Ce travail de thèse présente une étude théorique, numérique et expérimentale de l'intégration sur un guide d'onde diélectrique de chaînes de nanoparticules d'or supportant des résonances " plasmon de surface localisé ". Les guides d'onde à plasmon de surface localisé procurent un confinement sub-longueur d'onde de la lumière, ce qui permet d'envisager la réalisation de composants optiques ultra-compacts. Cependant, leurs pertes optiques élevées restreignent leur application à de courtes distances de propagation, contrairement aux guides d'onde diélectriques. Une combinaison judicieuse des deux types de guide doit donc permettre de bénéficier de leurs avantages respectifs. Dans un premier temps, nous avons étudié théoriquement les propriétés des chaînes des nanoparticules grâce à un modèle analytique basé sur l'approximation de dipôles ponctuels couplés, que nous avons développé. Cette étude a permis de déterminer la forme et les dimensions des nanoparticules qui ont ensuite été introduites dans un logiciel de FDTD pour simuler le couplage entre la chaîne de nanoparticules et le guide diélectrique (SOI ou en Si3N4). De cette étude numérique, nous avons déduit les géométries des structures à fabriquer. Les structures réalisées ont été caractérisées à l'aide d'un banc de transmission résolue spectralement, mis en place pendant cette thèse, et d'un système de mesures en champ proche optique en collaboration avec le LNIO (Troyes). Pour la première fois, nous avons montré expérimentalement les propriétés d'une chaîne courte de nanoparticules intégrée sur un guide SOI, ainsi que le phénomène de guides couplés entre une chaîne longue de nanoparticules et un guide SOI. Une valeur record de la constante de couplage a été obtenue, et ce, aux longueurs d'onde des télécoms (proche infrarouge). L'énergie lumineuse transportée par le mode TE du guide SOI peut ainsi être entièrement transférée au guide plasmonique en 4 ou 5 nanoparticules, soit une distance de propagation de moins de 600 nm. Nous avons également étudié les propriétés de réseaux de Bragg à base de plasmon de surface localisé en confrontant les résultats de mesures de transmission résolue spectralement aux résultats théoriques d'un modèle analytique basé à la fois sur l'approximation de dipôle ponctuel en régime quasi-statique et la théorie des modes couplés. Ces travaux ouvrent la voie à des applications de pinces optiques, de capteurs ou de spaser, qui bénéficieront de l'intégration de nanoparticules métalliques dans les circuits photoniques.

Les réseaux de diffraction sont largement utilisés dans le traitement optique de l'information. Toutefois, les applications nécessitent des efficacités de diffraction importantes, d'excellentes résolutions dans le domaine des fréquences spatiales et des temps de réponses appropriés à la fonction recherchée (grande durée de vie pour les mémoires, temps de réponses rapide pour les opérations de traitements de l'information...). Ces qualités étant difficiles à obtenir à l'aide des matériaux existants, une solution consiste à placer le matériau non-linéaire à l'intérieur d'une cavité Fabry-Pérot, avec le double avantage d'obtenir une efficacité de diffraction fortement accrue et une résolution dans le domaine des fréquences spatiales améliorée. Le mémoire rapporte comment l'utilisation d'un milieu intracavité amplificateur permet d'accroître encore davantage la puissance du faisceau diffracté, avec des efficacités de diffraction largement supérieures à l'unité. Les propriétés diffractives des réseaux d'indice et/ou de gain insérés dans un résonateur de Fabry-Pérot amplificateur de longueur supérieure ou égale à l'épaisseur du réseau sont analysées théoriquement et expérimentalement. Un modèle analytique a été élaboré et a permis de montrer l'immense potentiel de tels dispositifs, en terme de sélectivité angulaire et d'efficacité de diffraction, cette dernière pouvant être très largement supérieure à l'unité. Un dispositif expérimental a ensuite été conçu afin de prouver la faisabilité du concept et de valider le modèle analytique. Le milieu non-linéaire intracavité est un cristal de Nd:YVO4. Le réseau est inscrit optiquement par absorption de la figure d'interférence de deux faisceaux d'écriture. La diffraction du signal de lecture est analysée autour de la double résonance de Bragg et de Fabry-Pérot, ainsi qu'à proximité de l'une ou de l'autre résonance séparément, afin de remonter aux propriétés diffractives du réseau. Les résultats expérimentaux sont en bon accord avec les calculs numériques issus du modèle analytique. La comparaison avec le réseau de Bragg hors cavité montre l'amélioration significative apportée par la cavité amplificatrice: l'efficacité de diffraction est augmentée d'un facteur 5000 et la sélectivité angulaire d'un facteur proche de 20. Ces résultats sont très encourageants pour une application de ce type de dispositif au traitement optique de l'information, surtout dans le cas où une très forte sortance est nécessaire.

