The first one is finding materials and fibres that are available and competitive in price compared to asbestos fibres, and the second is providing inexpensive machines and equipment to produce non-asbestos FCB. In this research, an effort has been made to solve these two major problems. After the initial laboratory investigations on several natural and synthetic fibres some of the fibres with potential use in FCB were chosen for the further investigations. A slurry vacuum dewatering process was then designed and made for the laboratory use. The performance of material selections and mix designs selected from the laboratory studies were subsequently verified with factory Hatschek process in a factory site trial. Many specimens with natural and synthetic fibres incorporating silica fume and limestone powder were made and tested in the laboratory. Silica fume and limestone powder were used for enhancing flexural strength and suppression of alkalinity to reduce breakdown of the cellulose fibres. The results of mechanical, physical and II durability tests were analysed. The microstructure of the fibres and composites was also studied by SEM (Scanning Electron Microscopy). At some stages, mix design optimization was carried out to gain the highest flexural strength. The most suitable mixes were chosen for the factory site trials. A number of full-scale non-asbestos trial boards were made successfully in an asbestos FCB factory and tested in accordance with the current national and international standards. The results indicated that the trial boards fulfilled the requirements of the relevant standards. Based on the outcome of this research, a combination of acrylic fibres and waste cardboard in a mix incorporating silica fume and limestone powder in addition to Portland cement can be used to replace asbestos fibres. Although broadly compatible with the asbestos cement production process, this formulation change will necessitate some changes to the existing production lines in asbestos cement factories to produce non-asbestos FCB.

[EN] Several efforts have been made in experimental and theoretical research about shear to understand all the variables that influence the phenomenon. Nowadays, however, due to its complexity, the shear performance of structural concrete elements, especially those without any traditional transversal reinforcement, continue with no clear explanation of the problem. Uncertainty about the problem grows when new variables like fibres are incorporated into the shear study. Research works have demonstrated the effectiveness of steel fibre in improving the mechanical properties of concrete elements. Experimental results reveal that steel fibres have proven effective in improving shear resistance, and they confer some concrete elements more ductility. In adequate amounts, steel fibres can completely or partially substitute traditional shear reinforcements. This is why international codes have included some requirements to take into account the action of fibres on the shear response of concrete elements. However, most recommendations and requirements for steel fibre-reinforced concrete (SFRC) were originally created. New fibres with different materials properties and shapes, such as macrosynthetic fibres, are now available on the market. These fibres, some of which are made of polypropylene, are an alternative in the construction industry given their properties and final cost. Initially, polypropylene fibres were used to control shrinkage cracking. Nevertheless, in the last decade the chemical industry has created larger fibres with better surface shapes, which allows polypropylene fibres to meet the requirements of international codes so they can be used in structural elements. Within this framework, the present PhD thesis aims to contribute to knowledge about fibre reinforced concrete (FRC), especially to study the effectiveness of polypropylene fibres when used as shear reinforcement. For this purpose, a literature review of the material, polypropylene fibre-reinforced concrete (PFRC) and its structural applications is first carried out. This study also discusses the parameters that affect the shear behaviour of traditional concrete and FRC. In order to evaluate the effectiveness of polypropylene fibres in shear, three experimental campaigns are presented. Each campaign represents a different level of study. The first corresponds to the material level, where the shear behaviour of PFRC is evaluated by push-off specimens. The second level involves studying shear in real scale elements. For this purpose, shear critical slender beams were manufactured and tested. The last level corresponds to real application of polypropylene fibres to act as shear reinforcement. In this campaign, deep hollow core slabs, with real sections and supports conditions, were tested. At each level, the shear behaviour of PFRC was evaluated against control reinforced concrete specimens, which were also tested during each campaign. / [ES] Varias investigaciones experimentales y teóricas han sido realizadas para entender el comportamiento a cortante de elementos de hormigón y sus variables. Sin embargo, hoy en día debido a la complejidad del tema, el comportamiento a cortante de elementos de hormigón armado y en especial aquellos que no tienen refuerzo transversal, continúan sin tener una explicación clara. Por otro lado, esta complejidad del cortante aumenta cuando nuevas variables, como las fibras, se incorporan al estudio. Investigaciones han demostrado la efectividad de las fibras de acero para mejorar las propiedades mecánicas de hormigón. Según resultados experimentales, la fibra de acero mejora la resistencia cortante y ductilidad de ciertos elementos. Y en cantidades adecuadas, la fibra puede sustituir total o parcialmente los refuerzos tradicionales de cortante. Es así que varios códigos internacionales han incluido requisitos para tener a las fibras en la respuesta estructural de elementos de hormigón. Sin embargo, estos requerimientos se han creado originalmente para el hormigón reforzado con fibra de acero (Steel fibre-reinforced concrete -SFRC). Nuevas fibras con diferentes materiales y formas, como las fibras macro-sintéticas, han sido introducidas en el mercado. Estas fibras, también llamadas fibras de polipropileno o poliolefina, son una alternativa en la construcción debido a su propiedades y costo final. Inicialmente, las fibras de polipropileno eran usadas únicamente en el hormigón para controlar la fisuración por retracción. Sin embargo, en la última década la industria química ha desarrollado fibras más grandes y con mejores prestaciones de