Hundreds of thousands of vascular bypass grafts are implanted in the United States every year, but there has yet to be an ideal graft material to substitute for one’s own autologous vessel. Many synthetic materials have been shown to be successful vessel replacements; however, none have been proven to exhibit the same mechanical properties as native vessels, one of the most important criteria in selecting a vascular graft material. Part of this issue is due to the fact that, currently, there is no “gold standard” for testing the longitudinal and transverse tensile properties of small diameter tubular materials. While there are ASTM and ISO standards that suggest ways to test tubes in their original form, many researchers have published tensile strength data based on cutting the tube and testing it as a flat sample. Thus, it was the aim of this thesis to understand, establish, and implement accurate tensile testing methods of small diameter polymers in their original, tubular state on Cal Poly’s campus. Two test fixtures were created based on specified design criteria in order to test materials in their tubular form in both the longitudinal and transverse directions. Both fixtures were successful in testing PLGA and ePTFE samples, and statistical data was gathered for the transverse test fixture. The new transverse test fixture was tested against the current method of testing, and a significant (α = 0.05) difference between methods was established for ultimate tensile strength. This analysis, however, cannot determine which test method is more accurate, thus more extensive testing is required to verify the design of both fixtures. By developing a method for testing small diameter polymers in tubular form on Cal Poly’s campus, it allows for more testing of various small diameter tubes and more comparative data to validate each design. It also demonstrates a need for a more detailed and widespread standardization of testing for small diameter tubes, especially in vascular substitute applications where the ideal vessel replacement has yet to be found.

Three different polymers (a high-density polymer and two other polymers) were tested for use as an x-ray catheter in a radiation therapy application. This report describes the testing of these three materials to determine which material is the best option for a long use catheter. Tests included tensile, simulated clinical life, and other tests. Some testing was performed using nitrogen and an industrial coolant. Testing revealed significant non-circularities for some catheters. With increasing pressure, the circularity of these catheters increased. The tensile tests were performed on samples with varying doses of radiation. Tensile testing showed significant decreases in ultimate tensile strength with increasing radiation dose for both polyurethanes. Other testing was performed on the two polyurethanes to determine their compatibility with the industrial coolant. The test showed good compatibility with the coolant. Simulated clinical life tests were performed on a test fixture and with software to run the radiation source automatically for several hours at a time. Overall, one material was found to have very low ductility, made lower with increasing radiation. The material with the higher ductility was chosen as the better catheter material despite some disadvantages when compared to the stiffer polymer. This report describes necessary tests for thin polymer geometries used in applications where resistance to radiation, mechanical integrity, and coolant compatibility are the main considerations.

Composite materials are extensively used as an advanced engineering material, particularly in aerospace, automotive, and buildings industries due to its superior properties such as high strength to weight ratios and resistance to corrosion. As composite materials are rapidly replacing traditional materials in aircraft manufacturing, improved methods of identifying damage and critical failure is in development. One of the most commonly used procedures utilizes a health monitoring system that relies on transducers to monitor transmitted waves generated by ultrasonics. By replacing this method with a nanotechnology-based one, it is possible to efficiently detect damage without the time-extensive process of scanning the structure. This research investigated the development of a nanomaterial-based sensor for health monitoring of composite structures. To develop the sensor, carbon nanotube/epoxy mixture (2%wt CNT) was coated on a strand of E-glass fibre to be adhered onto a fiberglass composite specimen. The selection of E-glass fibre and fibreglass plate was largely due to its electrical insulating properties to demonstrate that the carbon nanotube is driving the sensing capabilities through its highly conductive nature. In addition, by adhering the coated E-glass fiber to a fibreglass coupon, the homogeneity and material properties were approximately maintained. Tensile testing of the specimen conducted through a Lloyd LD50 tensile testing machine provided data on the actual strain which was correlated with the experimental differential resistances measured by a multimeter, both at the same specified tensile loading conditions. With two sets of data, the experimental resistance data was calibrated with the actual strain data collected. Ultimately, the experimental sensors created a sample of gauge factors which represents 91.24% probability of replicating the observed range of gauge factors by using the same manufacturing procedures, providing a valid alternative and consistent method to detecting composite damage.

This thesis documents the tasks in support of the design and instrumentation of a miniature tensile load frame.

No description available.

This thesis focuses on the description of 3D printing technologies using the FDM method, which uses deposition of molten thermoplastics and their subsequent cooling and solidification layer by layer. This unique structure then shows a strong anisotropy of mechanical properties and, as a result, their testing and print settings are very important. Tensile testing of plastic materials, including indicators of mechanical properties, are described in this thesis according to ČSN EN ISO standard. The practical part presents the concept of a device capable of performing these tests. The block diagram indicates the functional elements and the connections among them. Tensile strength test is described together with results processing. Necessary product documentation is also included.