Bragg grating reflectors etched in amorphous silicon overlay films have been integrated with Ti:LiNbO3 optical waveguides. With a 12.5 mm long grating segment and an etch depth of ~ 93 nm in a 105 nm-thick silicon film, a narrow (0.05 nm) spectral bandwidth with a record high transmission dip (> 20 dB) was achieved at a wavelength of ~1542 nm for TE polarization on an x-cut, y-propagating substrate. The reflectance in the channel waveguides is found to be strongly dependent on the depth of the etched grating. The 3-dB bandwidth of 0.05 nm obtained for all tested samples is the smallest reported for waveguides in LiNbO3. The effect of the Bragg waveguide loss factor on the transmittance and reflectance spectra is investigated using a model for contra-directional coupling that includes an attenuation coefficient. The Bragg grating spectral characteristics are exploited to fabricate distributed Bragg feedback modulators (DBFM) and Bragg reflector Fabry-Perot modulators (BFPM). The sharp cut-off in transmission and reflection spectra, which is an inherent characteristic of Bragg grating, was tuned by applying voltage via the linear electrooptic effect, to produce intensity modulation. The Bragg grating based modulators consume less electric power compared to polarization intensity modulators (PIMs). The DBFM demonstrates 1/1.6 times the modulating voltage of a PIM with identical waveguide and electrode structure. The BFPM shows 1/3.3 times the modulating voltage of the PIM. No difference in the frequency response is observed among the three modulators. Comparison of the modulation sensitivity in the linear region indicates that the Bragg grating based modulators provide better sensitivity than that of the PIM with identical waveguide and electrode structure. These results indicate the potential advantage of the Bragg grating based modulators for enhanced modulation efficiency over conventional modulators. Further improvements can be expected from the optimization of the electrode design.

This thesis concerns various aspects of the durability offibre optic sensors embedded in composite. Since repair orreplacement of embedded sensors is not generally possible, thefunctional reliability of embedded sensors is one of the mostimportant prerequisites for successful use. The main researchobjective was to investigate the interaction between the sensorand the composite, and how this is affecting the mechanical andoptical sensor response. Fibre optic sensors embedded incomposite structures induce local stress concentrations whenthe composite is subjected to mechanical loads andenvironmental changes such as temperature and moisture. Acomplex transfer of stresses through the interfaces between theembedded sensor and the composite occurs and can result inlarge local stresses in the composite and a significant changein the response of the embedded sensor. These stressconcentrations make the interfaces susceptible todebonding. The sensor performance was studied experimentally andnumerically. Some basic results were generated for the EFPI andBragg grating sensors. The phase-strain response was determinedduring static and fatigue loading. The results showed that thesensors were more reliable in compression than in tensilestatic and fatigue loading. Generally, the sensor reliabilityduring loading was significantly improved for the Bragg gratingsensors over that of the EFPI sensor, as an effect of thesensor geometry. This was also demonstrated in theinvestigations on impacts. Impacts do not necessarily result indamage in the composite, but might cause debonding or otherfailure modes in the sensor area. Large, local stressconcentrations occur at several positions in the EFPI sensor,which pointed out that this sensor type was not suitable forembedded applications. The shift in focus from the sensor concept based on the EFPIsensor to that based on the Bragg grating sensor manifesteditself in several studies. The calculated deformation fieldaround an embedded optical fibre was verified in experimentsusing a high-resolution moiré interferometric technique.Furthermore, the improvement in the coating technology wasverified. A significant higher interfacial strength wasobtained with the silane-treated glass surface. The resultsindicated that at least a twofold improvement of the shearstrength was obtained. To simultaneously measure the in-plane strain components andthe temperature change, embedded Bragg grating sensors werearranged in a rosette configuration. The relationship betweenthe optical response from each sensor and the strains in thelaminate was numerically and analytically established. Damage lead to stress redistribution in the sensor region,which may influence the output from the embedded Bragg gratingsensor. The effect was numerically evaluated for interfacialdamage, and was compared to that of a sensor with undamagedinterface. The results showed that debonding might have asignificant influence, in particular for combined thermal andmechanical loading. <b>Keywords</b>: composites, fibre optic sensor, embedded, EFPIsensor, Bragg grating sensor, durability, fatigue, impact,strain measurement, interface, stress analysis

