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  • About
  • The Global ETD Search service is a free service for researchers to find electronic theses and dissertations. This service is provided by the Networked Digital Library of Theses and Dissertations.
    Our metadata is collected from universities around the world. If you manage a university/consortium/country archive and want to be added, details can be found on the NDLTD website.
51

Development of a forced-convection gas target for improved thermal performance

Uittenbosch, T., Buckley, K., Schaffer, P., Hoehr, C. 19 May 2015 (has links) (PDF)
Introduction The internal pressure experienced by a gas tar-get during irradiation is dependent on the beam energy deposited in the target, the beam cur-rent, and the thermal behaviour of the target. [1] The maximum beam energy deposited is a function of the cyclotron capabilities and the gas inventory within the target. The maximum beam current is limited by the pressure produced in the target and the ability of the target assembly to remain intact. This is also a function of the thermal behaviour of the target, which is difficult to predict a priori since it is dependent on such things as convection currents that occur during irradiation. We conducted bench tests with model gas targets with and without forced convection currents to observe the effect on thermal behaviour. Based on those results we constructed a prototype gas target, suitable for irradiation, with an internal fan assembly that is rotated via external magnets. Material and Methods Bench tests were conducted with cylindrical and conical target bodies of aluminum. A nickel-chromium heater wire was inserted into the gas volume through the normal beam entrance port (FIGURE 1) to heat the gas while water cooling was applied to the target body. The voltage and current of the heater coil was monitored along with the pressure inside the target and the water inlet and outlet temperature. In the case of tests with a driven fan blade either the voltage applied to the electric motor was monitored or the fan speed itself was recorded. By assuming the ideal gas law, the pressure gives the average bulk temperature and a global heat transfer coefficient can be calculated between the target gas and the cooling water. [2] A cylindrical target body was constructed that incorporated a fan blade driven by an external motor. This assembly used a simple o-ring seal on the rotating shaft. This seal was not robust enough for any tests under beam conditions. A prototype design suitable for in-beam operation employs a propeller mounted on a rotating disc housing two samarium cobalt magnets and spinning on two micro-bearings which are constructed to operate in high temperature environments. The micro-bearings are mounted on a pin projecting from a plate welded to the back of the gas target to allow assembly of the fan mechanism prior to attachment to the body (FIGURE 2).
52

Visual observation of boiling in batch-style water targets

Peeples, J., Stokely, M., Poorman, M., Magerl, M., Wieland, B. 19 May 2015 (has links) (PDF)
Introduction Batch-style water targets used for F-18 production are known to operate under boiling conditions in the target irradiation chamber, but the distribution of vapor under steady-state conditions was previously unknown. Thermal performance of batch targets has been correlated to average void in the target [1], but the simplified assumptions of such models do not represent the true non-uniform boiling behavior. Visualization targets can be used to observe boiling inside of a target during operation [2–5]. Commercial BTI targets operate at 28–35 bar (400–500 psi) with heat inputs of 0.5 to 3 kW and fill volumes of 1 to 4 mL. Recently, a visualization target featuring two transparent viewing windows was used to observe boiling conditions for realistic operating beam power, target pressure, and fill volume [4]. The same methodology has been applied to three additional visualization targets to examine the effect of target geometry on observed boiling phenomena. Material and Methods The original visualization target featured an aluminum body with a 0.127 mm (0.005 inch) integral aluminum beam window and two viewing windows made of optically clear sapphire (Al2O3). It was operated on an IBA 18/9 cyclotron with 18 MeV protons at beam power up to 1.1 kW, for pressures of 5 to 21 bar (70 to 300 psi), and a fill volume of 2.5 mL. All of the new designs featured a wider chamber to allow for higher beam transmission and an increased chamber height, consistent with cur-rent trends in high power targets. One target featured a reduced chamber depth, and another had a ramp in the back of the chamber to reduce fill volume. Target pressure was limited to a maximum of 14 bar (200 psi) due to the larger diameter beam window. A video camera was used to record the boiling conditions observed for each target under several lighting conditions. During irradiation, the proton beam excites the water molecules, producing visible blue light emissions during de-excitation. These light emissions provide a good indication of beam distribution and penetration depth. A strong backlight can be used to produce clearer images of bubbles generated during boiling. Results and Conclusion Proton range and visible blue light emissions were recorded in dark ambient conditions. The width of the Bragg peak and natural circulation in the bulk fluid were visible with good ambient lighting. Size and distribution of vapor bubbles could be observed by using a strong backlight. The beam current was increased gradually to determine the thermal limit for each target for several fill volumes and pressures. Two thermal limits were observed which resulted in some beam penetration in the top region of the beam. For lower fill volumes, steam ac-cumulates in or around the helium overpressure bubble, causing the helium bubble to move into the upper region of the beam. For higher fill volumes, beam penetration occurs due to excessive voiding, when bubbles produced in the beam region cannot rise quickly enough out of the path of the beam.
53