This thesis is part of an on going project within Autoliv Sweden AB to develop the process in changing the material in airbags. Most airbags are today constructed of fabric in polyamide 6.6 (PA6.6) and the thesis view the possibility of changing the material to one of three different polyesters (PET1, PET2, PET3). Both materials have different properties that have been looked into by two test methods, linear testing and dynamic testing with cold gas. The two testing methods were conducted on plain fabric and on fabric with seam to see differences in the materials when subjected to different stress caused by force or pressure. During testing the seam rupture was measured by filming the test sequences, and used for visual analysis. Tensile testing was conducted using a constant-rate-of-extension machine where the material is subjected to linear force until rupture. Dynamic testing was done with a cold nitrogen gas system using vessels to build up pressure that then releases towards the material putting it under stress. Tensile testing results for elongation do not have significant differences between testing in plain fabric or fabric with seam. PET2 have highest elongation in warp and weft. Visual analysis of specimens shows difference in how materials break, where the reference material in PA6.6 breaks more even than in PET materials. Dynamic testing show that the biggest seam opening do not occur at the highest pressure. In order to understand what is happening with the fabric during testing, three different times have been chosen in the pressure-time chart. Results in dynamic testing on fabric with seam show that PET3 have the smallest seam opening while reference material in PA6.6 has the largest opening. All PET materials have similar properties even if these are not always same as reference material in PA6.6. We can neither discard nor confirm our hypothesis of seam slippage and elongation relates equally in the same material independent of test method. From these results PET2 would not be recommended due to seam opens most at maximum force and the material has the biggest elongation. PET3 would be the recommended material, since seam opening is smallest at measured pressure. / Program: Textilingenjörsutbildningen

This Miniature mechanical testing study is concerned with the use of miniature specimens to identify the mechanical properties of stainless steel Type 304, sensitized Type 304 and SA516 Grade 70 carbon steel as a viable replacement for the standard sized mechanical testing. The study aims at obtaining suitable specimen geometry and tensile testing proce- dure for miniature mechanical testing whose mechanical properties are comparable to that of conventional specimens of ASTM A370-10 of the same steel. All specimens are at and the gauge length cross section will be varied to obtain suitable geometry. The miniature tensile testing results are further validated by using Monte Carlo Method (MCM) for uncertainty estimation in order to know the probability distribution of mechanical properties. Miniature specimens with a cross section of 3 mm2 and 12 mm gauge length are found to produce equiva- lent mechanical properties as tested from standard-sized specimens. If a reasonable agreement is received, it will provide us with a very useful tool to evaluate mechanical properties of de- graded materials, which cannot be removed from service for standard testing, for repair and service life evaluation.

Carbon nanotubes (CNTs) have been a major interest of study since 1991. A panel of properties and phenomena associated with carbon nanotubes due to their special combination of dimension, structure and topology have been investigated in the last years. Recently, it appears interesting to use carbon nanotubes at low loading content to obtain materials with enhanced mechanical and thermal properties. One of the major challenges is actually to disperse easily and individually these nanotubes in polymer matrices to obtain materials with increased properties for different application uses. Ethylene-vinyl acetate (EVA) copolymer is commonly used in cable industry. It is required to introduce high contents of alumina trihydrate (ATH) or magnesium dihydroxide (MDH) as fire retardant, to avoid fire hazards and reduce flammability. But this high mineral loading results in a decrease of the mechanical performances of the materials. This work aims at studying the influence of the incorporation of multiwall carbon nanotubes (MWNTs) on the tensile properties and the fire behavior of EVA nanocomposites. This work demonstrates, on one side, the significant effect of the previous nanotube coating by a thin layer of high density polyethylene (HDPE-coating) on the mechanical behavior of the so-obtained nanocomposites and explain, on the other side, the flame retardant efficiency of MWNTs in EVA nanocomposites. An original mechanism related to the action of the MWNTs during the combustion process is proposed and the effect of the HDE-coating on the cohesion of the residues is discussed.

This study focuses on the processing, structure and properties of polyacrylonitrile (PAN)/ carbon nanotube (CNT) composite carbon fibers. Small diameter PAN/CNT based carbon fibers have been processed using sheath-core and islands-in-a-sea (INS) fiber spinning technology. These methods resulted in carbon fibers with diameters of ~3.5 μm and ~1 μm (for sheath-core and INS respectively). Poly (methyl methacrylate) has been used as the sheath or the sea component, which has been removed prior to carbonization. These fibers have been stabilized and carbonized using a batch process. The effect of stabilization has been characterized by Fourier Transform Infrared Spectroscopy (FTIR), wide-angle X-ray diffraction (WAXD), and differential scanning calorimetry (DSC). A non-isothermal extent of cyclization (Mcyc) from the DSC kinetics study was developed in order to obtain an unbiased method for determining the optimal stabilization condition. The results of Mcyc were found to be in good agreement with the experimental FTIR and WAXD observations. The carbon fiber fracture surfaces have been examined using SEM. Various test parameters that affect the tensile properties of the precursor fiber (both PAN and PAN/CNT), as well as carbon fiber have been studied. In an attempt to validate single filament tests, fiber tow testing has also been done using standard test methods. Batch processed carbon fibers obtained via sheath-core geometry exhibited tensile strengths as high as 6.5 GPa, while fibers processed by islands-in-a-sea geometry exhibited strength values as high as 7.7 GPa.