The different topics of this thesis include high-temperaturestable fiber Bragg gratings, photosensitivity and fiber basedcomponents. Fiber Bragg gratings (FBG) are wavelength dispersiverefractive index structures manufactured through UV exposure ofoptical fibers. Their applications range from WDM filters,dispersion compensators and fiber laser resonators fortelecommunication applications to different types of point ordistributed sensors for a variety of applications. One aim of this thesis has been to study a new type of FBGreferred to as chemical composition grating. These gratingsdiffer from other types of FBG in that their refractive indexstructure is attributed to a change in the chemicalcomposition. Chemical composition gratings have shown to beextremely temperature stable surviving temperatures in excessof 1000 oC. Photosensitivity of pure silica and germanium-dopedcore fibers in the presence of hydroxyl groups has also beenstudied and different types of fiber based components have beendeveloped. The main result of the thesis is a better understanding ofthe underlying mechanism of the formation of chemicalcomposition gratings and their decay behavior at elevatedtemperatures. The refractive index modulation is caused by aperiodic change in the fluorine concentration, which has beenverified through time-of-flight secondary-ion-mass spectrometryand through studies of the decay behavior of chemicalcomposition gratings. A model based on diffusion of dopants hasbeen developed, which successfully predicts the thermal decayat elevated temperatures. Studies of the dynamics of chemicalcomposition grating formation have resulted in a manufacturingtechnique that allows for reproducible gratingfabrication. The main results regarding photosensitivity is a method tosignificantly increase the effect of UV radiation on standardtelecommunications fiber. The method, referred to asOH-flooding, has also been applied to pure-silica core fibersresulting in the first report of strong grating formation insuch fibers. Finally, research into different schemes for developingfiber-based components has resulted in two types of singlefiber integrated Mach-Zehnder interferometers; one passiveinterferometer that can be used as an optical filter and oneactive interferometer controlled with internal metalelectrodes. Keywords:optical fibers, fiber Bragg gratings,photosensitivity, thermal stability, fiber sensors, chemicalcomposition gratings, fiber components, Mach-Zehnderinterferometer, optical switch, optical modulator. / QC 20100607

This thesis describes research on near degenerate quasi phase-matched opticalparametric oscillators (OPO) where volume Bragg gratings (VBG) are used toproduce narrow oscillation bandwidth. These OPOs are then used to pump a secondOPO to generate mid-infrared radiation. The atmospheric transmission windows in the 3.5 to 5 μm wavelength region areused for seekers on infrared homing missiles. These missiles are available to guerrillaand terrorist groups and have been used in a number of attacks on military and civilianaircraft. Laser sources at the same wavelengths are an important component incountermeasure systems for aircraft self-protection. Similar laser sources also haveapplications in laser surgery. At wavelengths longer than 4 μm crystal materials for multi-Watt level averagepower nonlinear devices is a problem. The best solution so far is to use ZnGeP2(ZGP). ZGP and the available alternatives all have a problem of near-infraredabsorption, and a mid-infrared OPO thus has to use a pump wavelength near 2 μm.This pump source can be a neodymium laser at 1.06 μm with a near degenerate OPO. Nonlinear devices for low to medium pulse energies are dominated by quasi phasematchedmaterials because of their higher effective nonlinearities and lack of walkoff.In addition they allow type I interaction where signal and idler from the OPOhave the same polarization, which has the advantage that both waves can be used topump the ZGP OPO. The drawback of this is that the near-degenerate interaction hasvery wide gain bandwidth. Efficient pumping of the second OPO demands narrowbandwidth output from the first OPO.Volume Bragg gratings that are glass materials with a periodic refractive indexmodulation have emerged as high quality narrow bandwidth reflectors. By using aVBG as one cavity mirror in an OPO the feedback bandwidth and hence the OPOoscillation bandwidth can be kept very narrow. Signal and idler bandwidths of 10 and20 GHz (FWHM) at 2122 and 2135 nm, respectively, have been demonstrated. Thisshould be compared to the several hundred nanometre bandwidth from an OPO usingdielectric mirrors. Very narrow bandwidth operation has been achieved so close todegeneracy that the signal and idler are not resolvable. The total output energy generated in the PPKTP OPO (signal and idler together)has been used to pump a ZGP OPO that produced mid-IR radiation. Tuning of thesignal from a ZGP OPO from 2.9 μm to degeneracy at 4.3 μm has been shown, with acorresponding idler wavelength tuneable up to 8 μm. The highest conversionefficiency that has been reached from 1.06 μm to the mid-IR was 12 %. This setupused a PPKTP OPO with 30 % conversion efficiency and 13 nm separation of signaland idler (2122 and 2135 nm). The pulse repetition frequency was 20 kHz and thegenerated output power in the mid-IR was 3.2 W. / QC 20100517