Electronic transport in semiconductors

Vuong, T. H. H. January 1985 (has links)
The first part of this thesis is a study of thermally activated conduction, Hall effect, and Far-Infrared absorption in n-InP. Accurate measurements of threshold energies are deduced from the temperature dependence of these effects, after correction for Fermi level variations, and it is shown that the threshold for electrical conduction is higher than for Hall effect, or cyclotron resonance. An explanation is given in terms of the long range impurity potential fluctuations. The second part of this thesis presents measurements of the thermopower in heterostructures for the GaInAs - InP, GaInAs - InAlAs, and GaAs - GaAlAs systems, with and without magnetic field, for temperature varying from 2K to 10K. In high magnetic fields, strong oscillations of the thermopower are seen, with the same phase as the Shubnikov - de Haas oscillations in the resistivity, in accordance with theory. The magnitude and temperature dependence of the thermopower are mostly as predicted for the superlattice but those of the heterojunctions disagree with the predictions. A discussion of the cause of this disagreement is given. In the final part, the value of the relative energy shift between different valleys of the conduction band of a thin film of PbTe grown on BaF<sub>2</sub> is obtained. This will be used to obtain the deformation potential of PbTe.
54

A study of tokamak energy and particle transport, based on modulated electron cyclotron resonance heating

Deliyanakis, Nicholas January 1989 (has links)
A dynamical technique for the study of tokamak energy and particle transport has been developed. The plasma in the medium-sized DITE tokamak was perturbed by the application of modulated electron cyclotron resonance heating, with wave-launching from the high-field side. These experiments were carried out with absorption at various distances from the plasma centre, over a range of densities. Energy transport through the electron channel was dominant, and the variations in electron temperature and density were measured using the soft X-ray, electron cyclotron emission and microwave interferometer diagnostics. Analysis in the frequency domain enabled the propagation of the thermal wave to be followed. The observed behaviour was generally indicative of diffusive propagation of the thermal perturbation. Further observations indicated a modulation of the horizontal plasma shifts, diffusive propagation to the edge and a low modulation level of line-averaged density. In some atypical cases, the observed behaviour was qualitatively different; this type of behaviour was accompanied by a pronounced sawtooth oscillation locked with the modulation. Two models have been employed for the interpretation of these results. The first model, based on the diffusive thermal transport of the perturbation, has led to results in good agreement with the experimental data. Values of the electron thermal diffusivity were deduced, in good agreement with those obtained from the alternative techniques of power balance analysis and sawtooth heat pulse propagation analysis; such agreement has not been universally obtained in similar experiments. The width of the absorption region has emerged as an important consideration in this analysis. A more complex model, including non-linear, coupled equations of particle and energy balance, has produced results in partial agreement with the experimental data, supporting, to some extent, the presence of coupled transport. It has been demonstrated how perturbation techniques can afford a useful means of testing transport models.
55

Characterization of histone post-translational modification using reversed-phase high performance liquid chromatography and fourier transform ion cyclotron resonance mass spectrometry

Zhang, Liwen, January 2003 (has links)
Thesis (Ph. D.)--Ohio State University, 2003. / Title from first page of PDF file. Document formatted into pages; contains xv, 219 p.; also includes graphics (some col.) Includes bibliographical references (p. 147-173). Available online via OhioLINK's ETD Center
56

Fourier transform ion cyclotron resonance mass spectrometry instrumentation and methods for structural characterization of trapped biomolecular ions innovative MS/MS techniques, gas-phase hydrogen/deuterium exchange, and laser-induced fluorescence /

McFarland, Melinda A. Marshall, Alan G., January 2004 (has links)
Thesis (Ph. D.)--Florida State University, 2004. / Advisor: Dr. Alan G. Marshall, Florida State University, College of Arts and Sciences, Dept. of Chemistry and Biochemistry. Title and description from dissertation home page (viewed Jan. 12, 2005). Includes bibliographical references.
57

Development and evaluation of the central trapping electrode trapped-ion cell for Fourier transform mass spectrometry /

Ostrander, Chad Michael, January 2000 (has links)
Thesis (Ph. D.)--University of Texas at Austin, 2000. / Vita. Includes bibliographical references. Available also in a digital version from Dissertation Abstracts.
58

Examination of gas-phase conformations of oligonucleotides using electrospray ionization Fourier transform ion cyclotron resonance mass spectrometry /

Robinson, Jessica Marie, January 1998 (has links)
Thesis (Ph. D.)--University of Texas at Austin, 1998. / Vita. Includes bibliographical references (leaf 171). Available also in a digital version from Dissertation Abstracts.
59

Development and application of an on-line liquid chromatography interface for the analysis of biomolecules by Fourier transform ion cyclotron resonance mass spectrometry /

Harper, Carla Jo, January 1998 (has links)
Thesis (Ph. D.)--University of Texas at Austin, 1998. / Vita. Includes bibliographical references (leaves 183-195). Available also in a digital version from Dissertation Abstracts.
60

Observation and control of ion motion in fourier transform ion cyclotron resonance mass spectrometry /

Schmidt, Eric Grayson, January 1999 (has links)
Thesis (Ph. D.)--University of Texas at Austin, 1999. / Vita. Includes bibliographical references (leaves 219-228). Available also in a digital version from Dissertation Abstracts.

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