adherencia, que permiten a estas fibras cumplir con requisitos para ser utilizadas estructuralmente. En este contexto, la presente tesis pretende ser una contribución al conocimiento sobre el hormigón reforzado con fibras (Fibre-reinforced concrete - FRC), especialmente en la efectividad de las fibras de polipropileno como refuerzo a cortante. Para esto, primero se realiza un estudio bibliográfico del hormigón reforzado con fibra de polipropileno (PFRC) como material y sus aplicaciones estructurales. Este estudio también tratará sobre los parámetros que afectan el comportamiento a cortante del hormigón tradicional y hormigón reforzado con fibras. Para evaluar la efectividad de las fibras de polipropileno en el cortante, se realizarán tres campañas experimentales. Cada campaña representa un nivel de estudio diferente. El primero es a nivel material en donde se evalúa el comportamiento a cortante a través de especímenes tipo Push-off. El segundo nivel, corresponde al estudio del cortante en elementos a escala real. Para esto se fabrican y ensayan vigas esbeltas críticas a cortante. El último nivel corresponde a una aplicación real de fibras de polipropileno actuando como refuerzo cortante. En esta campaña, se fabrican y ensayan placas alveolares de gran canto con secciones y condiciones de apoyos reales. / [CA] Diverses investigacions experimentals i teòriques han estat realitzades per entendre el comportament a tallant d'elements de formigó i les seues variables. No obstant això, hui en dia a causa de la complexitat del tema, el comportament a tallant d'elements de formigó armat i especialment aquells que no tenen reforç transversal, continuen sense tindre una explicació clara. D'altra banda, aquesta complexitat del tallant augmenta quan noves variables, com les fibres, s'incorporen a l'estudi. Investigacions han demostrat l'efectivitat de les fibres d'acer per a millorar les propietats mecàniques del formigó. Segons resultats experimentals, les fibres d'acer milloren la resistència a tallant i la ductilitat de certs elements. A més, en quantitats adequades, les fibres poden substituir total o parcialment els reforços tradicionals de tallant. És així que diversos codis internacionals han inclòs requisits per a tindre amb compte la resposta estructural de les fibres en els elements de formigó. No obstant això, aquests requeriments s'han creat originalment per al formigó reforçat amb fibres d'acer (Steel fibre-reinforced concrete -SFRC). Noves fibres amb diferents materials i formes, com les fibres macro-sintètiques, han estat introduïdes al mercat. Aquestes fibres, també anomenades fibres de polipropilè o poliolefina, són una alternativa a la construcció a causa de les seues propietats i cost final. Inicialment, les fibres de polipropilè eren usades únicament en el formigó per controlar la fissuració per retracció. No obstant això, en l'última dècada, la industria química ha desenvolupat fibres més grans i amb millors prestacions d'adherència, que permeten a aquestes fibres complir amb requisits per a ser utilitzades estructuralment. En aquest context, la present tesi pretén ser una contribució al coneixement sobre el formigó reforçat amb fibres (Fibre-reinforced concrete - FRC), especialment en l'efectivitat de les fibres de polipropilè com a reforç a tallant. Per això, primer es realitza un estudi bibliogràfic del formigó reforçat amb fibres de polipropilè (PFRC) com a material i les seues plicacions estructurals. Aquest estudi també tractarà sobre els paràmetres que afecten el comportament a tallant del formigó tradicional i del formigó reforçat amb fibres. Per avaluar l'efectivitat de les fibres de polipropilè en el tallant, es realitzaran tres campanyes experimentals. Cada campanya representa un nivell d'estudi diferent. El primer és a nivell material on s'avalua el comportament a tallant a través d'espècimens tipus Push-off. El segon nivell, correspon a l'estudi del tallant en elements a escala real. Per això es fabriquen i assagen bigues esveltes crítiques a tallant. L'últim nivell correspon a una aplicació real de fibres de polipropilè actuant com a reforç a tallant. En aquesta campanya, es fabriquen i assagen plaques alveolars de gran cantell amb seccions i condicions de suports reals. / Ortiz Navas, FR. (2020). Effectiveness of polypropylene fibres as shear reinforcement in structural elements [Tesis doctoral no publicada]. Universitat Politècnica de València. https://doi.org/10.4995/Thesis/10251/153147 / TESIS

Tunnels in hard and jointed rock are normally excavated in an arch shape to enable the rock mass to support its weight. Since the beginning of the 1980's, fibre reinforced shotcrete (FRS) in combination with rock bolts have been the dominating support method for hard rock tunnels. This type of rock support is a complex composite structure in which the structural behaviour depends on interaction between shotcrete, rock and bolts. The design is commonly based on a rock mass classification system in combination with analytical solutions or finite element (FE) modelling. However, the in-situ variations of important properties of the shotcrete are normally neglected.The aim of this thesis was to increase the understanding regarding the environmental impact of different fibre types used as reinforcement in shotcrete. First, a brief introduction to rock support and the role of shotcrete is presented. Along with this the technical performance and a short review regarding the production process involved in producing steel, synthetic and basalt fibres. To understand the environmental impact with respect to the production of different fibre types, environmental product declaration (EPD) from various producers were studied. Here, the environmental performance was studied from cradle to gate for the different fibres. The goal of this thesis was to study the global warming potential of fibres during the production stages and EPDs were used to compare the environmental performance for different fibres of different types and materials. For each fibre type different producers are also compared.To study the environmental impact, a case study in which the shotcrete should fulfil a specified residual flexural strength, or a minimum energy absorption was used. Within this thesis, any potential effects of deterioration of fibres or the need of technical improvement during the technical lifespan was not included. Fibre dosages to fulfil the structural performance were selected based on the experimental testing from the literature. Finally, a detailed discussion regarding the optimum dosages of the different fibre types and their environmental impact is presented.