Theoretical and experimental studies of real-time interrogation of fiber Bragg grating (FBG) sensors based on chirped pulse compression with increased interrogation resolution and signal-to-noise ratio are presented. Two interrogation systems are proposed in this thesis. In the first interrogation system, a linearly chirped FBG (LCFBG) is employed as the sensing element. By incorporating the LCFBG in an optical interferometer as the sensor encoding system, employing wavelength-to-time mapping and chirped pulse compression technique, the correlation of output microwave waveform with a chirped reference waveform would provide an interrogation result with high speed and high resolution. The proposed system can provide an interrogation resolution as high as 0.25 μ at a speed of 48.6 MHz. The second interrogation system is designed to achieve simultaneous measurement of strain and temperature. In this system, a high-birefringence LCFBG (Hi-Bi LCFBG) is employed as a sensing element.

Fiber Bragg gratings (FBGs) are key elements in modern telecommunication and sensing applications. In optical communication, with the advancement of the Erbium doped fiber amplifier (EDFA), there is a great demand for devices with wavelength tunability over the Erbium gain bandwidth (in particular, for wavelength division multiplexing (WDM) networks). The center wavelength of a FBG can be shifted by means of change of temperature, pressure or mechanical axial strain. The axial strain approach is the best method among all other techniques because it allows relatively large wavelength shifts with high speed. Axial strain of up to 4% will be required to cover the whole EDFA region (more than 40 nm of central wavelength shift). The formation of Bragg grating results in significant reduction in mechanical strength of optical fibers especially in tension. As a result, axial strain of only about 1% can be achieved by mechanical stretching of FBGs. In order to achieve the remaining 3% strain compression of FBGs has to be applied. In this thesis, the design and analysis of a novel device for achieving central wavelength shift are presented. In particular, the device has achieved, for a fiber with 12 mm FBG, a shifting of 46 nm in compression and 10.5 nm in tension with a reflection power loss of less than 0.25 dB and a FWHM bandwidth variation of approximately 0.1 nm. Both variations are well below the Bellcore standards requirement of 0.5 dB for peak reflectivity variation and 0.1 nm for bandwidth variation. The device consists of two fixed and one guiding ferrules. The difficulties associated with compressing the FBG were handled by carefully selecting tolerances and adjustment procedures. The device allows both tension and compression of FBGs, and the use of different FBG lengths and actuators. The effects of glue deformation and bending of the FBG during compression were analyzed in detail. Further, using the piezoelectric transducer (PZT) actuator as a driver, tuning speed of around 1.5nm/ms was achieved.

Theoretical and experimental studies of real-time interrogation of fiber Bragg grating (FBG) sensors based on chirped pulse compression with increased interrogation resolution and signal-to-noise ratio are presented. Two interrogation systems are proposed in this thesis. In the first interrogation system, a linearly chirped FBG (LCFBG) is employed as the sensing element. By incorporating the LCFBG in an optical interferometer as the sensor encoding system, employing wavelength-to-time mapping and chirped pulse compression technique, the correlation of output microwave waveform with a chirped reference waveform would provide an interrogation result with high speed and high resolution. The proposed system can provide an interrogation resolution as high as 0.25 μ at a speed of 48.6 MHz. The second interrogation system is designed to achieve simultaneous measurement of strain and temperature. In this system, a high-birefringence LCFBG (Hi-Bi LCFBG) is employed as a sensing element.

The focus of this thesis is on the development of sensing devices based on optical fiber sensors, specifically optical Fiber Bragg Gratings (FBG), using laser microfabrication methods. FBG is a type of optical fibers whose spectral response is affected by applied strain and temperature. As a result, it can be calibrated for the measurement of physical parameters manifesting themselves in the changes of strain or temperature. The unique features of optical fiber sensors such as FBGs have encouraged the widespread use of the sensor and the development of optical fiber-based sensing devices for structural measurements, failure diagnostics, thermal measurements, pressure monitoring, etc. These features include light weight, small size, long-term durability, robustness to electromagnetic disturbances, and resistance to corrosion. Despite the encouraging features, there are some limitations and challenges associated with FBGs and their applications. One of the challenges associated with FBGs is the coupling of the effects of strain and temperature in the optical response of the sensors which affects the reliability and accuracy of the measurements. Another limitation of FBGs is insensitivity to the index of refraction of their surrounding medium. In liquids, the index of refraction is a function of concentration. Making FBGs sensitive to the index of refraction and keeping their thermal sensitivity intact enable optical sensors with the capability of the simultaneous measurement of concentration and temperature in liquids. Considering the unique features of FBGs, embedding of the sensors in metal parts for in-situ load monitoring is a cutting-edge research topic. Several industries such as machining tools, aerospace, and automotive industries can benefit from this technology. The metal embedding process is a challenging task, as the thermal decay of UV-written gratings can starts at a temperature of ~200 oC and accelerates at higher temperatures. As a result, the embedding process needs to be performed at low temperatures. The objective of the current thesis is to move forward the existing research front in the area of optical fiber sensors by finding effective solutions to the aforementioned limitations. The approaches consist of modeling, design, and fabrication of new FBG-based sensing devices. State-of-the-art laser microfabrication methods are proposed and implemented for the fabrication of the devices. Two approaches are adopted for the development of the FBG-based sensing devices: the additive method and the subtractive method. In both methods, laser direct microfabrication techniques are utilized. The additive method deals with the deposition of on-fiber metal thin films, and the subtractive method is based on the selective removal of materials from the periphery of optical fibers. To design the sensing devices and analyze the performance of the sensors, an opto-mechanical model of FBGs for thermal and structural monitoring is developed. The model is derived from the photo-elastic and thermo-optic properties of optical fibers. The developed model can be applied to predict the optical responses of a FBG exposed to structural loads and temperature variations with uniform and non-uniform distributions. The model is also extended to obtain optical responses of superstructure FBGs in which a secondary periodicity is induced in the index of refraction along the optical fiber. To address the temperature-strain coupling in FBGs, Superstructure FBGs (SFBG) with on-fiber metal thin films are designed and fabricated. It is shown that SFBGs have the capability of measuring strain and temperature simultaneously. The design of the sensor with on-fiber thin films is carried out by using the developed opto-mechanical model of FBGs. The performance of the sensor in concurrent measurement of strain and temperature is investigated by using a customized test rig. A laser-based Direct Write (DW) method, called Laser-Assisted Maskless Microdeposition (LAMM), is implemented to selectively deposit silver thin films on optical fibers and fabricate the superstructure FBGs. To attain thin films with premium quality, a characterization scheme is designed to study the geometrical, mechanical, and microstructural properties of the thin films in terms of the LAMM process parameters. A FBG, capable of measuring concentration and temperature of liquids is developed, and its performance is tested. Femtosecond laser micromachining is successfully implemented as a subtractive method for the sensor fabrication. For this purpose, periodic micro-grooves are inscribed in the cladding of regular FBGs so as to increase their sensitivity to the concentration of their surrounding liquid while keeping their thermal sensitivity intact. This type of sensors has the potential for applications in biomedical research, in which the in-situ measurement of the properties of biological analytes is required. Another accomplishment of this thesis is the development of FBG sensors embedded in metal parts for structural health monitoring using low temperature embedding processes. In this regard, the opto-mechanical model is extended to predict the optical response of the embedded FBGs. The embedding process involves low temperature casting, on-fiber thin film deposition, and electroplating methods. The performance of the embedded sensors is evaluated in structural loading and thermal cycling.